DE2504964A1 - Verfahren zum galvanischen abscheiden von nickel - Google Patents
Verfahren zum galvanischen abscheiden von nickelInfo
- Publication number
- DE2504964A1 DE2504964A1 DE19752504964 DE2504964A DE2504964A1 DE 2504964 A1 DE2504964 A1 DE 2504964A1 DE 19752504964 DE19752504964 DE 19752504964 DE 2504964 A DE2504964 A DE 2504964A DE 2504964 A1 DE2504964 A1 DE 2504964A1
- Authority
- DE
- Germany
- Prior art keywords
- nickel
- cathode
- electrolyte
- roughness
- precipitate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 10
- 230000008021 deposition Effects 0.000 title description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 78
- 229910052759 nickel Inorganic materials 0.000 claims description 39
- 239000003792 electrolyte Substances 0.000 claims description 25
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 10
- 239000010936 titanium Substances 0.000 claims description 10
- 229910052719 titanium Inorganic materials 0.000 claims description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 8
- 230000003746 surface roughness Effects 0.000 claims description 7
- 239000010935 stainless steel Substances 0.000 claims description 6
- 229910001220 stainless steel Inorganic materials 0.000 claims description 6
- 229910052782 aluminium Inorganic materials 0.000 claims description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 5
- 238000005422 blasting Methods 0.000 claims description 5
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 claims description 4
- 229910001069 Ti alloy Inorganic materials 0.000 claims description 3
- 238000004070 electrodeposition Methods 0.000 claims description 3
- 239000002244 precipitate Substances 0.000 description 16
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 7
- 239000004576 sand Substances 0.000 description 7
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 6
- 239000004327 boric acid Substances 0.000 description 6
- 238000005868 electrolysis reaction Methods 0.000 description 6
- 239000000853 adhesive Substances 0.000 description 4
- 230000001070 adhesive effect Effects 0.000 description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 238000000151 deposition Methods 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 229910052749 magnesium Inorganic materials 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 description 3
- 235000011152 sodium sulphate Nutrition 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 239000003082 abrasive agent Substances 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229910001200 Ferrotitanium Inorganic materials 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229910000978 Pb alloy Inorganic materials 0.000 description 1
- 206010035148 Plague Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 239000000227 bioadhesive Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000011093 chipboard Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000002706 hydrostatic effect Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007788 roughening Methods 0.000 description 1
- 229910001925 ruthenium oxide Inorganic materials 0.000 description 1
- WOCIAKWEIIZHES-UHFFFAOYSA-N ruthenium(iv) oxide Chemical compound O=[Ru]=O WOCIAKWEIIZHES-UHFFFAOYSA-N 0.000 description 1
- 238000005488 sandblasting Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 150000004764 thiosulfuric acid derivatives Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C1/00—Electrolytic production, recovery or refining of metals by electrolysis of solutions
- C25C1/06—Electrolytic production, recovery or refining of metals by electrolysis of solutions or iron group metals, refractory metals or manganese
- C25C1/08—Electrolytic production, recovery or refining of metals by electrolysis of solutions or iron group metals, refractory metals or manganese of nickel or cobalt
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrolytic Production Of Metals (AREA)
- Electrodes For Compound Or Non-Metal Manufacture (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA192,114A CA1036536A (en) | 1974-02-08 | 1974-02-08 | Electrodeposition of thick nickel deposits on permanent cathode blanks |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2504964A1 true DE2504964A1 (de) | 1975-08-14 |
