DE19812684A1 - Extraction of residual fluids from beer mash and fermentation stages, increases volume of beer produced from same quantity of ingredients - Google Patents
Extraction of residual fluids from beer mash and fermentation stages, increases volume of beer produced from same quantity of ingredientsInfo
- Publication number
- DE19812684A1 DE19812684A1 DE1998112684 DE19812684A DE19812684A1 DE 19812684 A1 DE19812684 A1 DE 19812684A1 DE 1998112684 DE1998112684 DE 1998112684 DE 19812684 A DE19812684 A DE 19812684A DE 19812684 A1 DE19812684 A1 DE 19812684A1
- Authority
- DE
- Germany
- Prior art keywords
- filter
- chamber
- beer
- mash
- fermentation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000855 fermentation Methods 0.000 title claims abstract description 21
- 230000004151 fermentation Effects 0.000 title claims abstract description 21
- 235000013405 beer Nutrition 0.000 title claims abstract description 19
- 239000004615 ingredient Substances 0.000 title abstract 2
- 238000000605 extraction Methods 0.000 title 1
- 239000012530 fluid Substances 0.000 title 1
- 238000000034 method Methods 0.000 claims abstract description 18
- 238000001914 filtration Methods 0.000 claims abstract description 5
- 239000000706 filtrate Substances 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 239000002351 wastewater Substances 0.000 claims description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 claims description 3
- 239000003463 adsorbent Substances 0.000 claims description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 2
- 239000001569 carbon dioxide Substances 0.000 claims description 2
- 239000011347 resin Substances 0.000 claims description 2
- 229920005989 resin Polymers 0.000 claims description 2
- 239000000377 silicon dioxide Substances 0.000 claims description 2
- 238000010025 steaming Methods 0.000 claims 1
- 238000013124 brewing process Methods 0.000 abstract 1
- 238000005352 clarification Methods 0.000 description 4
- 239000012528 membrane Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 239000012065 filter cake Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000003750 conditioning effect Effects 0.000 description 2
- 235000012054 meals Nutrition 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 210000005253 yeast cell Anatomy 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000036512 infertility Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000009928 pasteurization Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 238000009923 sugaring Methods 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C11/00—Fermentation processes for beer
- C12C11/003—Fermentation of beerwort
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/14—Lautering, i.e. clarifying wort
- C12C7/16—Lautering, i.e. clarifying wort by straining
- C12C7/163—Lautering, i.e. clarifying wort by straining with transport of the mash by or relative to a filtering surface
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
- C12H1/06—Precipitation by physical means, e.g. by irradiation, vibrations
- C12H1/063—Separation by filtration
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Biochemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Toxicology (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
Description
Die Erfindung betrifft ein Verfahren für die Herstellung von Bier. Das Hauptziel dieser Erfindung ist ein Verfahren vorzuschlagen, das die gegenwärtigen Produktverluste und die dadurch verursachten Abwasserprobleme bzw. -kosten erheblich vermindert.The invention relates to a method for the production of beer. The main goal of this Invention is a method to propose that the current product losses and the the resulting wastewater problems and costs are significantly reduced.
Eine Schätzung der weltweiten Produktverluste in Bierbrauereien bezogen auf Vor- und Endprodukte liegen bei 20-30%. Die Hauptverlustquellen treten bei der Maischbereitung, -filtration und den anschliessenden Bierklärungsvorgängen nach der Gärung auf. Aufgrund unvollständiger Zersetzung der Stärke und Polysen zu gärbaren Zucker bei der Maischbereitung, werden Produktverluste von bis zu 20% verursacht. Wegen unvollständiger Auswaschung des Restzuckers in dem grobkörnigen Filterbett der Läuterpfanne gehen bis zu 10% des verfügbaren Gärzuckers verloren. Bei den nach der Gärung anschliessenden Bierklärungsvorgängen ist je nach dem eingesetzten Brau-, bzw. Klärverfahren, z. B. wenn Ober- oder Untergärung oder wenn Konditionierungsmittel verwendet wird, mit Bierverlusten von bis zu 10% zu rechnen. Für jeden Liter des produzierten Biers werden 5-10 Liter von biologisch belastetem Abwasser erzeugt.An estimate of worldwide product losses in beer breweries based on pre and End products are 20-30%. The main sources of loss occur in the preparation of mash, -filtration and the subsequent beer clarification processes after fermentation. Due to incomplete decomposition of the starch and polyses to fermentable sugar of the mash preparation, product losses of up to 20% are caused. Because of incomplete washing out of the residual sugar in the coarse-grained filter bed of the The lauter tun is lost up to 10% of the available fermentation sugar. In the after the The subsequent beer clarification process depends on the brewing or Clarification processes, e.g. B. if top or bottom fermentation or if conditioning agents is used to anticipate beer losses of up to 10%. For every liter of Beer produced is 5-10 liters of biologically contaminated wastewater.
