CN86107462A - From the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof - Google Patents
From the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof Download PDFInfo
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- CN86107462A CN86107462A CN 86107462 CN86107462A CN86107462A CN 86107462 A CN86107462 A CN 86107462A CN 86107462 CN86107462 CN 86107462 CN 86107462 A CN86107462 A CN 86107462A CN 86107462 A CN86107462 A CN 86107462A
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Abstract
A kind of method of from the sand sagebrush (Artemisia filifolia) seed, producing colloid and byproduct thereof.Raw material goes out glue and material slag through screening, rinsing, dipping, stirring, centrifugation.Glue makes the aqueous artemisia glue of canescence after the modifying agent conditioning and concentrating; Continue concentrate drying, make the powdery artemisia glue; Material slag after coming unstuck makes byproduct artemisia oil, sand sagebrush (Artemisia filifolia) protein powder and sand sagebrush (Artemisia filifolia) meal through drying, drying, grinding and degreasing.Artemisia glue and byproduct thereof can be widely used in departments such as food, chemical industry, light textile, agricultural, oil.
Description
A kind of relating to from plant seed, particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof.
The existing gelationus method of producing from the sand sagebrush (Artemisia filifolia) seed is: the sand sagebrush (Artemisia filifolia) seed is added clear water dipping 5 minutes, with organizing agitator (8000～15000 rev/mins of rotating speeds) to stir at a high speed 1 minute, the expansible colloid is separated with seed, gained pulpous state liquid is centrifugal with 1500 rev/mins, collect the upper strata glue, centrifugal with 4000～5000 rev/mins again, alcohol embathes, drying under reduced pressure gets white paper pulp shape colloid, and productive rate is about 20%.See the 310th page of " Botany Gazette " magazine 1980 the 22nd the 3rd phase of volume.This method utilization organizes the strong shearing of agitator to smash effect to pieces at a high speed, destroys sand sagebrush (Artemisia filifolia) gelationus knot and forms shape tissue and envelope, and realization material slag (seed) separates with glue.Therefore the sand sagebrush (Artemisia filifolia) gelationus glue unit molecular weight of being produced is little, and glue fiber is short, and the gelatin viscosity value is low, can not satisfy the needs of industrialness production and application.Present this method is only made physico-chemical analysis for the laboratory and is used with test.
The inventor has proposed a kind of sand sagebrush (Artemisia filifolia) gelationus processing method of producing in No. 85108918, Chinese patent application.This method is: with the fragmentation of sand sagebrush (Artemisia filifolia) seed, with the aqueous solution dipping stripping colloid that is added with 5～30% conditioning agent (edible gum), filtration under diminished pressure makes Powdered artemisia glue after the drying and crushing.This method is used the expensive edible gum of volume in the course of processing, so the production cost height; Adopt the filtration under diminished pressure method to separate glue, gelationus productive rate and output are lower; Material slag (byproduct) is not considered comprehensive utilization yet.
In order to address the above problem, it is easy to the purpose of this invention is to provide a kind of technology, production cost is low, and is good in economic efficiency, the method for aqueous and powdery artemisia glue and the byproduct thereof of producing departments such as can being directly used in food, chemical industry, light industry, agricultural, oil from the sand sagebrush (Artemisia filifolia) seed that productive rate and output are high.
Method of the present invention is: raw material (sand sagebrush (Artemisia filifolia) seed) passes through screening, rinsing, floods, adds modifying agent Tiao Li And stirring, centrifugation goes out glue and material slag (seed), glue is nursed one's health with modifying agent, after concentrating or concentrating, add the modifying agent conditioning once more, promptly make the aqueous artemisia glue that can be directly used in foodstuff additive and other industrial uses.Before the raw material dipping earlier through rinsing, can further remove be difficult to isolating “ And with conventional cleaning (screening) machinery in the sand sagebrush (Artemisia filifolia) seed and take on stone " impurity such as (a kind of sand grains close) and not plump shell with the sand sagebrush (Artemisia filifolia) seed size, thereby improve quality product.Add modifying agent during stirring and can make the pH value of feed liquid and the requirement that the gelationus swelling property meets product specification.Change the kind of modifying agent and the relevant processing parameter (as churning time) of the corresponding change present method of addition ， And, can obtain all different artemisia glue series product of physical and chemical index and purposes.Said physical and chemical index refers to that gelationus swelling dispersiveness, viscosity, knot form complexing power (glue fiber length) and color and luster, smell etc.Separate feed liquid with centrifuging and can separate discharging slag and colloid with no damage, And can simplify technology, improve output and productive rate.With modifying agent nurse one's health isolated glue (at enrichment process forward and backward or respectively the conditioning all can), () ， And such as color and luster, fragrance can improve its keeping quality can further to improve gelationus physical and chemical index or apparent proterties.
