DE2512044A1 - Verfahren zur herstellung von granulen mit verminderter neigung zur bildung von staub und nach dem verfahren hergestellte granulen - Google Patents
Verfahren zur herstellung von granulen mit verminderter neigung zur bildung von staub und nach dem verfahren hergestellte granulenInfo
- Publication number
- DE2512044A1 DE2512044A1 DE19752512044 DE2512044A DE2512044A1 DE 2512044 A1 DE2512044 A1 DE 2512044A1 DE 19752512044 DE19752512044 DE 19752512044 DE 2512044 A DE2512044 A DE 2512044A DE 2512044 A1 DE2512044 A1 DE 2512044A1
- Authority
- DE
- Germany
- Prior art keywords
- granules
- detergent
- coating
- dust
- dusting tendency
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000008187 granular material Substances 0.000 title claims abstract description 88
- 239000003599 detergent Substances 0.000 title claims abstract description 19
- 239000000843 powder Substances 0.000 title claims description 5
- 238000010410 dusting Methods 0.000 title abstract description 5
- 230000003014 reinforcing effect Effects 0.000 title abstract 2
- 102000004190 Enzymes Human genes 0.000 claims abstract description 20
- 108090000790 Enzymes Proteins 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 14
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 11
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 239000000741 silica gel Substances 0.000 claims abstract description 7
- 229910002027 silica gel Inorganic materials 0.000 claims abstract description 7
- 239000005018 casein Substances 0.000 claims abstract description 5
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims abstract description 5
- 235000021240 caseins Nutrition 0.000 claims abstract description 5
- 229920000159 gelatin Polymers 0.000 claims abstract description 5
- 235000019322 gelatine Nutrition 0.000 claims abstract description 5
- 235000010265 sodium sulphite Nutrition 0.000 claims abstract description 5
- 108010010803 Gelatin Proteins 0.000 claims abstract description 4
- 239000008273 gelatin Substances 0.000 claims abstract description 4
- 235000011852 gelatine desserts Nutrition 0.000 claims abstract description 4
- 238000000576 coating method Methods 0.000 claims description 31
- 239000011248 coating agent Substances 0.000 claims description 29
- 239000000428 dust Substances 0.000 claims description 12
- 239000007787 solid Substances 0.000 claims description 10
- 238000002844 melting Methods 0.000 claims description 6
- 230000008018 melting Effects 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000000155 melt Substances 0.000 claims 1
- 238000003860 storage Methods 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 238000001816 cooling Methods 0.000 abstract description 2
- 239000000463 material Substances 0.000 description 21
- 229940088598 enzyme Drugs 0.000 description 18
- 239000000203 mixture Substances 0.000 description 13
- 239000011368 organic material Substances 0.000 description 10
- -1 water-soluble Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 6
- 239000007931 coated granule Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000011049 pearl Substances 0.000 description 5
- 108091005804 Peptidases Proteins 0.000 description 4
- 239000004365 Protease Substances 0.000 description 4
- 102000005158 Subtilisins Human genes 0.000 description 4
- 108010056079 Subtilisins Proteins 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 239000010419 fine particle Substances 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 3
- 230000003625 amylolytic effect Effects 0.000 description 3
- 235000014113 dietary fatty acids Nutrition 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000000194 fatty acid Substances 0.000 description 3
- 229930195729 fatty acid Natural products 0.000 description 3
- 102000013142 Amylases Human genes 0.000 description 2
- 108010065511 Amylases Proteins 0.000 description 2
- 235000019418 amylase Nutrition 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 230000009931 harmful effect Effects 0.000 description 2
- 239000001814 pectin Substances 0.000 description 2
- 235000010987 pectin Nutrition 0.000 description 2
- 229920001277 pectin Polymers 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000002797 proteolythic effect Effects 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 229960001922 sodium perborate Drugs 0.000 description 2
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 description 2
- 239000004382 Amylase Substances 0.000 description 1
- 244000063299 Bacillus subtilis Species 0.000 description 1