Fig. 1 zeigt das Fliessschema eines konventionellen Verfahrens einer Bierbrauerei. Die kostenverursachenden Stufen der Klärvorgänge 103, 105, 107, 109, 110, 112, 113, 114, 116, 117 werden durch die in Fig. 2 veranschaulichten Stufen 202, 204 des Verfahrens der Erfindung ersetzt. Die letztgenannten Einrichtungen stimmen mit einer Weiterentwicklung der in DE 44 37 175 beschriebenen Bandfilteranlage überein. Dies sind Bandfilter mit einer Filterkammer durch die ein Filterband über eine Stützfläche absatzweise transportierbar ist und durch die Stützfläche in eine untere Filtratkammer und eine obere Trübekammer unterteilt ist, wobei die Trübekammer deckelartig ausgebildet ist und das Filterband während des Betriebs wenn ein Druckabfall in der Filterkammer entsteht dichtend zwischen den Kanten des Filterdeckels und der Filtratkammer geführt wird. Der Vorteil der Weiterentwicklung dieses Druckfilters liegt in der Fähigkeit feinverteilte Fest stoff-Suspensionen unter Ausschluss von Luft vollautomatisch zu filtrieren, wobei austragbare Feststoffe und steriles Filtrat erzeugt werden. Durch den Einsatz von Membran filterelementen mit Porengrößen von 0.01-1.0 Mikron wird Malz- bzw. Getreideschrot für die Maischbereitung mit mittleren Korngrößen von 20-100 Mikron gemahlen. Solche Werte führen zu einer erheblich verbesserten Zuckerausbeute der Maische bei der Würzeherstellung und Auswaschung des resultierenden Filterkuchens. Erfindungsgemäß, wird der feinverteilte in Wasser suspendierte Maischschrot in einem reaktorartigen Bottich 201, nach stufenweiser Erhitzung mittels des Heizmantels 213, mittels der Vakuum erzeugungseinrichtung 216 unter Vakuum gesetzt und gleich danach mit Dampf durch einen Verteiler 217 geblasen, wobei der unerwünschte, flüchtige Anteil der Maische durch eine verhältnismäßig niedrige Temperatur entfernt wird. Sodann, um weitere unerwünschten eiweissähnlichen Stoffe abzuscheiden, wird mittels des Heissmantels 213 die Maische abgekühlt und dann durch die o.g. Filteranlage 202 filtriert. Erfindungsgemäß werden sowohl die durch Wärme als die durch Kälte abgeschiedenen Stoffe ohne Flockenbildung mit Hilfe des übriggebliebenen, feinverteilten Hülsenrests des feingemahlenen Malz mittels der Membranelemente abfiltriert. Der Filterkuchen wird dann nach Entzuckerung trocken-ausgetragen. Die geklärte, abgekühlte Würze wird dann dem reaktorähnlichen Gärkessel 203 zugeführt, wobei, um die noch in der Losung vorhandenen aber auch während der Gärung erzeugten eiweissähnlichen Substanzen schon vor aber auch während der Gärung zu entfernen, wird geeignetes Adsorbiermittel wie Kieselsäure, Harz, etc. zudosiert. Zweck dieses erfindungsgemäßen Vorgangs ist es die gärende Würze frei von Trübungen und nachtrübungs-verursachenden Substanzen zu halten um in dieser Weise ein stabilisiertes Bier schon bei der Gärung zu erzielen. Erfindungsgemäß, um die Gärung und daher den Stoffwechsel der Hefezellen besser zu steuern, werden programmierte Verhältnisse während der Gärung zwischen der Temperatur-, Druck- und Kohlendioxidentwicklung des Gärungsvorgangs mittels Regler 223, 220, 218 eingehalten. Während der Gärung und der nachfolgenden Filtration wird die Gärmasse durch das Rührwerk 222 schonend in Suspension gehalten. Dies dient der Sterilität der Betriebseinrichtungen, der Qualität und Ausbeute des Biers, einem reibungslosen Ablauf der Gärung sowie einer erheblichen Reduzierung des Reinigungsaufwands des Gärtanks 203 und der Filteranlage 204 und daher des Abwasserproblems. Erfindungsgemäß, um die in der Gärmasse vorhandenen Hefezellen zu schonen, wird dann die Gärmasse mittels Druckgas durch das in der Filterkammer abgedichtete Membranfilterelement gedruckt. Das in dieser Weise sterilfiltrierte und stabilisierte Bier wird sodann direkt