Be added with alkaline matter in the steeping fluid, its concentration is 0～1%, 15～50 ℃ of dipping temperatures, and preferably 40 ℃, dipping time is 10～60 minutes, is determined by experiment.Raw material adopts the advantage of alkaline impregnation to be to strengthen sand sagebrush (Artemisia filifolia) gelationus intensity, improves the viscosity and the toughness of feed liquid.After alkali lye was handled, the flavonoid pigment stripping in the raw material sand sagebrush (Artemisia filifolia) seed was removed after washing, can improve glue color and luster (becoming white powder by yellow-green colour).Alkaline matter also can impel the protein composition sex change Chen Dian And in the colloid to be removed, thereby has improved the preservation stability of glue, suppresses its brown stain.
Adopt rotating speed be 150～1000 rev/mins in, the stirrer of low speed stirs feed liquid, churning time is 30 seconds～60 minutes.Be characterized in that the mixer arm shearing force is little, both can promote gelationus swelling and homogeneous, unlikely again glue fiber is shredded.The purpose that stirs is not for separating material slag and colloid.Control different churning time (when stirrer rotating speed and one timing of paddle shape) and can produce the artemisia glue series product (aqueous) of various viscosity and swelling dispersion proterties easily.
This glue is through secondary concentration, and is dry under the cold condition below 75 ℃, can be made into the artemisia glue of powder (end) shape after the pulverizing.The powdery artemisia glue has kept the physicochemical property of aqueous artemisia glue substantially, but uses more conveniently, and is convenient to transportation and stores.
The material slag that is gone out by centrifugation is through secondary degumming, and centrifuge dripping is dry under 40～50 ℃ of temperature, through grind, screening, screen overflow (bran composition) and screen underflow degreasing (conventional milling process) respectively can make artemisia oil, sand sagebrush (Artemisia filifolia) protein powder and sand sagebrush (Artemisia filifolia) meal.And can be through further processing products such as extracting vitamin-E, tryptophane, calcium reinforcement powder, linolic acid from above byproduct.
Alkaline matter in the steeping fluid can be that " fluffy ash " (a kind of food natural mineral matter that contains alkaline matter), yellow soda ash (calcium), sodium hydroxide (potassium, calcium), calcium oxide, alkaline phosphate and other allow to be used for the alkaline chemical of food.
The modifying agent that feed liquid and concentrated glue are stirred in conditioning can be edible acids such as hydrochloric acid, citric acid, oxysuccinic acid; Can be edible gum classes such as sodium alginate, guar gum, pectin; Can be food antisepticses such as Sorbic Acid; Also can be flavouring agent (essence) or salt, xitix, Repone K, phosphoric acid salt, alum etc.Addition is 0～3% of a glue.
But fulling mill that the present invention selects for use or equipment continuously feeding, discharge ， And can wash the impurity at rinsing liquid bottom and top.
The stirrer that the present invention selects for use has at least two grid of rotating in opposite directions or the stirring blade of cydariform (bird-caging).As beating machiae.
The whizzer of the separation feed liquid that the present invention selects for use can be continuously or discontinuous operation, has the equipment and the function of separating material slag (seed), as basket-hanging, butterfly chip whizzer and follow-on specific equipment thereof.The centrifugal time is determined by experiment according to separating effect.
The whizzer that the present invention selects for use the concentrated glue of work to use can be general butterfly chip or spinning liquid whizzer.Be used to expect that the equipment of slag secondary degumming can be to produce the used stirring of colloid, centrifugation and concentrating unit; It can be above-mentioned suspended centrifugal that the material slag dries used whizzer.
