DE10114520A1 - Perfumes and their mixtures are immobilized with silicon dioxide to allow for release at high temperatures without liquefaction of the gel - Google Patents

Perfumes and their mixtures are immobilized with silicon dioxide to allow for release at high temperatures without liquefaction of the gel

Info

Publication number
DE10114520A1
DE10114520A1 DE2001114520 DE10114520A DE10114520A1 DE 10114520 A1 DE10114520 A1 DE 10114520A1 DE 2001114520 DE2001114520 DE 2001114520 DE 10114520 A DE10114520 A DE 10114520A DE 10114520 A1 DE10114520 A1 DE 10114520A1
Authority
DE
Germany
Prior art keywords
release
gel
silicon dioxide
mixtures
perfumes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE2001114520
Other languages
German (de)
Inventor
Florian Wolf
Gerd Mansfeld
Falk Harzke
Joerg Eilers
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Symrise AG
Original Assignee
Haarmann and Reimer GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Haarmann and Reimer GmbH filed Critical Haarmann and Reimer GmbH
Priority to DE2001114520 priority Critical patent/DE10114520A1/en
Priority to AU2002249265A priority patent/AU2002249265A1/en
Priority to PCT/EP2002/002686 priority patent/WO2002076514A2/en
Publication of DE10114520A1 publication Critical patent/DE10114520A1/en
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes
    • C11D3/502—Protected perfumes
    • C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/01—Deodorant compositions
    • A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/01—Deodorant compositions
    • A61L9/014—Deodorant compositions containing sorbent material, e.g. activated carbon
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
    • A61L9/02—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air by heating or combustion
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
    • A61L9/04—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
    • A61L9/04—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating
    • A61L9/048—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating air treating gels

Landscapes

  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Cosmetics (AREA)
  • Silicon Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

Immobilization of perfumes or perfume mixtures with SiO2.

Description

Die Erfindung betrifft die Immobilisierung von Duftstoffen oder Dufstoffmischungen mit Siliciumdioxid und die Verwendung der so hergestellten Parfumgele.The invention relates to the immobilization of fragrances or fragrance mixtures with silicon dioxide and the use of the perfume gels so produced.

Es bestand die Aufgabe Duftstoffe und/oder komplexe Parfumkompositionen zu immobilisieren um diese bei Bedarf durch Erwärmung freizusetzen (thermische Freisetzung). Hierfür werden Materialien benötigt, die auch bei höheren Tempera­ turen (bis 300°C) keine chemischen Zersetzungen oder Reaktionen mit Parfumölen und Trägermaterialien zeigten.The task was to create fragrances and / or complex perfume compositions immobilize to release them by heating if necessary (thermal Release). For this, materials are required, even at higher temperatures (up to 300 ° C) no chemical decomposition or reactions with perfume oils and showed substrates.

Gegenstand der vorliegenden Erfindung ist ein Verfahren zur Immobilsierung von Duftstoffen oder Dufstoffmischungen mit Siliciumdioxid.The present invention relates to a method for immobilizing Fragrances or fragrance mixtures with silicon dioxide.

Ein weiterer Gegenstand der vorliegenden Erfindung ist die Verwendung der durch Immobilsierung von Duftstoffen oder Dufstoffmischungen hergestellten Parfümgele zur thermischen Freisetzung des Duftstoffes oder der Duftstoffe.Another object of the present invention is the use of the Immobilization of perfumes or perfume mixtures produced perfume gels for the thermal release of the fragrance or fragrances.

Aus der Pharmazie sind hochdisperse pyrogene Siliciumdioxide, die sogenannten Aerosile® (Markenname der Firma Degussa), bekannt. Diese Siliciumdioxide sind unbrennbar, nicht toxisch, geruchlos und beispielsweise in Lebensmittelbedarfs­ gegenständen, Spielwaren, Kosmetika, Pharmazeutika zugelassen. Der Schmelz­ bereich liegt bei ca. 1700°C.Pharmaceuticals are highly dispersed fumed silicas, the so-called Aerosile® (brand name of Degussa), known. These are silica non-flammable, non-toxic, odorless and for example in food needs objects, toys, cosmetics, pharmaceuticals approved. The enamel range is approx. 1700 ° C.

Unsere Versuche führten zu dem Ergebnis, dass z. B. das Aerosil V 200 der Firma Degussa ein sehr gutes "Gelierungsmittel" für fast alle Parfumkompositionen ist.Our experiments led to the result that e.g. B. the company's Aerosil V 200 Degussa is a very good "gelling agent" for almost all perfume compositions.