verpackt 207. Fig. 1 shows the flow diagram of a conventional method of a brewery. The cost-causing stages of the clarification processes 103 , 105 , 107 , 109 , 110 , 112 , 113 , 114 , 116 , 117 are replaced by the stages 202 , 204 of the method of the invention illustrated in FIG. 2. The latter devices correspond to a further development of the belt filter system described in DE 44 37 175. These are belt filters with a filter chamber through which a filter belt can be transported in batches over a support surface and is divided into a lower filtrate chamber and an upper turbidity chamber by the support surface, the turbidity chamber being designed like a lid and the filter belt during operation if a pressure drop occurs in the filter chamber is sealingly guided between the edges of the filter cover and the filtrate chamber. The advantage of the further development of this pressure filter is the ability to filter finely divided solid suspensions in the absence of air in a fully automated manner, whereby removable solids and sterile filtrate are generated. The use of membrane filter elements with pore sizes of 0.01-1.0 microns grinds malt or grain meal for mash preparation with average grain sizes of 20-100 microns. Such values lead to a considerably improved sugar yield of the mash during the wort production and washing out of the resulting filter cake. According to the invention, the finely divided mashed meal suspended in water is placed in a reactor-like tub 201 , after gradual heating by means of the heating jacket 213 , placed under vacuum by means of the vacuum generating device 216 and then immediately blown with steam through a distributor 217 , the undesired, volatile portion of the mash is removed by a relatively low temperature. Then, in order to separate out further undesirable protein-like substances, the mash is cooled by means of the hot jacket 213 and then filtered through the above-mentioned filter system 202 . According to the invention, both the materials separated by heat and those by cold are filtered off without flaking with the aid of the remaining, finely divided sleeve residue of the finely ground malt by means of the membrane elements. The filter cake is then carried out dry after desugarization. The clarified, cooled wort is then fed to the reactor-like fermentation tank 203 , whereby, in order to remove the protein-like substances still present in the solution but also produced during the fermentation before but also during the fermentation, suitable adsorbent such as silica, resin, etc. is used. added. The purpose of this process according to the invention is to keep the fermenting wort free from turbidity and substances which cause turbidity in order to achieve a stabilized beer during fermentation. According to the invention, in order to better control the fermentation and therefore the metabolism of the yeast cells, programmed relationships are maintained during the fermentation between the temperature, pressure and carbon dioxide development of the fermentation process by means of regulators 223 , 220 , 218 . During fermentation and the subsequent filtration, the digestate is gently held in suspension by the agitator 222 . This serves to ensure the sterility of the operating facilities, the quality and yield of the beer, a smooth fermentation process and a considerable reduction in the cleaning effort of the fermentation tank 203 and the filter system 204 and therefore the wastewater problem. According to the invention, in order to protect the yeast cells present in the digestate, the digestate is then printed by means of compressed gas through the membrane filter element sealed in the filter chamber. The beer sterilized and stabilized in this way is then packaged directly 207 .
