CN2899931Y - Organic synthesizing device for laboratory - Google Patents

Organic synthesizing device for laboratory Download PDF

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Publication number
CN2899931Y
CN2899931Y CNU2006200297038U CN200620029703U CN2899931Y CN 2899931 Y CN2899931 Y CN 2899931Y CN U2006200297038 U CNU2006200297038 U CN U2006200297038U CN 200620029703 U CN200620029703 U CN 200620029703U CN 2899931 Y CN2899931 Y CN 2899931Y
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CN
China
Prior art keywords
organic matter
matter container
container
magnet
organic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CNU2006200297038U
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Chinese (zh)
Inventor
马首锋
禹殿波
张小林
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GONGYI YVHUA INSTRUMENT CO Ltd
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GONGYI YVHUA INSTRUMENT CO Ltd
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Priority to CNU2006200297038U priority Critical patent/CN2899931Y/en
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Publication of CN2899931Y publication Critical patent/CN2899931Y/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model discloses an organic synthesis device for the laboratory, which comprises a machine body, a stirring mechanism, a heating mechanism, a cooling mechanism, an organic matter vessel, a power mechanism, a drive mechanism and an electrical control mechanism; wherein a certain number of organic matter vessels are arranged on the middle baffle plate and the upper end panel of the machine body, the lower part of the organic matter vessel is provided with the heating mechanism, the back side of the organic matter vessel is provided with the cooling mechanism, the lower outer wall of the organic matter vessel is provided with a thermoscope, the heating mechanism, the cooling mechanism and the thermoscope are respectively connected with the electrical control mechanism, the lower part of the machine body is provided with a magnet tray and a magnet corresponding with the organic matter vessel, a rotary shaft of the magnet tray is respectively connected with the power mechanism through the drive mechanism, the magnetic blocks in the magnet tray, the magnet and the organic matter vessel form the stirring mechanism, the upper end of the organic matter vessel is provided with a plunger piston in order to conveniently take out the organic matter or fill the vessel with the inert gas. The utility model has the rational design and novel structure and can control the temperature of each organic matter vessel and have the high precision temperature control, thereby is safe to be used and has better economic benefits.