Method therefor technology of the present invention is simple, production cost low (can be less with or need not expensive food glue), and (efficient of centrifugation can reach tens of times of low pressure filtration method for output and productive rate height.The aqueous artemisia glue of products obtained therefrom is 30 times of raw material weight, Powdered artemisia glue be raw material weight 20%), made full use of byproduct, so economic benefit is very high, is suitable for large-scale industrial production in addition.The aqueous artemisia glue tool that the present invention produced half is mobile, and the apparent proterties of colloid is between colloidal sol and gel.Viscosity (1% solution) is between 20～1000 ° of E of viscosity Engler, and its swelling dispersiveness reduces with viscosity and increases, and glue fiber intensity and forming property of knot then increase with viscosity number.Change the artemisia glue (aqueous) that relevant processing parameter and modifying agent prescription can obtain various trait and purposes, can be widely used in departments such as food, light industry, chemical industry, weaving, oil and agricultural and do uses such as bonding complexing agent, thickening material, emulsion stabilizer, whipping agent, liniment.The Powdered artemisia glue that the present invention produced is a beige, except that the features and applications with above-mentioned aqueous artemisia glue, also has use, convenient transportation, the advantage of long preservative period.
Contain linolic acid 49.5% in the byproduct artemisia oil that the present invention produces, the about 600 milligrams/hectogram of vitamin-E (oil) is the very high grease of a kind of nutritive value, can be edible or make the paint industry raw material, and productive rate is about 20%.Contain biological value in the sand sagebrush (Artemisia filifolia) protein powder and be more than 66 the full price protein 60 %, all the other still have the volume tryptophane and the nutritive elements such as the calcium of powder content, phosphorus, iron that are equivalent to suckle, and can make food fortifier, or extract above-mentioned effective ingredient through deep processing.Productive rate is about 35%.Still contain multiple nutrients in the sand sagebrush (Artemisia filifolia) meal (bran), additive capable of using as feed, productive rate are about 12%.The gross output value of the said products (comprising byproduct) is 2～3 times of raw material valency, and promptly per kilogram sand sagebrush (Artemisia filifolia) seed can get 2.5 yuan of processing profits about (Renminbi).
Drawings attached of the present invention.
Fig. 1 is a process flow sheet of producing the method for colloid and byproduct thereof from the sand sagebrush (Artemisia filifolia) seed.
The present invention has 2 embodiment.
Embodiment 1:(most preferred embodiment adopts the described technical process of Fig. 1)
100 kilograms of sand sagebrush (Artemisia filifolia) seed raw materials, get 98 kilograms of pure product through screen, add fulling mill and use clear water rinsing 1 minute, despumation, move into impregnating autoclave, add 10 kilograms in yellow soda ash, add water to 3 tons, dipping is 30 minutes under 40 ℃ of water temperatures, discharge alkali lye (recyclable use again), feed liquid with flushing with clean water to pH value 8 when following, add water to 4 tons, move into stirrer, to nurse one's health to pH value be 6.5 And stirred 2 minutes with 600 rev/mins rotating speed with hydrochloric acid, moves into suspended centrifugal (mesh size 1.2 millimeter) with 2000 rev/mins rotating speed centrifugal 8 minutes, and isolated glue concentrates 3 minutes with 2500 rev/mins rotating speed again in butterfly chip whizzer, it is an amount of to add Sorbic Acid and essence, promptly get viscosity greater than 800 ° of E(estimated values) knot form 2.5 tons of shape glues, can directly be used as vermicelli, bean vermicelli, jam, jelly, the improvement of food such as ice-creams (additive) also can be done papermaking, the modifying agent of textile product.Above-mentioned glue concentrates as continuing, and below 75 ℃, Di temperature Gan Zao And pulverizes, and can make the Powdered colloid of beige, and about 21 kilograms of productive rate can be made the colloid of bread improver and above-mentioned various uses.Isolated material slag secondary adds water and comes unstuck, it is dry under 40～50 ℃ of temperature to dry ， And through suspended centrifugal, grinds, screening (80 order), obtain sand sagebrush (Artemisia filifolia) powder and bran (screen overflow), extract grease, make 21 kilograms of artemisia oils through lixiviation process, sand sagebrush (Artemisia filifolia) protein powder (screen underflow, canescence) 35 kilograms, 12 kilograms of sand sagebrush (Artemisia filifolia) meal (screen overflow, dark brown).About 500 yuan of the above product gross output value.
