CN219849542U - Methane disulfonic acid methylene ester refining equipment - Google Patents
Methane disulfonic acid methylene ester refining equipment Download PDFInfo
- Publication number
- CN219849542U CN219849542U CN202320835106.8U CN202320835106U CN219849542U CN 219849542 U CN219849542 U CN 219849542U CN 202320835106 U CN202320835106 U CN 202320835106U CN 219849542 U CN219849542 U CN 219849542U
- Authority
- CN
- China
- Prior art keywords
- filter
- box
- pipe
- suction filtration
- drying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- GWAOOGWHPITOEY-UHFFFAOYSA-N 1,5,2,4-dioxadithiane 2,2,4,4-tetraoxide Chemical compound O=S1(=O)CS(=O)(=O)OCO1 GWAOOGWHPITOEY-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 238000007670 refining Methods 0.000 title claims abstract description 23
- 238000005406 washing Methods 0.000 claims abstract description 44
- 238000000967 suction filtration Methods 0.000 claims description 32
- 238000001035 drying Methods 0.000 claims description 30
- 238000001914 filtration Methods 0.000 claims description 21
- 239000011521 glass Substances 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 239000002351 wastewater Substances 0.000 claims description 4
- 239000012535 impurity Substances 0.000 abstract description 5
- 239000000126 substance Substances 0.000 abstract description 4
- 239000000047 product Substances 0.000 description 25
- 238000000746 purification Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- AHIWWUJXDLMOKI-UHFFFAOYSA-N methoxysulfonylmethanesulfonic acid Chemical compound COS(=O)(=O)CS(O)(=O)=O AHIWWUJXDLMOKI-UHFFFAOYSA-N 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- 239000002904 solvent Substances 0.000 description 3
- 239000012043 crude product Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000001291 vacuum drying Methods 0.000 description 2
- FGRBYDKOBBBPOI-UHFFFAOYSA-N 10,10-dioxo-2-[4-(N-phenylanilino)phenyl]thioxanthen-9-one Chemical compound O=C1c2ccccc2S(=O)(=O)c2ccc(cc12)-c1ccc(cc1)N(c1ccccc1)c1ccccc1 FGRBYDKOBBBPOI-UHFFFAOYSA-N 0.000 description 1
- TVEXGJYMHHTVKP-UHFFFAOYSA-N 6-oxabicyclo[3.2.1]oct-3-en-7-one Chemical compound C1C2C(=O)OC1C=CC2 TVEXGJYMHHTVKP-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 208000032839 leukemia Diseases 0.000 description 1
- 239000000825 pharmaceutical preparation Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a methylene methane disulfonate refining device in the field of chemical refining and purifying, which comprises a filter washing box, wherein the filter washing box is used for refining and purifying methylene methane disulfonate, a filter pipe is screwed on one side surface of the filter washing box, a suction filter pipe is screwed on the other side surface of the filter washing box, the filter washing box is arranged to filter and wash a product, impurities doped in the product are removed, so that the purity of the product is improved, the purity of the product meets various requirements, the product can be guided into the filter washing box through the filter pipe, the product can be filtered and washed in the filter washing box, and then guided into the next device through the suction filter pipe, so that the next purifying and refining work can be performed, and the filter pipe and the suction filter pipe are screwed on the surface, so that the circulation of substances in the pipeline can be controlled through the valve.
Description
Technical Field
The utility model relates to the field of chemical refining and purification, in particular to methylene methane disulfonate refining equipment.
Background
Methylene methane disulfonate is a chemical substance with white or white-like crystal or crystalline powder in appearance, and can be used for synthesizing pharmaceutical preparations for treating leukemia and the like in animals.
The existing preparation method of the methane disulfonic acid methylene ester has many defects, the product obtained by the existing method for preparing the methane disulfonic acid methylene ester has poor color, many impurities and low purity, and resource waste is caused.
Therefore, we propose a methylene methane disulfonate refining apparatus.
Disclosure of Invention
The utility model aims to provide methane disulfonic acid methylene ester refining equipment for solving the problems in the background technology.
In order to achieve the above purpose, the present utility model provides the following technical solutions:
the utility model provides a methane disulfonic acid methylene ester refining plant, includes filtration washing case, its characterized in that: the surface of the filtering and washing box is fixedly provided with a transparent glass observation window, and the filtering and washing box is used for refining and purifying the methane disulfonic acid methylene.
