DE102013210679A1 - Verfahren zur Herstellung mehrwandiger Kohlenstoffnanoröhrchen, mehrwandiges Kohlenstoffnanoröhrchen und Kohlenstoffnanoröhrchenpulver - Google Patents

Verfahren zur Herstellung mehrwandiger Kohlenstoffnanoröhrchen, mehrwandiges Kohlenstoffnanoröhrchen und Kohlenstoffnanoröhrchenpulver Download PDF

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DE102013210679A1
DE102013210679A1 DE102013210679.3A DE102013210679A DE102013210679A1 DE 102013210679 A1 DE102013210679 A1 DE 102013210679A1 DE 102013210679 A DE102013210679 A DE 102013210679A DE 102013210679 A1 DE102013210679 A1 DE 102013210679A1
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carbon
carbon nanotubes
carbon nanotube
substrate
reactor
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German (de)
English (en)
Inventor
Heiko Hocke
Oliver Schlüter
Volker Michele
Leslaw Mleczko
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Covestro Deutschland AG
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Bayer MaterialScience AG
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Priority to DE102013210679.3A priority Critical patent/DE102013210679A1/de
Priority to US14/894,140 priority patent/US20160101979A1/en
Priority to EP14728201.6A priority patent/EP3003972A1/de
Priority to CN201480032433.3A priority patent/CN105246825A/zh
Priority to KR1020157034345A priority patent/KR20160015236A/ko
Priority to JP2016517604A priority patent/JP2016520510A/ja
Priority to PCT/EP2014/061722 priority patent/WO2014195415A1/de
Publication of DE102013210679A1 publication Critical patent/DE102013210679A1/de
Withdrawn legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/442—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating using fluidised bed process
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/168—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/26—Deposition of carbon only
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/06—Multi-walled nanotubes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/34—Length
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/36—Diameter
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Metallurgy (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
DE102013210679.3A 2013-06-07 2013-06-07 Verfahren zur Herstellung mehrwandiger Kohlenstoffnanoröhrchen, mehrwandiges Kohlenstoffnanoröhrchen und Kohlenstoffnanoröhrchenpulver Withdrawn DE102013210679A1 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
DE102013210679.3A DE102013210679A1 (de) 2013-06-07 2013-06-07 Verfahren zur Herstellung mehrwandiger Kohlenstoffnanoröhrchen, mehrwandiges Kohlenstoffnanoröhrchen und Kohlenstoffnanoröhrchenpulver
US14/894,140 US20160101979A1 (en) 2013-06-07 2014-06-05 Method for producing multi-walled carbon nanotubes, multi-walled carbon nanotubes and carbon nanotube powder
EP14728201.6A EP3003972A1 (de) 2013-06-07 2014-06-05 Verfahren zur herstellung mehrwandiger kohlenstoffnanoröhrchen, mehrwandiges kohlenstoffnanoröhrchen und kohlenstoffnanoröhrchenpulver
CN201480032433.3A CN105246825A (zh) 2013-06-07 2014-06-05 制造多壁碳纳米管的方法、多壁碳纳米管和碳纳米管粉末
KR1020157034345A KR20160015236A (ko) 2013-06-07 2014-06-05 다중-벽 탄소 나노튜브의 제조 방법, 다중-벽 탄소 나노튜브 및 탄소 나노튜브 분말
JP2016517604A JP2016520510A (ja) 2013-06-07 2014-06-05 多層カーボンナノチューブの製造方法、多層カーボンナノチューブおよびカーボンナノチューブ粉末
PCT/EP2014/061722 WO2014195415A1 (de) 2013-06-07 2014-06-05 Verfahren zur herstellung mehrwandiger kohlenstoffnanoröhrchen, mehrwandiges kohlenstoffnanoröhrchen und kohlenstoffnanoröhrchenpulver