- 235000014469 Bacillus subtilis Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 239000001828 Gelatine Substances 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 102000035195 Peptidases Human genes 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000001464 adherent effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229940025131 amylases Drugs 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 235000001727 glucose Nutrition 0.000 description 1
- 239000003752 hydrotrope Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 230000002366 lipolytic effect Effects 0.000 description 1
- 125000003071 maltose group Chemical group 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38672—Granulated or coated enzymes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/003—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic followed by coating of the granules
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1215674 | 1974-03-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2512044A1 true DE2512044A1 (de) | 1975-09-25 |
Family
ID=9999373
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752512044 Pending DE2512044A1 (de) | 1974-03-19 | 1975-03-19 | Verfahren zur herstellung von granulen mit verminderter neigung zur bildung von staub und nach dem verfahren hergestellte granulen |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE2512044A1 (enExample) |
| DK (1) | DK109675A (enExample) |
| NL (1) | NL7503115A (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1991017235A1 (en) * | 1990-05-04 | 1991-11-14 | Genencor International, Inc. | Granules containing both an enzyme and an enzyme protecting agent and detergent compositions containing such granules |
-
1975
- 1975-03-17 NL NL7503115A patent/NL7503115A/xx unknown
- 1975-03-18 DK DK109675A patent/DK109675A/da unknown
- 1975-03-19 DE DE19752512044 patent/DE2512044A1/de active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1991017235A1 (en) * | 1990-05-04 | 1991-11-14 | Genencor International, Inc. | Granules containing both an enzyme and an enzyme protecting agent and detergent compositions containing such granules |
Also Published As
| Publication number | Publication date |
|---|---|
| DK109675A (enExample) | 1975-09-20 |
| NL7503115A (nl) | 1975-09-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE69605009T2 (de) | Enzymhaltiges granulat und verfahren zu seiner herstellung | |
| DE69836348T2 (de) | Granulat enthaltend hydratisiertes sperrmaterial | |
| DE69632638T2 (de) | Mikrogranulaten zur nahrungs- oder futteranwendung | |
| DE69519944T2 (de) | Umhüllte enzymgranulate | |
| DE2730481C3 (de) | Verfahren zur Herstellung eines Enzymgranulats | |
| DE3882301T2 (de) | Enzymhaltiges Granulat und dessen Herstellungsverfahren. | |
| DE3689727T2 (de) | Granulierungsverfahren für enzyme. | |
| EP0707628B1 (de) | Umhüllte enzymzubereitung für wasch- und reinigungsmittel | |
| EP0191396B2 (de) | Verfahren zur Herstellung eines rieselfähigen Granulats | |
| EP0656058B1 (de) | Neue enzymgranulate | |
| EP0716685B1 (de) | Mehrenzymgranulat | |
| DE2831778B2 (de) | Verfahren zur Herstellung enzymhaldger Teilchen | |
| DE2137042A1 (de) | Verfahren zur Herstellung neuer Enzymaufbereitungen | |
| EP0522269B1 (de) | Verfahren zur Herstellung von Enzymzubereitungen | |
| DE102004021384A1 (de) | Verfahren zur Herstellung von Granulaten mit verbesserter Lagerstabilität und Abriebfestigkeit | |
| DE2435008A1 (de) | Verfahren zum ueberziehen von in wasser loeslichen oder dispergierbaren partikeln nach der fliessbettechnik | |
| DE2232354A1 (de) | Verfahren zur herstellung von enzympraeparaten | |
| WO1998026037A2 (de) | Umhüllte enzymzubereitung mit verbesserter löslichkeit | |
| DE2602260A1 (de) | Verfahren zur herstellung enzymhaltiger tierfuttermittel | |
| DE69403207T2 (de) | Wirbelbett beschichtete amidoperoxysäure enthaltende bleichmittel zusammentzung | |
| EP0246554B1 (de) | Enzymatische Backmittel | |
| DE2137043A1 (de) | Neues Enzympräparat und Verfahren zu seiner Herstellung | |
| EP0847243A1 (de) | Rieselfähiges granulat auf basis organischer säuren, verfahren zu seiner herstellung und seine verwendung | |
| DE2512044A1 (de) | Verfahren zur herstellung von granulen mit verminderter neigung zur bildung von staub und nach dem verfahren hergestellte granulen | |
| DD263790A1 (de) | Verfahren zur herstellung eines granulierten proteaseproduktes |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHJ | Non-payment of the annual fee |