Preferably, the filter pipe is screwed on one side surface of the filter washing box, and the suction filtration pipe is screwed on the other side surface of the filter washing box.
Preferably, one end of the filter pipe is connected with the reaction bin in a threaded manner and extends to the inside of the reaction bin, the filter pipe is used for communicating the reaction bin with the filtering washing box, and the foot pad is fixedly arranged at the lower end of the reaction bin.
Preferably, a feeding hole is formed in one side surface of the reaction bin, a water outlet is formed in the other side surface of the reaction bin, and the water outlet is used for outflow of wastewater generated by reaction.
Preferably, one end of the suction filtration pipe is in threaded connection with the suction filtration box and extends to the inside of the suction filtration box, and one side surface of the suction filtration box is in threaded connection with a return pipe.
Preferably, the surface threaded connection of suction filtration case one side has the drying tube, drying tube one end threaded connection has the drying cabinet, the drying tube all runs through the suction filtration case with the drying cabinet extends to its inside, drying cabinet one side surface hinge connection has the equipment door, equipment door surface fixed mounting has the handle.
Compared with the prior art, the utility model has the beneficial effects that:
1. according to the utility model, the filtering and washing box is arranged to filter and wash the product, so that impurities doped in the product are removed, the purity of the product is improved, and the purity of the product meets various requirements.
2. According to the utility model, the crude product of the methane disulfonic acid methylene ester can be generated through the arranged reaction bin, the poor solvent of the methane disulfonic acid methylene ester is arranged in the reaction bin, so that the methane disulfonic acid methylene ester is separated out, the separated methane disulfonic acid methylene ester is guided into the filter washing box through the arranged filter pipe, thus the filter washing work is carried out, the inside of the filter washing box can be observed through the arranged transparent glass observation window, the normal operation of the filter washing work is ensured, the filtered and washed product can be subjected to suction filtration through the arranged suction filtration box, further purification is carried out, the waste after the suction filtration can be returned to the reaction bin through the arranged return pipe, the raw material loss is reduced, the product in the suction filtration box can be guided into the drying box through the arranged drying pipe, and the product can be subjected to vacuum drying through the arranged drying box, thereby the high-purity product is obtained.
Drawings
FIG. 1 is a schematic diagram of the overall structure of the present utility model;
FIG. 2 is a schematic front view of the overall structure of the present utility model;
FIG. 3 is a schematic side view of the overall structure of the present utility model;
FIG. 4 is a schematic top view of the overall structure of the present utility model;
in the figure: 1. a reaction bin; 2. a feeding hole; 3. a transparent glass viewing window; 4. a water outlet; 5. foot pads; 6. a filter tube; 7. a suction filtration tube; 8. a return pipe; 9. a drying tube; 10. a filtering washing box; 11. a suction filtration box; 12. a drying box; 13. an equipment door; 14. a handle.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1 to 4, in the embodiment of the utility model, a methylene methane disulfonate refining device comprises a filter and washing box 10, wherein a transparent glass observation window 3 is fixedly arranged on the surface of the filter and washing box 10, the filter and washing box 10 is used for refining and purifying the methylene methane disulfonate, and the filter and washing box 10 is arranged to filter and wash products and remove impurities doped in the products, so that the purity of the products is improved, the purity of the products meets various requirements, and the inside of the filter and washing box 10 can be observed through the arranged transparent glass observation window 3, so that the normal operation of the filter and washing is ensured.
Wherein, filter tube 6 is connected with to filter box 10 side surface screw thread spin, filter box 10 opposite side surface screw thread spin is connected with suction filtration pipe 7, can guide into filter box 10 with the result through the filter tube 6 that sets up to carry out the filtration washing work to the result, can guide into next equipment with the result that filters the washing in the filter box 10 through the suction filtration pipe 7 that sets up, thereby carry out the purification refining work of next step, filter tube 6 and suction filtration pipe 7 surface screw thread install the valve, can control the circulation of the material in the pipeline through the valve.