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102013210679.3A DE102013210679A1 (de) 2013-06-07 2013-06-07 Verfahren zur Herstellung mehrwandiger Kohlenstoffnanoröhrchen, mehrwandiges Kohlenstoffnanoröhrchen und Kohlenstoffnanoröhrchenpulver

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US (1) US20160101979A1 (enExample)
EP (1) EP3003972A1 (enExample)
JP (1) JP2016520510A (enExample)
KR (1) KR20160015236A (enExample)
CN (1) CN105246825A (enExample)
DE (1) DE102013210679A1 (enExample)
WO (1) WO2014195415A1 (enExample)

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Publication number Priority date Publication date Assignee Title
US10914002B2 (en) * 2015-04-12 2021-02-09 Clb Americas, Inc. Apparatus and process for semi-continuous and multi-step composite production
KR102579608B1 (ko) * 2016-08-04 2023-09-18 에스케이이노베이션 주식회사 탄소나노튜브의 제조방법
US11043338B2 (en) * 2017-11-09 2021-06-22 Korea Research Institute Of Chemical Technology Manufacturing method of porous composite electrode and organic removal method of porous composite electrode
CN108946704B (zh) * 2018-08-20 2020-03-31 山东晶石大展纳米科技有限公司 一种连续化制备高纯碳纳米管的方法及装置
GB201816575D0 (en) * 2018-10-11 2018-11-28 Seeds Capital Ltd Novel carbon nano-structures for energy generation and energy storage applications
KR20210127620A (ko) * 2020-04-13 2021-10-22 에이에스엠 아이피 홀딩 비.브이. 질소 함유 탄소 막을 형성하는 방법 및 이를 수행하기 위한 시스템
JP7712628B2 (ja) * 2021-10-08 2025-07-24 国立大学法人千葉大学 含窒素炭素材料の製造方法
CN114953672B (zh) * 2022-05-30 2023-06-09 常州市贝美家居科技有限公司 一种墙板及其制备工艺
WO2025135042A1 (ja) * 2023-12-22 2025-06-26 住友化学株式会社 炭素および水素の製造方法、及び、炭素繊維

Citations (12)

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Publication number Priority date Publication date Assignee Title
GB1469930A (en) 1974-10-11 1977-04-06 Atomic Energy Authority Uk Carbon filaments
EP0056004A2 (en) 1981-01-05 1982-07-14 Exxon Research And Engineering Company Production of carbon filaments in the presence of iron monoxide
WO1986003455A1 (en) 1984-12-06 1986-06-19 Hyperion Catalysis International, Inc. Carbon fibrils, method for producing same, and compositions containing same
US20030129122A1 (en) * 2001-10-31 2003-07-10 National University Of Singapore Carbon nanotubes fabrication and hydrogen production
US20050063891A1 (en) * 2003-09-02 2005-03-24 Cambridge University Technical Services Limited Method of producing carbon nanoparticles
WO2007118668A2 (de) 2006-04-15 2007-10-25 Bayer Materialscience Ag Verfahren zur herstellung von kohlenstoffnanoröhrchen in einer wirbelschicht
CN101279731A (zh) * 2007-04-06 2008-10-08 阿科玛法国公司 由可再生原料生产碳纳米管的方法
KR20090017889A (ko) * 2007-08-16 2009-02-19 세메스 주식회사 촉매 분산 유동층을 이용한 탄소 나노튜브 합성 장치
WO2009036877A2 (de) 2007-09-14 2009-03-26 Bayer Materialscience Ag Kohlenstoffanoröhrchenpulover, kohlenstoffanoröhrchen und verfahren zu ihrer herstellung
WO2009080204A1 (de) 2007-12-20 2009-07-02 Bayer Technology Services Gmbh Verfahren zur herstellung von stickstoff-dotierten kohlenstoffnanoröhrchen
KR20120001448A (ko) * 2010-06-29 2012-01-04 제일모직주식회사 격벽이 형성된 탄소나노튜브 합성용 유동층 반응기 및 이를 이용한 탄소나노튜브의 합성방법
CN102320593A (zh) * 2011-08-30 2012-01-18 中国科学院金属研究所 高抗氧化性、高纯、单／双壁碳纳米管的可控制备方法