Family
ID=4099130
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752504964 Withdrawn DE2504964A1 (de) | 1974-02-08 | 1975-02-06 | Verfahren zum galvanischen abscheiden von nickel |
Country Status (11)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1866461A1 (en) | 2005-03-09 | 2007-12-19 | XSTRATA Queensland Limited | Stainless steel electrolytic plates |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS531603A (en) * | 1976-06-29 | 1978-01-09 | Asahi Glass Co Ltd | Pretreatment of cathode to be used at deposition of metal by electrolysis from solution containing metal salt |
| US4097347A (en) * | 1976-08-23 | 1978-06-27 | Packer Elliot L | Electrolytic recovery of metals |
| US4147597A (en) * | 1978-02-21 | 1979-04-03 | The International Nickel Company, Inc. | Method for producing electrolytic nickel in particulate forms under condition of high and variable internal stress |
| US5256709A (en) * | 1991-07-22 | 1993-10-26 | Owens-Corning Fiberglas Technology, Inc. | Unsaturated polyester resin compositions containing compatible compounds having aromatic substituents |
| US5256708A (en) * | 1991-07-22 | 1993-10-26 | Owens-Corning Fiberglas Technology, Inc. | Unsaturated polyester resin compositions containing compatible compounds having sulfur-containing substituents |
| WO2002002848A2 (en) * | 2000-06-30 | 2002-01-10 | Honeywell International Inc. | Method and apparatus for processing metals, and the metals so produced |
| FI20110210A7 (fi) * | 2011-06-23 | 2012-12-24 | Outotec Oyj | Kestokatodi ja menetelmä kestokatodin pinnan käsittelemiseksi |
| CN104073842A (zh) * | 2011-10-13 | 2014-10-01 | 金川集团有限公司 | 一种电积、电解镍的阴极板 |
| FR3014709B1 (fr) * | 2013-12-16 | 2016-01-29 | Airbus Operations Sas | Procede de traitement de deux surfaces de deux pieces metalliques |
| CN113638008A (zh) * | 2021-09-14 | 2021-11-12 | 广西银亿新材料有限公司 | 一种无钠化制备电解镍厚板的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2480771A (en) * | 1946-04-12 | 1949-08-30 | Int Nickel Co | Process for the electrolytic recovery of nickel |
| US2536877A (en) * | 1947-10-17 | 1951-01-02 | Anaconda Copper Mining Co | Cathode |
| US2597296A (en) * | 1948-10-01 | 1952-05-20 | Int Nickel Co | Forming starting sheets for electrolytic refining of nickel |
| US2646396A (en) * | 1949-03-17 | 1953-07-21 | Reginald S Dean | Method of making electroformed articles |
| JPS4846514A (enrdf_load_stackoverflow) * | 1971-10-18 | 1973-07-03 |
-
1974
- 1974-02-08 CA CA192,114A patent/CA1036536A/en not_active Expired
- 1974-04-11 US US459883A patent/US3883411A/en not_active Expired - Lifetime
-
1975
- 1975-01-16 JP JP50007394A patent/JPS50109819A/ja active Pending
- 1975-01-17 ZA ZA00750338A patent/ZA75338B/xx unknown
- 1975-01-21 FI FI750139A patent/FI72151C/fi not_active IP Right Cessation
- 1975-01-24 GB GB3123/75A patent/GB1489984A/en not_active Expired
- 1975-02-03 ZM ZM10/75A patent/ZM1075A1/xx unknown
- 1975-02-06 NO NO750387A patent/NO143388C/no unknown
- 1975-02-06 DE DE19752504964 patent/DE2504964A1/de not_active Withdrawn
- 1975-02-07 FR FR7503849A patent/FR2260634B1/fr not_active Expired
- 1975-02-07 SE SE7501366A patent/SE406941B/xx unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1866461A1 (en) | 2005-03-09 | 2007-12-19 | XSTRATA Queensland Limited | Stainless steel electrolytic plates |
Also Published As
| Publication number | Publication date |
|---|---|
| ZM1075A1 (en) | 1976-12-21 |
| NO143388C (no) | 1981-01-28 |
| SE7501366L (enrdf_load_stackoverflow) | 1975-08-11 |
| CA1036536A (en) | 1978-08-15 |
| AU7742375A (en) | 1976-07-22 |
| NO143388B (no) | 1980-10-20 |
| SE406941B (sv) | 1979-03-05 |
| FI750139A7 (enrdf_load_stackoverflow) | 1975-08-09 |
| US3883411A (en) | 1975-05-13 |
| FI72151C (fi) | 1987-04-13 |
| ZA75338B (en) | 1976-01-28 |
| JPS50109819A (enrdf_load_stackoverflow) | 1975-08-29 |
| NO750387L (enrdf_load_stackoverflow) | 1975-08-11 |
| GB1489984A (en) | 1977-10-26 |
| FR2260634B1 (enrdf_load_stackoverflow) | 1979-09-28 |
| FR2260634A1 (enrdf_load_stackoverflow) | 1975-09-05 |
| FI72151B (fi) | 1986-12-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| 8130 | Withdrawal |