Wherein, filter tube 6 one end threaded connection has reaction storehouse 1 and extends to the inside of reaction storehouse 1, filter tube 6 is linked together reaction storehouse 1 and filtration washing case 10, and reaction storehouse 1 lower extreme fixed mounting has pad foot 5, can produce methane disulfonic acid methyl ester crude through the reaction storehouse 1 that sets up, and reaction storehouse 1 is inside to be provided with methane disulfonic acid methyl ester's poor solvent, thereby make methane disulfonic acid methyl ester precipitate, guide into filtration washing case 10 with the methane disulfonic acid methyl ester that will precipitate through filter tube 6 that sets up, thereby carry out filtration washing work, can play fixed support effect simultaneously with equipment keeping away from ground through pad foot 5 that sets up.
Wherein, feed hole 2 has been seted up on reaction storehouse 1 one side surface, and delivery port 4 has been seted up on reaction storehouse 1 opposite side surface, and delivery port 4 is used for the outflow of the produced waste water of reaction, thereby can throw into reaction storehouse 1 with the reaction material through the feed hole 2 that sets up, can collect the produced waste water of reaction after centralized processing, avoid polluting the environment through delivery port 4 that sets up.
Wherein, suction filtration pipe 7 one end threaded connection has suction filtration case 11 and extends to the inside of suction filtration case 11, and suction filtration case 11 one side surface threaded connection has back flow 8, can carry out the suction filtration through the product of filtering the washing through setting up suction filtration case 11, further purification, can flow back the waste material after the suction filtration to reaction storehouse 1 through the back flow 8 that sets up, reduced the raw materials loss for raw materials yield increases, and back flow 8 surface screw thread installs the valve, can control the circulation of the interior material of back flow 8 through the valve.
Wherein, suction box 11 one side surface threaded connection has drying tube 9, drying tube 9 one end threaded connection has drying cabinet 12, drying tube 9 all runs through suction box 11 and drying cabinet 12 and extends to its inside, drying cabinet 12 one side surface hinged connection has equipment door 13, equipment door 13 surface fixed mounting has handle 14, can carry out the vacuum drying to the product in the suction box 11 through the drying cabinet 12 of setting, thereby obtain the high-purity product, can take out final high-purity product through equipment door 13 of setting, be more convenient for assist opening equipment door 13 through the handle 14 of setting, the valve is installed to drying tube 9 surface threaded simultaneously, can control the circulation of the interior material of drying tube 9 through the valve.
The working principle of the utility model is as follows: in the use process of methane disulfonic acid methylene ester refining equipment, the reaction bin arranged can generate methane disulfonic acid methylene ester crude product, the reaction bin is internally provided with poor solvent of methane disulfonic acid methylene ester, thereby the methane disulfonic acid methylene ester is separated out, the separated methane disulfonic acid methylene ester is guided into a filtering and washing box through a set filter pipe, thereby filtering and washing work is carried out, the filtering and washing box is arranged to filter and wash products, impurities doped in the products are removed, thereby the purity of the products is improved, the purity of the products meets various requirements, the inside of the filtering and washing box can be observed through a set transparent glass observation window, the normal operation of the filtering and washing work is ensured, the products subjected to filtering and washing can be subjected to suction filtration through the set suction filtration box, further purification is carried out, the waste subjected to suction filtration can be refluxed to the reaction bin through the set reflux pipe, the raw material loss is reduced, the products in the suction filtration box can be guided into a drying box through a set drying pipe, and the products can be dried in vacuum through the set drying box, thereby the products with high purity are obtained.
The present utility model is not limited to the above-mentioned embodiments, and any person skilled in the art, based on the technical solution of the present utility model and the inventive concept thereof, can be replaced or changed within the scope of the present utility model.
Claims (6)
1. The utility model provides a methane disulfonic acid methylene ester refining plant, includes filtration washing case (10), its characterized in that: the surface of the filtering and washing box (10) is fixedly provided with a transparent glass observation window (3), and the filtering and washing box (10) is used for refining and purifying the methane disulfonic acid methylene ester.
2. A methylene methane disulfonate refining apparatus according to claim 1 wherein: the filter washing box is characterized in that a filter pipe (6) is connected to one side surface of the filter washing box (10) in a threaded screwing mode, and a suction filtration pipe (7) is connected to the other side surface of the filter washing box (10) in a threaded screwing mode.