Embodiment 2:
100 kilograms of sand sagebrush (Artemisia filifolia) seed raw materials, get 98 kilograms of pure product through screen, add fulling mill clear water rinsing 1 minute, despumation, move into impregnating autoclave, add 1 kilogram in yellow soda ash, add 3 tons in water, 40 ℃ of dippings of control water temperature 10 minutes, discharge alkali lye (recyclable use again), feed liquid is below 7.5 with flushing with clean water to pH value, adds water to 4 tons, moves into stirrer, 8 kilograms of 4 kilograms of adding citric acids and sodium alginates conditioning And stirred 30 minutes with 1000 rev/mins rotating speed, afterwards feed liquid was moved into suspended centrifugal with 1000 rev/mins rotating speed centrifugal 3 minutes, and isolated glue moves into butterfly chip whizzer and concentrates 2 minutes with 2000 rev/mins, it is an amount of to add 10 kilograms in Repone K and essence, promptly make the sand sagebrush (Artemisia filifolia) glue that oyster white or canescence viscosity are lower than 30 ° of E, can be used for fruit, egg coating antistaling agent and make various stablizers, emulsifying agent or make other industrial glue, this glue productive rate is 3 tons.Isolated material slag secondary adds water and comes unstuck, and it is dry under 40～50 ℃ of temperature to dry ， And through suspended centrifugal, grinds, and (80 order) ， And degreasings get 20 kilograms of artemisia oils, 35 kilograms of sand sagebrush (Artemisia filifolia) protein powders, 12 kilograms of sand sagebrush (Artemisia filifolia) meal, about 500 yuan of the product gross output value in screening.
Claims (10)
1, a kind of from plant seed, particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, raw material (sand sagebrush (Artemisia filifolia) seed) is through screening, dipping, concentrated aqueous artemisia glue and the material slag made, it is characterized in that (screening back) also passed through rinsing, (dipping), added modifying agent conditioning and stirring, after centrifugation goes out glue and material slag, add modifying agent and nurse one's health glue and also (concentrate).
2, described a kind of from plant seed according to claim (1), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that being added with in the steeping fluid alkaline matter, its concentration is 0～1%, 15～50 ℃ of dipping temperatures, preferably 40 ℃, dipping time is 10～60 minutes.
3, described a kind of from plant seed according to claim (1) or (2), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that adopting rotating speed be 150～1000 rev/mins in, low-speed mixer stirs feed liquid, churning time is 30 seconds～60 minutes.
4, described a kind of from plant seed according to claim (1) or (2), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that glue through secondary concentration, the artemisia glue of powder (end) shape is made in cryodrying below 75 ℃ after the pulverizing.
5, described a kind of from plant seed according to claim (3), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that glue through secondary concentration, cryodrying below 75 ℃.Make the artemisia glue of powder (end) shape after the pulverizing.
6, described a kind of from plant seed according to claim (1) or (2), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that expecting that slag is through secondary degumming, centrifuge dripping, dry under 40～50 ℃ of temperature, grind screening, screen overflow (bran composition) and screen underflow degreasing respectively make artemisia oil, sand sagebrush (Artemisia filifolia) protein powder and sand sagebrush (Artemisia filifolia) meal.
7, described a kind of from plant seed according to claim (3), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that expecting that slag is through secondary degumming, centrifuge dripping, dry under 40～50 ℃ of temperature, grind screening, screen overflow (bran composition) and screen underflow degreasing respectively make artemisia oil, sand sagebrush (Artemisia filifolia) protein powder and sand sagebrush (Artemisia filifolia) meal.
8, described a kind of from plant seed according to claim (2), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that the alkaline matter in the steeping fluid can be " fluffy ash " (a kind of food natural mineral matter that contains alkaline matter), yellow soda ash (calcium), sodium hydroxide (potassium, calcium), calcium oxide, alkaline phosphate and other allow to be used for the alkaline chemical of food.
9, described a kind of from plant seed according to claim (1) or (2), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that nursing one's health the modifying agent that stirs feed liquid and concentrated glue can be edible acids such as hydrochloric acid, citric acid, oxysuccinic acid, can be edible gum classes such as sodium alginate, guar gum, pectin, can be food antisepticses such as Sorbic Acid, also can be flavouring agent (essence) or salt, xitix, Repone K, phosphoric acid salt, alum etc., addition be 0～3% of a glue.