Der dabei entstandene entwässerte Hefefilterkuchen wird dann ausgetragen 215. Erfindungsgemäß wird die Hauptmenge des stark-reduzierten anfallenden Abwassers bei dem vorhin beschriebenen Verfahren der Erfindung entsteht bei der Reinigung und Sterilisierung der Filteranlagen 202, 204. Erfindungsgemäß, um das Abwasser aufzubereiten und für Reinigungs- und Sterilisierungszwecke wiederzu-verwenden, wird eine weitere Membranfilteranlage 211 eingesetzt. Erfindungsgemäß wird das gesamte alkohol- und würzehaltige Behälterspülwasser von 201, 203 sowie Entzuckerungswasser von 202, 204 als Speisewasser für die Maischbereitung verwendet. Es entsteht auf dieser Weise hinsichtlich Abwasser eine geschlossene Brauerei. The resulting dewatered yeast filter cake is then discharged 215 . According to the invention, the majority of the greatly reduced wastewater produced in the method of the invention described above is produced during the cleaning and sterilization of the filter systems 202 , 204 . According to the invention, in order to treat the waste water and reuse it for cleaning and sterilization purposes, a further membrane filter system 211 is used. According to the invention, the entire alcohol and wort-containing container rinse water from 201 , 203 and de-sugaring water from 202 , 204 is used as feed water for the preparation of the mash. This creates a closed brewery with regard to waste water.
101101
Maischtun
Doing mash
102102
Maischkessel
Mash kettle
103103
Läutertun
Purification
104104
Würzekessel
Wort kettle
105105
Hopfenfilter
Hop filter
106106
Würzebottich
Wort tub
107107
Zentrifuge
centrifuge
108108
Würzekühler
Wort cooler
109109
Braukessel
Brewing kettle
110110
Zentrifuge
centrifuge
111111
Kühler
cooler
112112
Konditionierungskessel
Conditioning kettle
113113
Zentrifuge
centrifuge
114114
Bierfilter
Beer filter
115115
Pasteurisierung
pasteurization
116116
Hefefilter
Yeast filter
117117
Bodensatzfilter
Sediment filter
201201
Maischkessel
Mash kettle
202202
Maischfilter
Mash filter
203203
Braukessel
Brewing kettle
204204
Bierfilter
Beer filter
207207
Abfüllanlage
Bottling line
211211
Abwasseraufbereitung
Wastewater treatment
213213
Wärmeübertragungsmantel
Heat transfer jacket
215215
Hefeaustragung
Yeast delivery
216216
Vakuumanlage
Vacuum system
217217
Dampfzufuhr
Steam supply
218218
CO2 CO 2
-Durchflußregler
-Flow regulator
219219
Heiz-/Kühlmittelzufuhr
Heating / coolant supply
220220
Druckregler
Pressure regulator
222222
Gärkesselrührwerk
Proofing tank agitator
223223
Temperaturregler
Temperature controller
Claims (7)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE1998112684 DE19812684A1 (en) | 1998-03-23 | 1998-03-23 | Extraction of residual fluids from beer mash and fermentation stages, increases volume of beer produced from same quantity of ingredients |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE1998112684 DE19812684A1 (en) | 1998-03-23 | 1998-03-23 | Extraction of residual fluids from beer mash and fermentation stages, increases volume of beer produced from same quantity of ingredients |
Publications (1)
Publication Number | Publication Date |
---|---|
DE19812684A1 true DE19812684A1 (en) | 1999-09-30 |
Family
ID=7861969
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE1998112684 Withdrawn DE19812684A1 (en) | 1998-03-23 | 1998-03-23 | Extraction of residual fluids from beer mash and fermentation stages, increases volume of beer produced from same quantity of ingredients |
Country Status (1)
Country | Link |
---|---|
DE (1) | DE19812684A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE112008004043T5 (en) | 2007-09-10 | 2013-03-21 | Peter Anthony Miller | Methods and systems of total capture and recovery of used organic and inorganic matter from self-sustaining human settlements |
-
1998
- 1998-03-23 DE DE1998112684 patent/DE19812684A1/en not_active Withdrawn
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE112008004043T5 (en) | 2007-09-10 | 2013-03-21 | Peter Anthony Miller | Methods and systems of total capture and recovery of used organic and inorganic matter from self-sustaining human settlements |
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Legal Events
Date | Code | Title | Description |
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8120 | Willingness to grant licenses paragraph 23 | ||
8130 | Withdrawal |