3. A methylene methane disulfonate refining apparatus according to claim 2 wherein: one end of the filter pipe (6) is connected with the reaction bin (1) in a threaded manner and extends to the inside of the reaction bin (1), the filter pipe (6) is used for communicating the reaction bin (1) with the filtering and washing box (10), and the foot pad (5) is fixedly arranged at the lower end of the reaction bin (1).
4. A methylene methane disulfonate refining apparatus according to claim 3 wherein: the reaction bin (1) is characterized in that a feeding hole (2) is formed in one side surface of the reaction bin, a water outlet (4) is formed in the other side surface of the reaction bin (1), and the water outlet (4) is used for outflow of wastewater generated by reaction.
5. A methylene methane disulfonate refining apparatus according to claim 2 wherein: one end of the suction filtration pipe (7) is connected with a suction filtration box (11) in a threaded manner and extends to the inside of the suction filtration box (11), and a return pipe (8) is connected with one side surface of the suction filtration box (11) in a threaded manner.
6. A methylene methane disulfonate refining apparatus according to claim 5 wherein: the novel vacuum filter is characterized in that a drying pipe (9) is connected to one side surface of the suction filter box (11) in a threaded mode, one end of the drying pipe (9) is connected with a drying box (12) in a threaded mode, the drying pipe (9) penetrates through the suction filter box (11) and the drying box (12) and extends into the drying box, an equipment door (13) is connected to one side surface of the drying box (12) in a hinged mode, and a handle (14) is fixedly arranged on the surface of the equipment door (13).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320835106.8U CN219849542U (en) | 2023-04-14 | 2023-04-14 | Methane disulfonic acid methylene ester refining equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320835106.8U CN219849542U (en) | 2023-04-14 | 2023-04-14 | Methane disulfonic acid methylene ester refining equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219849542U true CN219849542U (en) | 2023-10-20 |
Family
ID=88336295
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320835106.8U Active CN219849542U (en) | 2023-04-14 | 2023-04-14 | Methane disulfonic acid methylene ester refining equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219849542U (en) |
-
2023
- 2023-04-14 CN CN202320835106.8U patent/CN219849542U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102755765B (en) | Deep-purification impurity-removing treatment device of tobacco extraction liquid and impurity removing control method thereof | |
| CN219849542U (en) | Methane disulfonic acid methylene ester refining equipment | |
| CN201161242Y (en) | Filtering cleaning machine | |
| CN112156523A (en) | Suction filtration device for preparing shaddock peel biological adsorbent and use method thereof | |
| CN108187400B (en) | Material filtering mechanism for chemical equipment | |
| CN207562887U (en) | A kind of esterifying kettle with liquid waste treating apparatus | |
| CN216427241U (en) | Peony seed oil refining equipment | |
| CN215276033U (en) | Automatic pressure filtrate recovery device of plate and frame filter press | |
| CN209917711U (en) | Paper pulp agitator with filtering capability | |
| CN108245986B (en) | A plasma adsorption and filtration device for production of blood coagulation factor class blood products | |
| CN208975278U (en) | A kind of Chinese medicine production peony seed oil filter device | |
| CN208387802U (en) | A kind of propolis equipment for purifying with purity determination device | |
| CN220224755U (en) | Paper pulp filtering device inside paper pulp tank | |
| CN219210560U (en) | Vinegar brewing device for raw material purification | |
| CN220460062U (en) | Multistage filtration's papermaking effluent treatment plant | |
| CN103922558A (en) | Sludge filtering machine | |
| CN203820615U (en) | Sludge filtering machine | |
| CN203075732U (en) | Automatic solid-liquid separation filter | |
| CN219355443U (en) | A filter edulcoration device for resin glue solution | |
| CN216799704U (en) | High-efficient compounding device is used in production of digital printing coating ink | |
| CN215271839U (en) | Water circulation device for vase | |
| CN219701288U (en) | Convenient calcium carbonate production, filtration, collection and transfer device | |
| CN216513736U (en) | Six-in-one oil expression all-in-one machine | |
| CN210206174U (en) | Separation equipment for separating acid sludge and glycerin in biodiesel | |
| CN213377664U (en) | Centrifugal filter is used in coating production |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |