DE2152463A1 - METHOD FOR PROCESSING PLASTIC POWDERS TO BE SINTERED - Google Patents

METHOD FOR PROCESSING PLASTIC POWDERS TO BE SINTERED

Info

Publication number
DE2152463A1
DE2152463A1 DE19712152463 DE2152463A DE2152463A1 DE 2152463 A1 DE2152463 A1 DE 2152463A1 DE 19712152463 DE19712152463 DE 19712152463 DE 2152463 A DE2152463 A DE 2152463A DE 2152463 A1 DE2152463 A1 DE 2152463A1
Authority
DE
Germany
Prior art keywords
sintered
plastic powders
processing plastic
sintering
ultrasonic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE19712152463
Other languages
German (de)
Other versions
DE2152463B2 (en
DE2152463C3 (en
Inventor
auf Nichtnennung. P Antrag
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cichos manfred dipl-Phys
Original Assignee
Cichos manfred dipl-Phys
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to BE788881D priority Critical patent/BE788881A/en
Application filed by Cichos manfred dipl-Phys filed Critical Cichos manfred dipl-Phys
Priority to DE19712152463 priority patent/DE2152463B2/en
Priority to IT2897072A priority patent/IT967278B/en
Priority to NL7212354A priority patent/NL7212354A/xx
Priority to DD16571872A priority patent/DD99950A5/xx
Priority to JP10512972A priority patent/JPS4851056A/ja
Priority to FR7237335A priority patent/FR2156893A1/en
Publication of DE2152463A1 publication Critical patent/DE2152463A1/en
Publication of DE2152463B2 publication Critical patent/DE2152463B2/en
Application granted granted Critical
Publication of DE2152463C3 publication Critical patent/DE2152463C3/de
Granted legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B13/00Conditioning or physical treatment of the material to be shaped
    • B29B13/007Treatment of sinter powders

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)

Description

Verfahren zur Verarbeitung/00 zu sinternden Kunststoffpulvern.Method of processing / 00 to sintered plastic powders.

Die Erfindung betrifft ein Verfahren, Kunststoffe, die nur durch einen Sinterprozeß verarbeitet werden können, dadurch schneller, besser und gleichmäßiger zu sintern, daß die zum Sintern erforderliche Wärme im Innern des Sinterkörpers selbst teilweise oder ganz durch eingeleitete Ultraschall-Energie erzeugt wird. .;The invention relates to a method that plastics only by a sintering process can be processed, thereby faster, better and more uniform sintering that the heat required for sintering in the interior of the sintered body itself partially or generated entirely by introduced ultrasonic energy. .;

Verschiedene technisch wichtige Kunststoffe (z.B. Polytetr&flupräthylen) lassen sich nur über Sinterverfahren auf zwei verschiedene Arten verarbeiten. Einmal wird der in Pulverform vorliegende Kunststoff kalt unter Druck in entsprechenden Matrizen verdichtet und anschließend mit oder ohne Matrize in einem Ofen nach einem bestimmten Temperaturplan erhitzt bis der gesamte Kunststoffkörper homogen durchgesintert und verfestigt ist.Various technically important plastics (e.g. polytetrafluoroethylene & flupraethylene) can only be processed in two different ways using sintering processes. One is the powdered one Plastic is compacted cold under pressure in appropriate dies and then with or without a die in an oven after a heated to a specific temperature plan until the entire plastic body is homogeneously sintered and solidified.

Zum anderen lassen sich zylindrische Körper - Stäbe, Rohre usw. -durch kontinuierliche Extrusion herstellen. Hierbei wird das Kunststoffpulver durch einen auf- und abfahrenden Preßstempel in das senkrecht stehende Extruderrohr gepreßt, das auf einer Länge von einigen Metern mit Heizmanschetten umgeben ist. Auf dem Weg durch das Extruderrohr wird der Kunststoff aufgeheizt und gesintert. Wegen der geringen Wärmeleitfähigkeit der o.g. Kunststoffe sind beide Sinterverfahren sehr langwierig. Das Sintern im Ofen dauert je nach Größe des Werkstückes mehrere Stunden. Beim Extrudieren erzielt man je nach Durchmesser des Stabes oder Rohres 0,25-1 m/h Vorschub. Durch das erfindungsgemäße Verfahren wird die Verarbeitungszeit dieser Kunststoffe dadurch verkürzt, daß die Erhitzung durch Ultraschall von innen heraus erfolgt.On the other hand, cylindrical bodies - rods, pipes, etc. - can be produced by continuous extrusion. Here is the Plastic powder is pressed into the vertical extruder tube by a ram moving up and down, which over a length is surrounded by a few meters with heating jackets. On the way through the extruder pipe, the plastic is heated and sintered. Because of the low thermal conductivity of the above plastics both sintering processes are very tedious. Sintering in the furnace takes several hours, depending on the size of the workpiece. When extruding, you achieve depending on the diameter of the rod or tube 0.25-1 m / h feed. The process according to the invention shortens the processing time of these plastics in that the heating is carried out by ultrasound from the inside out.