Description

The laboratory organic synthesis plant
One. technical field: the utility model relates to a kind of reaction synthesis device, particularly relates to a kind of laboratory organic synthesis plant.
Two. background technology: along with the raising and the expanding economy of technology, China progressively strengthens the technology and economic input of organic synthesis research, and obtain significant achievement, but, owing to be subjected to the restriction of domestic and international condition, cause China at design of organic synthesis instrument and manufacture view and there is a certain distance abroad.(Granted publication number is CN2616537Y to Chinese patent, the patent No. is 02233602.8) a kind of " organic compound synthesizer " disclosed, it mainly is made up of synthetic kettle, condensing reflux tower, automatically unloading annex, heating jacket, center cooling coil, it adopts multiple cooling provision, course of reaction is controlled easily, pressure can not occur raises and the material from leakage phenomenon, but, it is used in the needs of large-scale production, complex structure, cost is higher, can not be used in the demand of scientific research institution, and it is promoted market and is restricted.
Three. the utility model content:
The purpose of this utility model: overcome the defective of prior art, provide a kind of, simple in structure, cost is lower, can be simultaneously carry out different temperatures control and the high laboratory organic synthesis plant of temperature control precision to a plurality of organic matter containers.
The technical solution of the utility model: a kind of laboratory organic synthesis plant, contain organism, rabbling mechanism, heating arrangements, cooling body, the organic matter container, actuating unit, transmission mechanism and electrical equipment control mechanism, wherein the organic matter container of some is installed on the intermediate membrane and upper end plate of body by geometrical clamp respectively, described organic matter container bottom is provided with heating arrangements, thereafter the side is provided with cooling body, and the outer wall of organic matter container is provided with thermal detector, heating arrangements, cooling body and thermal detector connect with electrical equipment control mechanism respectively, to control the temperature in each organic matter container, underpart is equipped with and organic matter container lifting magnet and magnet one to one, the rotating shaft of lifting magnet connects with actuating unit respectively by transmission mechanism, described lifting magnet, magnetic patch in magnet and the organic matter container constitutes rabbling mechanism, the organic matter container upper end is provided with plunger, is convenient to extract organic matter or filling with inert gas in container.
Described organic matter container bottom is installed on the intermediate membrane of body by following geometrical clamp, and be provided with the temperature adjustment rod of heating arrangements in the following geometrical clamp, organic matter container top is installed on the temperature control panel of side, back by last geometrical clamp, the trailing flank of temperature control panel contacts with the coldplate of cooling body, be provided with the pipeline of arranging according to certain rule in the coldplate, described pipe ends is communicated with cooling liquid inlet and cooling liquid outlet respectively, the leading flank of temperature control panel is provided with dividing plate, and adjacent organic matter container is spaced from each other; The upper end plate of body is all run through in all organic matter container upper end portions, and its upper port is provided with the sealing capping plug, the outside of all organic matter container upper end portions and sealing capping plug all is set with container cover plate, and all container cover plates make all organic matter container relative fixed by bolting together.
Be respectively equipped with on the described body leading flank and organic matter container electrical control panel one to one, this panel is provided with display list and switch, and underpart is equipped with the wiring board of electrical equipment control mechanism, and electric component connects by lead.
Described organic matter container is a teat glass, or is the metal test tube; Described transmission mechanism is belt and belt pulley, or is chain and sprocket wheel; Described actuating unit is a motor; Described heating arrangements is an electrical heating mechanism, and its temperature adjustment rod connects with power supply by lead.
The top of described body is provided with the double glazing cover.
The beneficial effects of the utility model:
1. the utility model can carry out different temperatures control and temperature control precision height to a plurality of organic matter containers simultaneously, it adopts a plurality of organic matter containers, and the following heating temperature adjustment rod that all is equipped with of each container, heat as required, be provided with coldplate in container rear in addition, can carry out cooling to container, intensification and cooling by not stopping like this, guarantee the needed temperature of each container, make different organic matters keep different reaction temperatures, use very convenient, thermal detector connects with electrical equipment control mechanism in addition, at any time heating and cooling are adjusted, so its temperature controlled precision height, temperature can accurately be controlled at ± 0.5 ℃ scope in, improve the accuracy and the efficient of synthetic reaction.
2. the utility model modern design, simple in structure, in the organic matter container, put into magnetic patch, thereunder be provided with rotating magnet, drive magnetic patch by the magnet that rotates and in container, rotate, thereby realize stirring, the seal of vessel problem of having avoided conventional plug-in type agitator to cause like this, therefore reasonable in design, each parts is made easily in addition, and cost is lower, its rotating speed can show by display list, be convenient to control rate.
3. the utility model is safe in utilization, and the expansion of liquids formula safety that the heating accessory adopts design temperature independent of each other to regulate is just in case leak electricity, when surpassing capping, heating power supply cuts off automatically, the situation that temperature is too high, influence synthetic reaction can not occur, and is fool proof.In addition, be equipped with the very high reflux condensing tube of backflow efficient, can have realized long-time reaction, improved combined coefficient on test tube top.
4. the utility model scope of application is wide, and extensive market is convenient to promotion and implementation, has better economic and social benefit.
Four. description of drawings:
Fig. 1 is the structural representation of laboratory with organic synthesis plant
Fig. 2 is the left-hand sectional structure chart of laboratory shown in Figure 1 with organic synthesis plant
Five. the specific embodiment:
Embodiment: referring to Fig. 1 and Fig. 2, among the figure, the bottom of five teat glasses 4 is installed on the intermediate membrane of body 18 by fixing 8 folders down, and be provided with the temperature adjustment rod 22 of heating arrangements in the following geometrical clamp 8, teat glass 4 tops are installed on the temperature control panel 25 of side, back by last geometrical clamp 24, the trailing flank of temperature control panel 25 contacts with the coldplate of cooling body 7, be provided with the pipeline of arranging according to certain rule in the coldplate 7, pipe ends is communicated with cooling liquid inlet 20 and cooling liquid outlet 19 respectively, the leading flank of temperature control panel 25 is provided with dividing plate, and adjacent glass test tube 4 is spaced from each other; The outer wall of teat glass 4 is provided with thermal detector (not drawing among the figure), heating arrangements, cooling body and thermal detector connect with electrical equipment control mechanism respectively, to control the temperature in each teat glass 4, crossbearer 11 is installed in the bottom of body 18 by perpendicular frame 15, on crossbearer 11, be separately installed with and teat glass 4 lifting magnet 10 and magnet 9 one to one, the rotating shaft of lifting magnet 10 connects with motor 13 respectively by transmission mechanism 12, lifting magnet 10, magnetic patch (not drawing among the figure) in magnet 9 and the teat glass 4 constitutes rabbling mechanism, driving magnetic patch by the magnet 9 that rotates rotates in teat glass 4, thereby realize stirring, the seal of vessel problem of having avoided conventional plug-in type agitator to cause like this, teat glass 4 upper ends are provided with plunger 2, are convenient to extract organic matter or to filling with inert gas in vitro.Teat glass 4 upper port are provided with sealing ring 5 and sealing capping plug 1, and the outside of teat glass 4 upper ends and sealing capping plug 1 all is set with container cover plate 3, and all container cover 3 plates are fixed together by bolt 6, guarantee all teat glass 4 relative fixed.The front panel 16 of body 18 is respectively equipped with and teat glass 4 electrical control panel 17 and battery main switch one to one, this panel 17 is provided with display list and switch, the wiring board of electrical equipment control mechanism is installed on the support 14 of body 18 bottoms, electric component connects by lead, wherein electrical equipment control mechanism and the electric elements that adopted are existing common technology, do not describe in detail.
As required, teat glass 4 also can replace with other container, such as adopting metal test tube etc.; Transmission mechanism is 12 can be belt and belt sheave structure, also can be chain and chain sprocket structure; The top of body 18 is provided with double glazing cover 21.
This device by heat up and cooling do not stop regulate, guarantee each teat glass 4 needed temperature, make different organic matters keep different reaction temperatures, therefore present embodiment can carry out five kinds of research experiments under the condition of different temperatures, improved combined coefficient, certainly, the quantity of teat glass 4 also can be four, six, eight or the like, determines as required.
The specific constructive form of the value volume and range of product of change teat glass and heating arrangements, cooling body can be formed a plurality of embodiment, is common excursion of the present utility model, does not describe in detail one by one at this.

