CN2841122Y - Portable constant-temperature solid-liquid separating device - Google Patents
Portable constant-temperature solid-liquid separating device Download PDFInfo
- Publication number
- CN2841122Y CN2841122Y CN 200520098698 CN200520098698U CN2841122Y CN 2841122 Y CN2841122 Y CN 2841122Y CN 200520098698 CN200520098698 CN 200520098698 CN 200520098698 U CN200520098698 U CN 200520098698U CN 2841122 Y CN2841122 Y CN 2841122Y
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- chuck
- constant temperature
- solid
- circulation fluid
- liquid separation
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Abstract
The utility model discloses a portable constant-temperature solid-liquid separating device which is mainly composed of a circulating bath constant-temperature system, a feeding mixing system and a jacketed solid-liquid separating system. The device can feed during mixing in a constant-temperature state to achieve the constant-temperature solid-liquid separation. The utility model is suitable for the separation of mixtures and the purification of products in chemical experiment. The utility model has the advantages of easy operation, safe use, stable condition, convenient carrying, etc.
Description
Technical field
The utility model relates to chemical experimental facilities field, particularly a kind of portable constant temperature equipment for separating liquid from solid.
Background technology
Chinese patent 91226168.4 has been announced a kind of " novel filtration and suction filtration device " of being made up of funnel and bottle,suction, be characterized in that funnel and bottle,suction all have the water filling interlayer, although this device has overcome traditional Buchner funnel and bottle,suction when the recrystallization operation, the easily too early crystallization of saturated solution in the heat filter, stop up filter opening, the saturated solution that leaches in the bottle,suction is early analysed because of being cooled off by air, be difficult for inclining and defective such as, but it is synthetic only to be used for trace and semimicro, nor should be used for the separation between the big material of viscosity.
Summary of the invention
In order to overcome the problem that said apparatus exists, the utility model is on the basis of existing " novel filtration and suction filtration device ", a kind of portable constant temperature equipment for separating liquid from solid is provided, but this device has been paid special attention to constant temperature, can have been stirred the structural design of continued operation aspect, can be under condition of stirring while feeding in raw material, finish constant temperature Separation of Solid and Liquid operation experiments, be applicable to the separation of mixture in the chemical experiment and the purifying of product, have easy and simple to handle, safe in utilization, advantages such as conditional stability, and in light weight, volume is little, be easy to carry.
The technical scheme in the invention for solving the technical problem is as follows: this device is mainly bathed constant temperature system, reinforced stirring system and chuck solid-liquid separation system by circulation and is constituted, circulation is bathed constant temperature system and is connected as a single entity by chuck layer 6 and chuck solid-liquid separation system, and reinforced stirring system connects socket 3 by reinforced stirring system and is connected with the chuck solid-liquid separation system.
Circulation is bathed constant temperature system and is adopted circulating pump 12 to link to each other with constant temperature bath device 13 with chuck circulation fluid import 9 respectively by circulation fluid tube connector 16, and the outlet 5 of chuck circulation fluid links to each other with constant temperature bath device 13 by circulation fluid tube connector 16.Can operate temperature required setting constant temperature scope according to the constant temperature Solid-Liquid Separation, need not to consider that environmental factor such as cool ambient air changes the influence to the Solid-Liquid Separation operation.
In the reinforced stirring system, the charge door 1 and shaft socket 2 one of band ground, shaft 15 is clamped in the shaft socket 2, and electric blender 14 is installed in shaft 15 upper ends, and shaft 15 lower ends are equipped with paddle 11.When separating relatively large supersaturated solution or separate the big material of viscosity, stir, can impel mixture to reach fully and separate.Adopt the charge door and the mechanical agitator interface one of band ground, can be applicable to the operation slightly in enormous quantities in the pilot scale, can carry out the limit and separate, stir on the limit, the continous way lock out operation that the limit is reinforced.
