CN208320052U - A kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones - Google Patents
A kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones Download PDFInfo
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- CN208320052U CN208320052U CN201820683539.5U CN201820683539U CN208320052U CN 208320052 U CN208320052 U CN 208320052U CN 201820683539 U CN201820683539 U CN 201820683539U CN 208320052 U CN208320052 U CN 208320052U
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- reaction kettle
- flavones
- purifying
- kettle
- purification
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Abstract
The utility model discloses a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones, including control cabinet, column, reaction kettle and centrifugation motor, the column side is provided with the control cabinet, the reaction kettle is provided on the column, the reactor bottom is provided with retarder, the retarder is provided with the centrifugation motor far from the side of the reaction kettle, and the reaction kettle side is provided with heater box, and the reaction kettle is provided with waste material clean-up port far from the side of the heater box.Beneficial effect is: the utility model can realize the automatic flavones purification to Akebia trifoliate koiaz Peels, refining effect is preferable, purification efficiency is higher, and is provided with display screen, can remind the operation of operator's next step in time, to operator without technical requirements, the purifying tomography devices of the flavones are reasonable in design, and the degree of automation is higher, greatly improve the purification efficiency of flavones, improve the purification precision of flavones, economy with higher.
Description
Technical field
The utility model relates to flavones technical field of purification, and in particular to a kind of purifying for Akebia trifoliate koiaz Peels flavones
Tomography devices.
Background technique
Made of flavones refers to that two phenyl ring (A- and B- ring) with phenolic hydroxyl group are interconnected by central thricarbon atom
A series of compounds, basic parent nucleus are 2- phenyl chromone.Natural flavonoid compound exists mostly in the form of glycoside, and by
Various flavonoid glycoside can be formed in type, quantity, coupled position and the connecting mode difference of sugar.Form the sugar of flavonoid glycoside
Class includes monosaccharide and disaccharide, trisaccharide and acylated sugar.Flavonoid glycoside solid is amorphous powder, remaining flavone compound is mostly to crystallize
Property solid.The different color of flavone compound is that natural pigment family is added to more multicolour.This is because shape in its parent nucleus
At intersection conjugated system, and by electronics transfer, rearrangement, make to be conjugated chain elongation, thus shows color.Flavonoid glycoside is generally readily soluble
In the strong solvent of Yu Shui, ethyl alcohol, methanol isopolarity, but it is insoluble in or does not dissolve in the organic solvents such as benzene, chloroform.In recent years, city
It has had already appeared on about Akebia trifoliate koiaz Peels flavones equipment for purifying, but structure is complicated mostly for these equipment, automates journey
Degree is not high, and purification efficiency is lower, and purification precision is not high, is unable to satisfy the demand of existing market.
Utility model content
The purpose of this utility model is that solve the above-mentioned problems and provides a kind of for Akebia trifoliate koiaz Peels flavones
Purifying tomography devices.
The utility model achieves the above object through the following technical schemes:
A kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones, including control cabinet, column, reaction kettle and centrifugation electricity
Machine, the column side are provided with the control cabinet, and the reaction kettle, the reactor bottom setting are provided on the column
There is retarder, the retarder is provided with the centrifugation motor, the reaction kettle side setting far from the side of the reaction kettle
There is heater box, the reaction kettle is provided with waste material clean-up port far from the side of the heater box, and waste material clean-up port side is set
It is equipped with drain pipe one, the reaction kettle is provided with crush box far from the side of the column, and the crush box side is provided with powder
Broken motor, transmission belt is provided on the crushing motor, and the transmission belt is provided with belt far from described one end for crushing motor
It takes turns, is provided with feed opening on the crush box, the crush box side is provided with cylinder, and the cylinder is far from the crush box
Side is provided with support frame, and purification kettle is provided on support frame as described above, and membrane separator, the film point are provided on the purification kettle
The side of the purification kettle is provided with drawing liquid case from device, perfusion tube, drawing liquid case side are provided on the drawing liquid case
It is provided with purification filling opening, the purification kettle side is provided with incubator, and the purification bottom portion is provided with drain pipe two, described
It is provided with reaction filling opening at the top of reaction kettle, filter plate is provided in the reaction kettle, is provided with guide pad on the filter plate,
Display screen is provided on the control cabinet, the display screen side is provided with control button.