Claims (5)

1. laboratory organic synthesis plant, contain organism, rabbling mechanism, heating arrangements, cooling body, the organic matter container, actuating unit, transmission mechanism and electrical equipment control mechanism, it is characterized in that: the organic matter container of some is installed on the intermediate membrane and upper end plate of body by geometrical clamp respectively, described organic matter container bottom is provided with heating arrangements, thereafter the side is provided with cooling body, and the outer wall of organic matter container is provided with thermal detector, heating arrangements, cooling body and thermal detector connect with electrical equipment control mechanism respectively, to control the temperature in each organic matter container, underpart is equipped with and organic matter container lifting magnet and magnet one to one, the rotating shaft of lifting magnet connects with actuating unit respectively by transmission mechanism, described lifting magnet, magnetic patch in magnet and the organic matter container constitutes rabbling mechanism, the organic matter container upper end is provided with plunger, is convenient to extract organic matter or filling with inert gas in container.
2. laboratory according to claim 1 organic synthesis plant, it is characterized in that: described organic matter container bottom is installed on the intermediate membrane of body by following geometrical clamp, and be provided with the temperature adjustment rod of heating arrangements in the following geometrical clamp, organic matter container top is installed on the temperature control panel of side, back by last geometrical clamp, the trailing flank of temperature control panel contacts with the coldplate of cooling body, be provided with the pipeline of arranging according to certain rule in the coldplate, described pipe ends is communicated with cooling liquid inlet and cooling liquid outlet respectively, the leading flank of temperature control panel is provided with dividing plate, and adjacent organic matter container is spaced from each other; The upper end plate of body is all run through in all organic matter container upper end portions, and its upper port is provided with the sealing capping plug, the outside of all organic matter container upper end portions and sealing capping plug all is set with container cover plate, and all container cover plates make all organic matter container relative fixed by bolting together.
3. laboratory according to claim 1 and 2 organic synthesis plant, it is characterized in that: be respectively equipped with on the described body leading flank and organic matter container electrical control panel one to one, this panel is provided with display list and switch, underpart is equipped with the wiring board of electrical equipment control mechanism, and electric component connects by lead.
4. laboratory according to claim 3 organic synthesis plant is characterized in that: described organic matter container is a teat glass, or is the metal test tube; Described transmission mechanism is belt and belt pulley, or is chain and sprocket wheel; Described actuating unit is a motor; Described heating arrangements is an electrical heating mechanism, and its temperature adjustment rod connects with power supply by lead.
5. laboratory according to claim 4 organic synthesis plant is characterized in that: the top of described body is provided with the double glazing cover.
CNU2006200297038U 2006-01-04 2006-01-04 Organic synthesizing device for laboratory Expired - Lifetime CN2899931Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU2006200297038U CN2899931Y (en) 2006-01-04 2006-01-04 Organic synthesizing device for laboratory

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNU2006200297038U CN2899931Y (en) 2006-01-04 2006-01-04 Organic synthesizing device for laboratory

Publications (1)

Publication Number Publication Date
CN2899931Y true CN2899931Y (en) 2007-05-16

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Application Number Title Priority Date Filing Date
CNU2006200297038U Expired - Lifetime CN2899931Y (en) 2006-01-04 2006-01-04 Organic synthesizing device for laboratory

Country Status (1)

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CN (1) CN2899931Y (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108031140A (en) * 2018-01-22 2018-05-15 上海仪乐智能仪器有限公司 A kind of automatic lot reflux condensate device
CN109259513A (en) * 2018-09-25 2019-01-25 湘南学院 A kind of chemistry teaching displaying device and its application method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108031140A (en) * 2018-01-22 2018-05-15 上海仪乐智能仪器有限公司 A kind of automatic lot reflux condensate device
CN109259513A (en) * 2018-09-25 2019-01-25 湘南学院 A kind of chemistry teaching displaying device and its application method

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CX01 Expiry of patent term

Granted publication date: 20070516

EXPY Termination of patent right or utility model