Bottom in the chuck solid-liquid separation system is equipped with glass core filter plate 10, has overcome Buchner funnel replacing filter paper inconvenience and the aggressive solvent defective to the filter paper influence, and the clean glass core of drip washing filter plate 10 after only needing to use is promptly reusable; The chuck circulation fluid outlet 5 of chuck layer 6 is higher than chuck circulation fluid import 9, can guarantee good constant temperature effect; The exit is provided with outlet valve 7 under the chuck solid-liquid separation system, and the bottom of valve is provided with discharging socket 8, and convenient the connection is subjected to liquid container, in time migrates out separating liquid.
Description of drawings
Accompanying drawing is a structural representation of the present utility model.Among the figure: 1, charge door, 2, the shaft socket, 3, reinforced stirring system connects socket, 4, the last end interface of chuck solid-liquid separation system, 5, chuck circulation fluid outlet, 6, the chuck layer, 7, the outlet valve of chuck solid-liquid separation system, 8, the discharging socket of chuck solid-liquid separation system, 9, the import of chuck circulation fluid, 10, glass core filter plate, 11, paddle, 12, circulating pump, 13, constant temperature bath device, 14, electric blender, 15, shaft, 16, the circulation fluid tube connector.
The specific embodiment
Below in conjunction with apparatus structure, embodiment and accompanying drawing the utility model is further described.
This device is mainly bathed constant temperature system, reinforced stirring system and chuck solid-liquid separation system by circulation and is constituted, circulation is bathed constant temperature system and is connected as a single entity by chuck layer 6 and chuck solid-liquid separation system, and reinforced stirring system connects socket 3 by reinforced stirring system and is connected with the chuck solid-liquid separation system.
Circulation is bathed constant temperature system and is adopted circulating pump 12 to link to each other with constant temperature bath device 13 with chuck circulation fluid import 9 respectively by circulation fluid tube connector 16, and the outlet 5 of chuck circulation fluid links to each other with constant temperature bath device 13 by circulation fluid tube connector 16.Can operate temperature required setting constant temperature scope according to the constant temperature Solid-Liquid Separation, need not to consider that environmental factor such as cool ambient air changes the influence to the Solid-Liquid Separation operation.
In the reinforced stirring system, the charge door 1 and shaft socket 2 one of band ground, shaft 15 is clamped in the shaft socket 2, and electric blender 14 is installed in shaft 15 upper ends, and shaft 15 lower ends are equipped with paddle 11.When separating relatively large supersaturated solution or separate the big material of viscosity, stir, can impel mixture to reach fully and separate.Adopt the charge door and the mechanical agitator interface one of band ground, can be applicable to the operation slightly in enormous quantities in the pilot scale, can carry out the limit and separate, stir on the limit, the continous way lock out operation that the limit is reinforced.
Bottom in the chuck solid-liquid separation system is equipped with glass core filter plate 10, has overcome Buchner funnel replacing filter paper inconvenience and the aggressive solvent defective to the filter paper influence, and the clean glass core of drip washing filter plate 10 after only needing to use is promptly reusable; The chuck circulation fluid outlet 5 of chuck layer 6 is higher than chuck circulation fluid import 9, can guarantee good constant temperature effect; The exit is provided with outlet valve 7 under the chuck solid-liquid separation system, and the bottom of valve is provided with discharging socket 8, and convenient the connection is subjected to liquid container, in time migrates out separating liquid.
This device is applied to the separation of mixture.
Hot water circulating pump is opened in the insulation of employing thermostat water bath, required constant temperature scope is set, circulator bath constant temperature on the thermostat water bath electronic relay.Add the hot supersaturated solution of mixture from charge door, stir, when the temperature of mixture is consistent with the jacket water (J.W.) bath temperature, on the discharging socket of chuck equipment for separating liquid from solid, connect there-necked flask, open the outlet valve of chuck equipment for separating liquid from solid, start vavuum pump, there-necked flask is vacuumized the constant temperature suction filtration.On the glass core filter plate is the indissoluble thing, is lyotrope solution in the there-necked flask, thereby reaches the purpose of separation.
This device is applied to the low temperature crystallization of product.