In above structure, equipment power supply is connected, starts the control button on the control cabinet, the crushing motor is opened
Akebia trifoliate koiaz Peels are added by the feed opening in beginning work, and Akebia trifoliate koiaz Peels are laggard by the crushing of the crush box
Enter to the reaction kettle, after the crush box completion of processing, the crushing motor stops working, and at this moment, the display screen is opened
Begin prompt liquid feeding, and suitable hydrochloric ethanol solution is added by the reaction filling opening, starts the control button herein,
The heater box is started to work, and is heated to the liquid in crush box, is started to keep the temperature when being heated to certain temperature, work as heat preservation
To the stipulated time, the cylinder is started to work, and the filter plate is driven to be filtered, and the display screen display cleaning passes through institute
It states waste material clean-up port and waste material is cleaned out into the reaction kettle, suitable sodium hydroxide solution is added by the reaction filling opening,
Start the control button herein, the centrifugation motor is started to work, by the retarder to the liquid in the reaction kettle
Start to stir, when stirring the stipulated time, the centrifugation motor stops working, start to staticly settle, when reaching the stipulated time,
The drawing liquid case is started to work, and is extracted out the supernatant in the reaction kettle by the perfusion tube, supernatant passes through the film
The purification kettle is entered after separator filtering, the incubator is started to work, and the temperature control in the purification kettle is being advised
Determine range, when supernatant is extracted out from the reaction kettle completely, the heater box stops working, the display screen display cleaning,
Clear water successively is added by the purification filling opening to be washed, after addition ethanol solution is cleaned, the incubator continues
It is heated, flavones starts to be crystallized, and after crystallization, takes out flavones crystallization and is dried.
In order to further increase the effect of flavones purifying chromatography, the control cabinet is connect by screw with the column, institute
Column is stated to connect by bolt with the reaction kettle.
In order to further increase the effect of flavones purifying chromatography, the retarder is connect by bolt with the reaction kettle,
The centrifugation motor is connect by bolt with the retarder.
In order to further increase the effect of flavones purifying chromatography, the heater box is connect by bolt with the reaction kettle.
In order to further increase the effect of flavones purifying chromatography, the crush box is connect by bolt with the reaction kettle.
In order to further increase the effect of flavones purifying chromatography, the cylinder is connect by bolt with the reaction kettle, institute
Support frame is stated to connect by screw with the reaction kettle.
In order to further increase the effect of flavones purifying chromatography, the purification kettle is connect by screw with support frame as described above.
Beneficial effect is: the utility model can realize to the purification of the automatic flavones of Akebia trifoliate koiaz Peels, refining effect compared with
Good, purification efficiency is higher, and is provided with display screen, can remind the operation of operator's next step in time, to operator without
The purifying tomography devices of technical requirements, the flavones are reasonable in design, and the degree of automation is higher, greatly improve mentioning for flavones
Pure efficiency improves the purification precision of flavones, economy with higher.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
Some embodiments of the utility model, for those of ordinary skill in the art, in the premise of not making the creative labor property
Under, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is a kind of structural representation of purifying tomography devices for Akebia trifoliate koiaz Peels flavones described in the utility model
Figure；
Fig. 2 is a kind of filter plate structure of purifying tomography devices for Akebia trifoliate koiaz Peels flavones described in the utility model
Schematic diagram；
Fig. 3 is a kind of control box structure of purifying tomography devices for Akebia trifoliate koiaz Peels flavones described in the utility model
Schematic diagram.
The reference numerals are as follows:
1, control cabinet；2, column；3, reaction kettle；4, it is centrifuged motor；5, retarder；6, heater box；7, crush box；8, it crushes
Motor；9, transmission belt；10, belt pulley；11, feed opening；12, cylinder；13, support frame；14, kettle is purified；15, membrane separator；16,
Drawing liquid case；17, perfusion tube；18, filling opening is purified；19, incubator；20, drain pipe two；21, filling opening is reacted；22, waste material is clear
Manage mouth；23, drain pipe one；24, guide pad；25, filter plate；26, display screen；27, control button.
