DE1062679B - Device for carrying out chemical reactions with finely divided sodium amalgam - Google Patents

Device for carrying out chemical reactions with finely divided sodium amalgam

Info

Publication number
DE1062679B
DE1062679B DEH31922A DEH0031922A DE1062679B DE 1062679 B DE1062679 B DE 1062679B DE H31922 A DEH31922 A DE H31922A DE H0031922 A DEH0031922 A DE H0031922A DE 1062679 B DE1062679 B DE 1062679B
Authority
DE
Germany
Prior art keywords
sodium amalgam
chemical reactions
carrying
finely divided
out chemical
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DEH31922A
Other languages
German (de)
Inventor
Dipl-Chem Dr Georg Scheurich
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GEORG SCHEURICH DIPL CHEM DR
Original Assignee
GEORG SCHEURICH DIPL CHEM DR
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by GEORG SCHEURICH DIPL CHEM DR filed Critical GEORG SCHEURICH DIPL CHEM DR
Priority to DEH31922A priority Critical patent/DE1062679B/en
Publication of DE1062679B publication Critical patent/DE1062679B/en
Pending legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series

Description

Vorrichtung zur Durchführung chemischer Reaktionen mit feinverteiltem Natriumamalgam Es ist bekannt, daß die Geschwindigkeit chemischer Reaktionen, an denen feste Stoffe beteiligt sind, durch Vergrößerung deren Oberfläche stark beschleunigt werden kann. Gegenstand vorliegender Erfindung ist eine Apparatur, mit der eine solche Oberflächenvergrößerung bei Natriumamalgam in sehr wirksamer Weise dadurch gelingt, daß dieses in besonders feine Tröpfchen übergeführt wird. Device for carrying out chemical reactions with finely divided Sodium amalgam It is known that the speed of chemical reactions, at where solid substances are involved, greatly accelerated by enlarging their surface can be. The present invention is an apparatus with which a such surface enlargement in sodium amalgam in a very effective manner thereby succeeds in converting this into particularly fine droplets.

Erfindungsgemäß besteht die Apparatur aus einem aufrecht stehenden zylindrischen Gefäß oder Fallrohr 1, das in gewissen Abständen voneinander mehrere Siebböden 2 zweckmäßig in Form engmaschiger Netze enthält. An einer zentral in dem Gefäß 1 angebrachten und in Rotation versetzbaren Weile 3 sind über jedem Siebboden Bürsten 4 angebracht. Diese Bürsten verteilen das Natriumamalgam zu äußerst feinen Tröpfchen, von denen bei ihrem Passieren jedes einzelnen Siebs immer wieder neue reaktionsfähige Tröpfchenoberflächen geschaffen werden. Die Zuführung des Natriumamalgams erfolgt aus einem Vorratsgefäß 5 durch eine Düse 6. According to the invention, the apparatus consists of an upright one cylindrical vessel or downpipe 1, which at certain distances from each other several Contains sieve trays 2 appropriately in the form of close-meshed networks. At one central point in that Vessel 1 attached and rotatable shaft 3 are above each sieve tray Brushes 4 attached. These brushes spread the sodium amalgam extremely fine Droplets, of which new ones keep coming through every single sieve reactive droplet surfaces are created. The feeding of the sodium amalgam takes place from a storage vessel 5 through a nozzle 6.

Das gleichzeitig als Reaktionsgefäß dienende Fallrohr 1 ist an seinem Boden mit Einlaßrohren 7 und 8 für mit dem Natriumamalgam in Reaktion zu bringende Gase und Flüssigkeiten versehen. Das Gaszug leitungsrohr 7 mündet in dem Gefäß 1 zweckmäßig in einen Gasverteiler 9. Am oberen Ende des Fallrohrs 1 befinden sich ein Gas ableitungs rohr 10 und ein Flüssigkeitsableitungsrohr 11. Zum Abführen des während einer Reaktion gebildeten Quecksilbers kann ein Dberlaufrohr 12 dienen. The downpipe 1, which also serves as a reaction vessel, is on his Bottom with inlet pipes 7 and 8 for to be reacted with the sodium amalgam Provide gases and liquids. The gas train pipe 7 opens into the vessel 1 expediently in a gas distributor 9. At the upper end of the downpipe 1 are located a gas discharge pipe 10 and a liquid discharge pipe 11. To discharge the An overflow tube 12 can serve as mercury formed during a reaction.

Claims (1)

PATENTANSPRUCH: Vorrichtung zur Durchführung chemischer Reaktionen mit feinverteiltem Natriumamalgam, bestehend aus einem mit Anschlüssen für Zu- und Ableitung von Gasen und Flüssigkeiten versehenen Fall rohr (1), in dem über mehreren in Abständen voneinander angebrachten Sieben (2) Bürsten (4) angeordnet sind, die in an sich bekannter Weise an einer senkrechten, zentralen, rotierbaren Welle (3) angebracht sind. PATENT CLAIM: Device for carrying out chemical reactions with finely divided sodium amalgam, consisting of one with connections for inlet and outlet Discharge of gases and liquids provided case pipe (1) in which several spaced apart sieves (2) brushes (4) are arranged, which in a manner known per se on a vertical, central, rotatable shaft (3) are appropriate. In Betracht gezogene Druckschriften: USA.-Patentschrift Nr. 2 539 699. References considered: U.S. Patent No. 2,539 699. In Betracht gezogene ältere Patente: Deutsches Patent Nr. 958 736. Older patents considered: German Patent No. 958 736.
DEH31922A 1954-10-11 1954-10-11 Device for carrying out chemical reactions with finely divided sodium amalgam Pending DE1062679B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEH31922A DE1062679B (en) 1954-10-11 1954-10-11 Device for carrying out chemical reactions with finely divided sodium amalgam

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEH31922A DE1062679B (en) 1954-10-11 1954-10-11 Device for carrying out chemical reactions with finely divided sodium amalgam

Publications (1)

Publication Number Publication Date
DE1062679B true DE1062679B (en) 1959-08-06

Family

ID=7151751

Family Applications (1)

Application Number Title Priority Date Filing Date
DEH31922A Pending DE1062679B (en) 1954-10-11 1954-10-11 Device for carrying out chemical reactions with finely divided sodium amalgam

Country Status (1)

Country Link
DE (1) DE1062679B (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2539699A (en) * 1944-06-13 1951-01-30 Eastman Kodak Co Distillation process and apparatus
DE958736C (en) * 1951-10-31 1957-02-21 Chemie Linz Ag Process for the production of metal salts and other metal compounds by reacting the liquid amalgam of the metal

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2539699A (en) * 1944-06-13 1951-01-30 Eastman Kodak Co Distillation process and apparatus
DE958736C (en) * 1951-10-31 1957-02-21 Chemie Linz Ag Process for the production of metal salts and other metal compounds by reacting the liquid amalgam of the metal

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