Ein ausreichender Gelierungseffekt wird mit einem Anteil an Aerosil V 200 von 7 bis 15 Gew.-% erreicht. Zur Herstellung wird das Aerosil vorgelegt und der Duftstoff und/oder die komplexe Parfumkomposition hinzugegeben. Anschließend wird die Mischung durch Rühren homogenisiert. A sufficient gelling effect is achieved with a proportion of Aerosil V 200 from 7 to 15 wt .-% reached. The aerosil and the fragrance are presented for manufacture and / or the complex perfume composition is added. Then the Mix homogenized by stirring.  

Mit dieser Entwicklung steht ein Parfumgel zur Verfügung, in dem der Parfumöl­ anteil 85 bis 93% beträgt. Die Freisetzung der Duftstoffe kann kontinuierlich (auch bei Raumtemperatur) erfolgen, da eine "Verkapselung" des Parfumöls nicht erzielt wird.With this development, a perfume gel is available in which the perfume oil share is 85 to 93%. The release of the fragrances can be continuous (too at room temperature) because the perfume oil is not "encapsulated" becomes.

Eine Temperaturerhöhung beschleunigt die Freisetzung des Parfumöls ähnlich wie bei einem flüssig vorliegenden Produkt. Als wichtiger zusätzlicher Effekt ist hervorzuheben, dass sich das Gel auch bei erhöhten Temperaturen nicht verflüssigt, so das ein Ver- oder Auslaufen von Parfumgel-Dosierungen nicht erfolgt. Nach vollständiger Verdampfung des Duftstoffes und/oder der komplexen Parfum­ komposition bleibt als Rückstand das Siliciumdioxid als staubähnlicher Feststoff zurück.An increase in temperature accelerates the release of the perfume oil in a similar way with a liquid product. As an important additional effect to emphasize that the gel does not liquefy even at elevated temperatures, so that perfume gel doses do not run or run out. To complete evaporation of the fragrance and / or the complex perfume The composition remains the silicon dioxide as a dust-like solid back.

Claims (3)

1. Verfahren zur Immobilsierung von Duftstoffen oder Duftstoffmischungen mit Siliciumdioxid.1. Process for immobilizing fragrances or fragrance mixtures with Silica. 2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass der Gehalt an Siliciumdioxid im Parfümgel im Bereich von 7 bis 15 Gew.-% liegt.2. The method according to claim 1, characterized in that the content of Silicon dioxide in the perfume gel is in the range from 7 to 15% by weight. 3. Verwendung der nach wenigstens einem der Ansprüche 1 bis 2 hergestellten Parfümgele zur thermischen Freisetzung des Duftstoffes oder der Duftstoffe.3. Use of the produced according to at least one of claims 1 to 2 Perfume gels for thermal release of the fragrance or fragrances.
DE2001114520 2001-03-23 2001-03-23 Perfumes and their mixtures are immobilized with silicon dioxide to allow for release at high temperatures without liquefaction of the gel Withdrawn DE10114520A1 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
DE2001114520 DE10114520A1 (en) 2001-03-23 2001-03-23 Perfumes and their mixtures are immobilized with silicon dioxide to allow for release at high temperatures without liquefaction of the gel
AU2002249265A AU2002249265A1 (en) 2001-03-23 2002-03-12 Use of solid particles for thermally extracting perfume oils and/or aromas
PCT/EP2002/002686 WO2002076514A2 (en) 2001-03-23 2002-03-12 Use of solid particles for thermally extracting perfume oils and/or aromas

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2001114520 DE10114520A1 (en) 2001-03-23 2001-03-23 Perfumes and their mixtures are immobilized with silicon dioxide to allow for release at high temperatures without liquefaction of the gel

Publications (1)

Publication Number Publication Date
DE10114520A1 true DE10114520A1 (en) 2002-09-26

Family

ID=7678876

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2001114520 Withdrawn DE10114520A1 (en) 2001-03-23 2001-03-23 Perfumes and their mixtures are immobilized with silicon dioxide to allow for release at high temperatures without liquefaction of the gel

Country Status (1)

Country Link
DE (1) DE10114520A1 (en)

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
Chemical Abstract, DN 126:308631 CAPLUS *
JP 06263618 A.,In: Patent Abstracts of Japan *

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Legal Events

Date Code Title Description
OM8 Search report available as to paragraph 43 lit. 1 sentence 1 patent law
8127 New person/name/address of the applicant

Owner name: DRAGOCO GERBERDING & CO. AG, 37603 HOLZMINDEN, DE

8127 New person/name/address of the applicant

Owner name: SYMRISE GMBH & CO. KG, 37603 HOLZMINDEN, DE

8139 Disposal/non-payment of the annual fee