Specific embodiment
The utility model is described in further detail with reference to the accompanying drawing:
As shown in Figure 1-Figure 3, a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones, including control cabinet 1, column
2, reaction kettle 3 and centrifugation motor 4,2 side of column is provided with control cabinet 1, reaction kettle 3,3 bottom of reaction kettle is provided on column 2
It is provided with retarder 5, retarder 5 is provided with centrifugation motor 4 far from the side of reaction kettle 3, and 3 side of reaction kettle is provided with heater box
6, reaction kettle 3 is provided with waste material clean-up port 22 far from the side of heater box 6, and 22 side of waste material clean-up port is provided with drain pipe one
23, reaction kettle 3 is provided with crush box 7 far from the side of column 2, and 7 side of crush box, which is provided with, crushes motor 8, crushes on motor 8
It is provided with transmission belt 9, transmission belt 9 is provided with belt pulley 10 far from the one end for crushing motor 8, is provided with feed opening on crush box 7
11,7 side of crush box is provided with cylinder 12, and cylinder 12 is provided with support frame 13 far from the side of crush box 7, sets on support frame 13
It is equipped with purification kettle 14, purifies and is provided with membrane separator 15 on kettle 14, membrane separator 15 is provided with pumping far from the side of purification kettle 14
Liquid case 16 is provided with perfusion tube 17 on drawing liquid case 16, and 16 side of drawing liquid case is provided with purification filling opening 18, and purification 14 side of kettle is set
It is equipped with incubator 19, purification 14 bottom of kettle is provided with drain pipe 2 20, and reaction filling opening 21, reaction are provided at the top of reaction kettle 3
It is provided with filter plate 25 in kettle 3, guide pad 24 is provided on filter plate 25, display screen 26, display screen 26 are provided on control cabinet 1
Side is provided with control button 27.
In above structure, equipment power supply is connected, starts the control button 27 on control cabinet 1, motor 8 is crushed and starts to work,
Akebia trifoliate koiaz Peels are added by feed opening 11, Akebia trifoliate koiaz Peels are entering reaction kettle 3 after the crushing of crush box 7,
It after 7 completion of processing of crush box, crushes motor 8 and stops working, at this moment, display screen 26 starts to prompt liquid feeding, by reacting liquid feeding
Suitable hydrochloric ethanol solutions are added in mouth 21, start control button 27 herein, heater box 6 is started to work, in crush box 7
Liquid heated, start to keep the temperature when being heated to certain temperature, when heat preservation is to the stipulated time, cylinder 12 is started to work, band
Dynamic filter plate 25 is filtered, and waste material is cleaned out reaction kettle 3 by waste material clean-up port 22, passed through by the display cleaning of display screen 26
Suitable sodium hydroxide solution is added in reaction filling opening 21, starts control button 27 herein, and centrifugation motor 4 is started to work, passed through
Retarder 5 starts to stir to the liquid in reaction kettle 3, and when stirring the stipulated time, centrifugation motor 4 stops working, and starts to stand
Precipitating, when reaching the stipulated time, drawing liquid case 16 is started to work, and is extracted out the supernatant in reaction kettle 3 by perfusion tube 17, on
Clear liquid enters purification kettle 14 after filtering by membrane separator 15, incubator 19 is started to work, and makes to purify the temperature control in kettle 14
System is in prescribed limit, and when supernatant is extracted out from reaction kettle 3 completely, heater box 6 stops working, the display cleaning of display screen 26, first
Clear water is added by purification filling opening 18 afterwards to be washed, after addition ethanol solution is cleaned, incubator 19 continues to add
Heat, flavones starts to be crystallized, and after crystallization, takes out flavones crystallization and is dried.
In order to further increase the effect of flavones purifying chromatography, control cabinet 1 is connect by screw with column 2, and column 2 passes through
Bolt is connect with reaction kettle 3, and retarder 5 is connect by bolt with reaction kettle 3, and centrifugation motor 4 is connected by bolt and retarder 5
Connect, heater box 6 connect by bolt with reaction kettle 3, and crush box 7 is connect by bolt with reaction kettle 3, cylinder 12 pass through bolt and
Reaction kettle 3 connects, and support frame 13 is connect by screw with reaction kettle 3, and purification kettle 14 is connect by screw with support frame 13.