Adopt the freezing bath fireless cooker of constant temperature, open freezing bath circulating pump, on the freezing bath fireless cooker of constant temperature electronic relay required constant temperature scope is set, circulating frozen is bathed constant temperature.Add the solution of room temperature from charge door, slowly stir, when crystal is separated out fully, on the discharging socket of chuck equipment for separating liquid from solid, connect there-necked flask, open the outlet valve of chuck equipment for separating liquid from solid, start vavuum pump, there-necked flask is vacuumized the constant temperature suction filtration.On the glass core filter plate is the low temperature crystallization product, is crystalline mother solution in the there-necked flask, thereby reaches the purpose of separation.
Claims (5)
1, a kind of portable constant temperature equipment for separating liquid from solid, mainly bathing constant temperature system, reinforced stirring system and chuck solid-liquid separation system by circulation constitutes, it is characterized in that circulation bath constant temperature system is connected as a single entity by chuck layer (6) and chuck solid-liquid separation system, reinforced stirring system is connected with the chuck solid-liquid separation system by reinforced stirring system connection socket (3).
2, portable constant temperature equipment for separating liquid from solid according to claim 1 is characterized in that glass core filter plate (10) is installed in the bottom in the chuck solid-liquid separation system, and the chuck circulation fluid outlet (5) of chuck layer (6) is higher than chuck circulation fluid import (9).
3, portable constant temperature equipment for separating liquid from solid according to claim 1 is characterized in that outlet is provided with outlet valve (7) under the chuck Solid-Liquid Separation system, and the bottom of valve is provided with discharging socket (8).
4, portable constant temperature equipment for separating liquid from solid according to claim 1, the circulating pump (12) of bathing in the constant temperature system that it is characterized in that circulating links to each other with constant temperature bath device (13) with chuck circulation fluid import (9) respectively by circulation fluid tube connector (16), and chuck circulation fluid outlet (5) links to each other with constant temperature bath device (13) by circulation fluid tube connector (16).
5, portable constant temperature equipment for separating liquid from solid according to claim 1, the charge door (1) and shaft socket (2) one that it is characterized in that band ground in the reinforced stirring system, shaft (15) is clamped in the shaft socket (2), electric blender (14) is installed in shaft (15) upper end, and shaft (15) lower end is equipped with paddle (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200520098698 CN2841122Y (en) | 2005-11-10 | 2005-11-10 | Portable constant-temperature solid-liquid separating device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200520098698 CN2841122Y (en) | 2005-11-10 | 2005-11-10 | Portable constant-temperature solid-liquid separating device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2841122Y true CN2841122Y (en) | 2006-11-29 |
Family
ID=37445024
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200520098698 Expired - Fee Related CN2841122Y (en) | 2005-11-10 | 2005-11-10 | Portable constant-temperature solid-liquid separating device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2841122Y (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104225991A (en) * | 2014-09-06 | 2014-12-24 | 陈巧琴 | Circulation type portable filter |
| CN107881102A (en) * | 2017-11-23 | 2018-04-06 | 希施生物科技（上海）有限公司 | One kind is used for nucleic acid DNA/RNA type of production automatic synthesizers |
| CN110585749A (en) * | 2019-08-26 | 2019-12-20 | 浙江工业大学 | Device and method for separating viscous solid-liquid mixture |
-
2005
- 2005-11-10 CN CN 200520098698 patent/CN2841122Y/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104225991A (en) * | 2014-09-06 | 2014-12-24 | 陈巧琴 | Circulation type portable filter |
| CN107881102A (en) * | 2017-11-23 | 2018-04-06 | 希施生物科技（上海）有限公司 | One kind is used for nucleic acid DNA/RNA type of production automatic synthesizers |
| CN107881102B (en) * | 2017-11-23 | 2021-04-09 | 希施生物科技（上海）有限公司 | Automatic synthesizer for nucleic acid DNA/RNA production |
| CN110585749A (en) * | 2019-08-26 | 2019-12-20 | 浙江工业大学 | Device and method for separating viscous solid-liquid mixture |
| CN110585749B (en) * | 2019-08-26 | 2022-04-19 | 浙江工业大学 | Device and method for separating viscous solid-liquid mixture |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20061129 Termination date: 20091210 |