Die thermischen Wirkungen von Ultraschallschwingungen werden seit langem beim Ultraschall-Kunststoff-Schweißen angewendet, jedoch findet die Umsetzung von akustischer in thermische Energie hierbei stets nur an der Grenzfläche der beiden zu verschweißenden Körper statt und diese sollen mit einander verschmolzen werden. Zudem sind für das Kunststoffschweißen mit Ultraschall nur bestimmte leicht schmelzende Kunststoffe geeignet. Bei dem erfindungsgemäßen Verfahren findet dagegen eineThe thermal effects of ultrasonic vibrations are It has been used for a long time in ultrasonic plastic welding, but the conversion of acoustic into thermal energy always takes place only at the interface between the two bodies to be welded and these should be fused together. In addition, for plastic welding with Ultrasound only suitable for certain easily melting plastics. In the method according to the invention, on the other hand, there is one

- 2 303819/0370- 2 303819/0370

Volumenerhitzung statt, die zu sinternden Kunststoffe schmelzen ferner nicht, sonst könnte man sie wie Thermoplaste auf Spritzgießmaschinen schnell verarbeiten.Volume heating instead of melting the plastics to be sintered furthermore not, otherwise they could be processed quickly like thermoplastics on injection molding machines.

Das neue Verfahren findet hauptsächlich zur Durchsatzsteigerung beim Extrudieren der zu sinternden Kunststoffe Anwendung. Hierbei wird das Kunststoffpulver durch ein im Verhältnis zur gesamten. Extruderlänge relativ kurzes Rohr gepreßt, das durch außen angebrachte Schwingerelemente zu radialen Schwingungen angeregt wird. Das Rohr kann am Eintritten der Mitte oder am Ende des Extruderrohres angebracht sein, es hat den gleichen Innendurchmesser wie das übrige Extruderrohr. Der unter Druck stehende Pulverstrang passiert beispielsweise zuerst das Schwingrohr, wird dort in kurzer Zeit von innen her aufgeheizt und sintert von der Rohrachse ausgehend bis zu einer gewissen Randzone hin. Der restliche Querschnitt wird anschließend leicht in der üblichen Art von außen durch konventionelle Beheizung zu Ende gesintert. Die Durchsatzsteigerung durch die rasche Ultraschallaufheizung kann das Doppelte bis Dreifache der gewöhnlichen Produktion betragen. Bei Sinterung in der Matrize kann die Ultraschallenergie in ähnlicher Weise durch geeignet geformte Ultraschall schwinger, die den Matrizenmantel im wesentlichen senkrecht zu seiner Oberfläche erregen, in den zu sinternden Körper eingeleitet werden.The new process is mainly used to increase throughput when extruding the plastics to be sintered. Here, the plastic powder is replaced by one in relation to the total. Extruder length, a relatively short pipe is pressed, which is excited to radial vibrations by vibrating elements attached to the outside. The tube can be attached at the inlet in the middle or at the end of the extruder tube; it has the same inner diameter as the rest of the extruder tube. The pressurized powder strand, for example, first passes the oscillating tube, where it is heated from the inside in a short time and, starting from the tube axis, sinters up to a certain edge zone. The remaining cross-section is then easily sintered to the end in the usual way from the outside by conventional heating. The increase in throughput due to the rapid ultrasonic heating can be twice to three times the normal production. When sintering in the die, the ultrasonic energy can be introduced into the body to be sintered in a similar manner by suitably shaped ultrasonic vibrators which excite the die jacket essentially perpendicular to its surface.