10, described a kind of from plant seed according to claim (3), particularly from the sand sagebrush (Artemisia filifolia) seed, produce the method for colloid and byproduct thereof, it is characterized in that nursing one's health the modifying agent that stirs feed liquid and concentrated glue can be edible acids such as hydrochloric acid, citric acid, oxysuccinic acid, can be edible gum classes such as sodium alginate, guar gum, pectin, can be food antisepticses such as Sorbic Acid, also can be flavouring agent (essence) or salt, xitix, Repone K, phosphoric acid salt, alum etc., addition be 0～3% of a glue.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN86107462A CN86107462B (en) | 1986-11-04 | 1986-11-04 | Process for producing gum from seeds of wormwood |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN86107462A CN86107462B (en) | 1986-11-04 | 1986-11-04 | Process for producing gum from seeds of wormwood |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN86107462A true CN86107462A (en) | 1987-07-22 |
| CN86107462B CN86107462B (en) | 1988-09-07 |
Family
ID=4803571
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN86107462A Expired CN86107462B (en) | 1986-11-04 | 1986-11-04 | Process for producing gum from seeds of wormwood |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN86107462B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102504650A (en) * | 2011-10-26 | 2012-06-20 | 甘肃省博物馆 | Preparation method and application of composite material for protecting paper files |
| CN103113484A (en) * | 2013-01-29 | 2013-05-22 | 陕西师范大学 | Processing method of sand sagebrush emulsifier |
| CN104799275A (en) * | 2015-03-20 | 2015-07-29 | 赤峰金淼食品科技有限公司 | Preparation method for preparing artemis sphaerocephala krasch seed mixing powder |
| CN106977613A (en) * | 2016-01-18 | 2017-07-25 | 王耀富 | A kind of method that artemisia desertorum polysaccharide is extracted in the seed from sand sagebrush (Artemisia filifolia) |
| CN108338355A (en) * | 2018-02-10 | 2018-07-31 | 张芸 | A kind of preparation method of food thickening agent |
| CN109265575A (en) * | 2018-09-03 | 2019-01-25 | 西北大学 | A kind of 4 oxygen methyl glucose uronic acid class xylans obtained from artemisia seed gum and its application in terms of inhibiting liver tumour |
| CN115093733A (en) * | 2022-06-13 | 2022-09-23 | 内蒙古伏羲文化传播有限公司 | Sand-made 3D color-fixing sand painting sand-art environment-friendly material and application thereof |
-
1986
- 1986-11-04 CN CN86107462A patent/CN86107462B/en not_active Expired
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102504650A (en) * | 2011-10-26 | 2012-06-20 | 甘肃省博物馆 | Preparation method and application of composite material for protecting paper files |
| CN102504650B (en) * | 2011-10-26 | 2013-11-06 | 甘肃省博物馆 | Preparation method and application of composite material for protecting paper files |
| CN103113484A (en) * | 2013-01-29 | 2013-05-22 | 陕西师范大学 | Processing method of sand sagebrush emulsifier |
| CN103113484B (en) * | 2013-01-29 | 2016-01-13 | 陕西师范大学 | A kind of working method of sand sagebrush emulsifier |
| CN104799275A (en) * | 2015-03-20 | 2015-07-29 | 赤峰金淼食品科技有限公司 | Preparation method for preparing artemis sphaerocephala krasch seed mixing powder |
| CN104799275B (en) * | 2015-03-20 | 2017-07-14 | 赤峰金淼食品科技有限公司 | The preparation method that modulation sand sagebrush (Artemisia filifolia) seed reconstitutes powder |
| CN106977613A (en) * | 2016-01-18 | 2017-07-25 | 王耀富 | A kind of method that artemisia desertorum polysaccharide is extracted in the seed from sand sagebrush (Artemisia filifolia) |
| CN106977613B (en) * | 2016-01-18 | 2020-01-17 | 王耀富 | Method for extracting artemisia desertorum polysaccharide from artemisia desertorum seeds |
| CN108338355A (en) * | 2018-02-10 | 2018-07-31 | 张芸 | A kind of preparation method of food thickening agent |
| CN109265575A (en) * | 2018-09-03 | 2019-01-25 | 西北大学 | A kind of 4 oxygen methyl glucose uronic acid class xylans obtained from artemisia seed gum and its application in terms of inhibiting liver tumour |
| CN109265575B (en) * | 2018-09-03 | 2020-11-06 | 西北大学 | 4O-methylglucuronic acid xylan obtained from Artemisia desertorum seed gum and its application in inhibiting liver tumor |
| CN115093733A (en) * | 2022-06-13 | 2022-09-23 | 内蒙古伏羲文化传播有限公司 | Sand-made 3D color-fixing sand painting sand-art environment-friendly material and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN86107462B (en) | 1988-09-07 |
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