The basic principles and main features and advantage of the utility model have been shown and described above.The technical staff of the industry
It should be appreciated that the present utility model is not limited to the above embodiments, the above embodiments and description only describe this
The principle of utility model, on the premise of not departing from the spirit and scope of the utility model, the utility model also has various change
And improvement, these various changes and improvements fall within the scope of the claimed invention.
Claims (7)
1. a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones, it is characterised in that: including control cabinet (1), column
(2), reaction kettle (3) and centrifugation motor (4), column (2) side is provided with the control cabinet (1), sets on the column (2)
It is equipped with the reaction kettle (3), reaction kettle (3) bottom is provided with retarder (5), and the retarder (5) is far from the reaction
The side of kettle (3) is provided with the centrifugation motor (4), and reaction kettle (3) side is provided with heater box (6), the reaction kettle
(3) side far from the heater box (6) is provided with waste material clean-up port (22), and waste material clean-up port (22) side is provided with row
Liquid pipe one (23), the reaction kettle (3) are provided with crush box (7) far from the side of the column (2), the crush box (7) one
Side, which is provided with, crushes motor (8), is provided with transmission belt (9) on the crushing motor (8), the transmission belt (9) is far from the powder
One end of broken motor (8) is provided with belt pulley (10), is provided with feed opening (11) on the crush box (7), the crush box (7)
Side is provided with cylinder (12), and the cylinder (12) is provided with support frame (13), the branch far from the side of the crush box (7)
It is provided with purification kettle (14) on support (13), is provided with membrane separator (15), the membrane separator on the purification kettle (14)
(15) side far from purification kettle (14) is provided with drawing liquid case (16), is provided with perfusion tube on the drawing liquid case (16)
(17), drawing liquid case (16) side is provided with purification filling opening (18), and purification kettle (14) side is provided with incubator
(19), purification kettle (14) bottom is provided with drain pipe two (20), is provided with reaction filling opening at the top of the reaction kettle (3)
(21), it is provided with filter plate (25) in the reaction kettle (3), is provided with guide pad (24), the control on the filter plate (25)
It is provided with display screen (26) on case (1) processed, display screen (26) side is provided with control button (27).
2. a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones according to claim 1, it is characterised in that: institute
It states control cabinet (1) to connect by screw with the column (2), the column (2) is connect by bolt with the reaction kettle (3).
3. a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones according to claim 1, it is characterised in that: institute
It states retarder (5) to connect by bolt with the reaction kettle (3), the centrifugation motor (4) passes through bolt and the retarder (5)
Connection.
4. a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones according to claim 1, it is characterised in that: institute
Heater box (6) are stated to connect by bolt with the reaction kettle (3).
5. a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones according to claim 1, it is characterised in that: institute
Crush box (7) are stated to connect by bolt with the reaction kettle (3).
6. a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones according to claim 1, it is characterised in that: institute
It states cylinder (12) to connect by bolt with the reaction kettle (3), support frame as described above (13) is connected by screw and the reaction kettle (3)
It connects.
7. a kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones according to claim 1, it is characterised in that: institute
Purification kettle (14) is stated to connect by screw with support frame as described above (13).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820683539.5U CN208320052U (en) | 2018-05-09 | 2018-05-09 | A kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820683539.5U CN208320052U (en) | 2018-05-09 | 2018-05-09 | A kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones |
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| Publication Number | Publication Date |
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| CN208320052U true CN208320052U (en) | 2019-01-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201820683539.5U Expired - Fee Related CN208320052U (en) | 2018-05-09 | 2018-05-09 | A kind of purifying tomography devices for Akebia trifoliate koiaz Peels flavones |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109621483A (en) * | 2019-01-23 | 2019-04-16 | 云南广福药业有限公司 | It is a kind of for extracting the device of Caulis Kadsurae |
-
2018
- 2018-05-09 CN CN201820683539.5U patent/CN208320052U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109621483A (en) * | 2019-01-23 | 2019-04-16 | 云南广福药业有限公司 | It is a kind of for extracting the device of Caulis Kadsurae |
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| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190104 Termination date: 20190509 |
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| CF01 | Termination of patent right due to non-payment of annual fee |