CS207487B2 - Method of extracting the surface non-active material - Google Patents
Method of extracting the surface non-active material Download PDFInfo
- Publication number
- CS207487B2 CS207487B2 CS785077A CS785077A CS207487B2 CS 207487 B2 CS207487 B2 CS 207487B2 CS 785077 A CS785077 A CS 785077A CS 785077 A CS785077 A CS 785077A CS 207487 B2 CS207487 B2 CS 207487B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- ketone
- acetate
- carbon atoms
- weight
- feedstock
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 20
- 239000011149 active material Substances 0.000 title abstract 4
- 150000002576 ketones Chemical class 0.000 claims abstract description 37
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000000284 extract Substances 0.000 claims abstract description 16
- 239000002904 solvent Substances 0.000 claims abstract description 11
- 125000004432 carbon atom Chemical group C* 0.000 claims description 40
- 239000000463 material Substances 0.000 claims description 28
- 239000004094 surface-active agent Substances 0.000 claims description 24
- 239000002994 raw material Substances 0.000 claims description 18
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical group CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 10
- 239000011368 organic material Substances 0.000 claims description 9
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 claims description 8
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 claims description 8
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropanol acetate Natural products CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 claims description 5
- 229940011051 isopropyl acetate Drugs 0.000 claims description 5
- GWYFCOCPABKNJV-UHFFFAOYSA-N isovaleric acid Chemical compound CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 claims description 5
- -1 C6 alkyl acetate Chemical compound 0.000 abstract description 14
- 239000005416 organic matter Substances 0.000 abstract description 2
- 150000001336 alkenes Chemical class 0.000 description 21
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 20
- 238000000605 extraction Methods 0.000 description 17
- 150000003333 secondary alcohols Chemical class 0.000 description 13
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 12
- 239000000203 mixture Substances 0.000 description 10
- 150000003839 salts Chemical class 0.000 description 10
- 239000000126 substance Substances 0.000 description 10
- 229940043265 methyl isobutyl ketone Drugs 0.000 description 7
- 238000006386 neutralization reaction Methods 0.000 description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 5
- 239000003599 detergent Substances 0.000 description 5
- 229910052920 inorganic sulfate Inorganic materials 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 150000001242 acetic acid derivatives Chemical class 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 229910052938 sodium sulfate Inorganic materials 0.000 description 4
- 235000011152 sodium sulphate Nutrition 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
- 239000003502 gasoline Substances 0.000 description 3
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 3
- 159000000000 sodium salts Chemical class 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 230000001180 sulfating effect Effects 0.000 description 2
- 238000005670 sulfation reaction Methods 0.000 description 2
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 2
- 239000004711 α-olefin Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 241000792859 Enema Species 0.000 description 1
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910052936 alkali metal sulfate Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 150000008051 alkyl sulfates Chemical class 0.000 description 1
- 229940045714 alkyl sulfonate alkylating agent Drugs 0.000 description 1
- 150000008052 alkyl sulfonates Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 239000012223 aqueous fraction Substances 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000011033 desalting Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000007920 enema Substances 0.000 description 1
- 229940079360 enema for constipation Drugs 0.000 description 1
- 230000006203 ethylation Effects 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 230000011987 methylation Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000006207 propylation Effects 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000019635 sulfation Effects 0.000 description 1
- 150000003457 sulfones Chemical class 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0488—Flow sheets
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB4983176A GB1553386A (en) | 1976-11-30 | 1976-11-30 | Extraction of non-surface active material from aqueous sulphated or sulphonated organic matter |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS207487B2 true CS207487B2 (en) | 1981-07-31 |
Family
ID=10453710
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS785077A CS207487B2 (en) | 1976-11-30 | 1977-11-28 | Method of extracting the surface non-active material |
Country Status (12)
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB480904A (en) * | 1935-12-24 | 1938-03-02 | Bataafsche Petroleum | A process for refining capillary-active alkyl esters of sulphuric acid and/or salts thereof in aqueous solutions |
| GB480940A (en) * | 1936-10-10 | 1938-03-02 | Bataafsche Petroleum | A process for preparing pure or substantially pure salts of acid esters of polybasic inorganic acids |
| US2700052A (en) * | 1952-03-25 | 1955-01-18 | Kellogg M W Co | Preparation of detergent compositions |
| GB1099784A (en) * | 1965-05-05 | 1968-01-17 | British Hydrocarbon Chem Ltd | Separating alkane sulphonic acids from mixtures |
| FR1547452A (fr) * | 1967-06-12 | 1968-11-29 | Aquitaine Petrole | Procédé de préparation d'acides sulfoniques et de sulfonates organiques |
| US3888917A (en) * | 1968-09-27 | 1975-06-10 | Marathon Oil Co | Organic sulfonate extraction process |
-
1976
- 1976-11-30 GB GB4983176A patent/GB1553386A/en not_active Expired
-
1977
- 1977-10-24 CA CA000289302A patent/CA1120054A/en not_active Expired
- 1977-11-25 BE BE1008543A patent/BE861192A/xx not_active IP Right Cessation
- 1977-11-25 IT IT3009577A patent/IT1143719B/it active
- 1977-11-28 AU AU31018/77A patent/AU510816B2/en not_active Expired
- 1977-11-28 DE DE19772753024 patent/DE2753024A1/de active Granted
- 1977-11-28 CS CS785077A patent/CS207487B2/cs unknown
- 1977-11-28 ES ES464545A patent/ES464545A1/es not_active Expired
- 1977-11-28 JP JP14170377A patent/JPS5368728A/ja active Pending
- 1977-11-28 FR FR7735730A patent/FR2371952A1/fr active Granted
- 1977-11-28 SE SE7713444A patent/SE442296B/sv not_active IP Right Cessation
- 1977-11-28 NL NL7713059A patent/NL7713059A/xx not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| AU510816B2 (en) | 1980-07-17 |
| GB1553386A (en) | 1979-09-26 |
| ES464545A1 (es) | 1978-09-01 |
| DE2753024A1 (de) | 1978-06-01 |
| BE861192A (nl) | 1978-05-25 |
| FR2371952A1 (fr) | 1978-06-23 |
| NL7713059A (nl) | 1978-06-01 |
| CA1120054A (en) | 1982-03-16 |
| SE442296B (sv) | 1985-12-16 |
| SE7713444L (sv) | 1978-05-31 |
| FR2371952B1 (enrdf_load_stackoverflow) | 1981-01-09 |
| IT1143719B (it) | 1986-10-22 |
| DE2753024C2 (enrdf_load_stackoverflow) | 1989-10-05 |
| AU3101877A (en) | 1979-06-07 |
| JPS5368728A (en) | 1978-06-19 |
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