3Q9819/Q37Q3Q9819 / Q37Q

Claims (3)

21524832152483 PATENTANSPROCHEPATENT CLAIM Verfahren zur Verarbeitung von zu sinternden Kunststoffpulvern dadurch gekennzeichnet, daß die zum Sintern erforderliche Wärme im Innern des Sinterkörpers teilweise oder ganz durch eingeleitete Ultraschallenergie erzeugt wird.Method for processing plastic powders to be sintered, characterized in that the heat required for sintering is generated in the interior of the sintered body partially or entirely by introduced ultrasonic energy. 2. Verfahren nach Anspruch 1 dadurch gekennzeichnet, daß die Ultraschallenergie durch ein radial schwingendes Rohr in den Sinterkörper eingeleitet wird.2. The method according to claim 1, characterized in that the ultrasonic energy through a radially vibrating tube in the Sintered body is initiated. 3. Verfahren nach Anspruch 1 dadurch gekennzeichnet, daß die Schallenergie über den Mantel der Matrize, der im wesentlichen senkrecht zu seiner Oberfläche zu Ultraschallschwlngungen erregt wird, in den Sinterkörper eingeleitet wird.3. The method according to claim 1, characterized in that the sound energy over the jacket of the die, which is substantially perpendicular to its surface to ultrasonic vibrations is excited, is introduced into the sintered body. 309819/Ö370309819 / Ö370
DE19712152463 1971-10-21 1971-10-21 Device for continuous extrusion sintering Granted DE2152463B2 (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
BE788881D BE788881A (en) 1971-10-21 SINTERING PROCESS OF POWDERED PLASTICS
DE19712152463 DE2152463B2 (en) 1971-10-21 1971-10-21 Device for continuous extrusion sintering
IT2897072A IT967278B (en) 1971-10-21 1972-09-08 PROCEDURE FOR PROCESSING PLASTIC MATERIAL POWDERS TO BE SINTERED
NL7212354A NL7212354A (en) 1971-10-21 1972-09-12
DD16571872A DD99950A5 (en) 1971-10-21 1972-09-18
JP10512972A JPS4851056A (en) 1971-10-21 1972-10-20
FR7237335A FR2156893A1 (en) 1971-10-21 1972-10-20 Plastic moulding - by heating plastic chips using ultrasonic vibrations

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19712152463 DE2152463B2 (en) 1971-10-21 1971-10-21 Device for continuous extrusion sintering

Publications (3)

Publication Number Publication Date
DE2152463A1 true DE2152463A1 (en) 1973-05-10
DE2152463B2 DE2152463B2 (en) 1975-01-02
DE2152463C3 DE2152463C3 (en) 1975-08-21

Family

ID=5823007

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19712152463 Granted DE2152463B2 (en) 1971-10-21 1971-10-21 Device for continuous extrusion sintering

Country Status (7)

Country Link
JP (1) JPS4851056A (en)
BE (1) BE788881A (en)
DD (1) DD99950A5 (en)
DE (1) DE2152463B2 (en)
FR (1) FR2156893A1 (en)
IT (1) IT967278B (en)
NL (1) NL7212354A (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61181630A (en) * 1985-02-07 1986-08-14 Beishin Kogyo Kk Method of molding powdery particle
US4793954A (en) * 1987-08-17 1988-12-27 The B. F. Goodrich Company Shear processing thermoplastics in the presence of ultrasonic vibration
FR2657291B1 (en) * 1990-01-23 1992-05-15 Dias Ind Sarl PROCESS FOR THE MANUFACTURE OF A COMPOSITE MATERIAL COMPRISING THE MIXTURE OF AT LEAST TWO COMPONENTS AND COMPOSITE MATERIAL OBTAINED.

Also Published As

Publication number Publication date
FR2156893A1 (en) 1973-06-01
NL7212354A (en) 1973-04-25
JPS4851056A (en) 1973-07-18
IT967278B (en) 1974-02-28
DD99950A5 (en) 1973-09-05
DE2152463B2 (en) 1975-01-02
DE2152463C3 (en) 1975-08-21
BE788881A (en) 1973-01-02

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Legal Events

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C3 Grant after two publication steps (3rd publication)