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JP2004277201A (ja) * 2003-03-13 2004-10-07 Mitsubishi Chemicals Corp カーボンナノチューブ
KR100745736B1 (ko) * 2006-02-23 2007-08-02 삼성에스디아이 주식회사 카본나노튜브, 이를 포함한 담지 촉매 및 상기 담지 촉매를이용한 연료전지
DE102009038464A1 (de) * 2009-08-21 2011-02-24 Bayer Materialscience Ag Kohlenstoffnanoröhrchen-Agglomerat
DE102010008173A1 (de) * 2010-02-16 2012-03-01 Bayer Materialscience Aktiengesellschaft Herstellung von Kohlenstoffnanoröhrchen
FR2972942B1 (fr) * 2011-03-21 2017-11-24 Arkema France Procede de fabrication de nanotubes de carbone et appareil pour la mise en oeuvre du procede.

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GB1469930A (en) 1974-10-11 1977-04-06 Atomic Energy Authority Uk Carbon filaments
EP0056004A2 (en) 1981-01-05 1982-07-14 Exxon Research And Engineering Company Production of carbon filaments in the presence of iron monoxide
WO1986003455A1 (en) 1984-12-06 1986-06-19 Hyperion Catalysis International, Inc. Carbon fibrils, method for producing same, and compositions containing same
EP0205556A1 (en) 1984-12-06 1986-12-30 Hyperion Catalysis Int CARBON FIBERS, THEIR PRODUCTION AND COMPOSITIONS CONTAINING THEM.
EP0205556B1 (en) 1984-12-06 1995-05-10 Hyperion Catalysis International, Inc. Carbon fibrils, method for producing same, and compositions containing same
US20030129122A1 (en) * 2001-10-31 2003-07-10 National University Of Singapore Carbon nanotubes fabrication and hydrogen production
US20050063891A1 (en) * 2003-09-02 2005-03-24 Cambridge University Technical Services Limited Method of producing carbon nanoparticles
WO2007118668A2 (de) 2006-04-15 2007-10-25 Bayer Materialscience Ag Verfahren zur herstellung von kohlenstoffnanoröhrchen in einer wirbelschicht
CN101279731A (zh) * 2007-04-06 2008-10-08 阿科玛法国公司 由可再生原料生产碳纳米管的方法
KR20090017889A (ko) * 2007-08-16 2009-02-19 세메스 주식회사 촉매 분산 유동층을 이용한 탄소 나노튜브 합성 장치
WO2009036877A2 (de) 2007-09-14 2009-03-26 Bayer Materialscience Ag Kohlenstoffanoröhrchenpulover, kohlenstoffanoröhrchen und verfahren zu ihrer herstellung
WO2009080204A1 (de) 2007-12-20 2009-07-02 Bayer Technology Services Gmbh Verfahren zur herstellung von stickstoff-dotierten kohlenstoffnanoröhrchen
KR20120001448A (ko) * 2010-06-29 2012-01-04 제일모직주식회사 격벽이 형성된 탄소나노튜브 합성용 유동층 반응기 및 이를 이용한 탄소나노튜브의 합성방법
CN102320593A (zh) * 2011-08-30 2012-01-18 中国科学院金属研究所 高抗氧化性、高纯、单／双壁碳纳米管的可控制备方法

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Publication number Publication date
US20160101979A1 (en) 2016-04-14
EP3003972A1 (de) 2016-04-13
WO2014195415A1 (de) 2014-12-11
JP2016520510A (ja) 2016-07-14
CN105246825A (zh) 2016-01-13
KR20160015236A (ko) 2016-02-12

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