CN2805996Y - Continuous preparation apparatus for high-purity gold nano-powder - Google Patents
Continuous preparation apparatus for high-purity gold nano-powder Download PDFInfo
- Publication number
- CN2805996Y CN2805996Y CN 200520013538 CN200520013538U CN2805996Y CN 2805996 Y CN2805996 Y CN 2805996Y CN 200520013538 CN200520013538 CN 200520013538 CN 200520013538 U CN200520013538 U CN 200520013538U CN 2805996 Y CN2805996 Y CN 2805996Y
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- China
- Prior art keywords
- tube
- swivel
- liquid level
- sodium hydroxide
- hydroxide solution
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- Expired - Fee Related
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Abstract
The utility model discloses a continuous preparation device for nano gold powder with high purity, which comprises a temperature controlled heating device. The utility model is characterized in that the temperature controlled heating device comprises a heating body which is provided with a heating through hole, and a spiral tube is arranged in the heating through hole. The inlet end of the spiral tube is connected with a loading hopper tube by a first rotary joint, and the outlet end of the spiral tube is connected with an unloading hopper tube by a second rotary joint. The first rotary joint is fixed on a supporting frame, and the second rotary joint is fixed on an electric machine transmission device. The first rotary joint is provided with a first sealing ring, and the second rotary joint is provided with a second sealing ring. The utility model has the advantages of convenient operation for filling raw material, serialized ingress and egress of power material, large output and high purity of prepared nano gold powder. The spiral tube can be driven by the electric machine transmission device to rotate endlessly, so as to ensure that power is fully and evenly stirred. The utility model can be used for continuously preparing nano gold powder with high purity, and can increase the yield of nano gold powder with high purity.
Description
Technical field
The utility model relates to a kind of process units that is used for preparing high-purity nano bronze body, especially relates to a kind of serialization process units of high-purity nano bronze body.
Background technology
Existing high-purity nano bronze body preparation method normally will prepare nano-Au solution in other container, after the drying, powder is tiled in the ceramic boat, puts into a quartz ampoule temperature control heating of bringing the gas outlet into again, and the gas that reaction is produced is handled.This method has limited the volume production of nano gold powder, and inconvenient operation also is difficult to prepare highly purified nano gold powder.
Summary of the invention
Technical problem to be solved in the utility model is the serialization process units that a kind of high-purity nano bronze body is provided at above-mentioned prior art present situation, can be used for preparing continuously high-purity nano bronze body, improves the output of high-purity nano bronze body.
The utility model solves the problems of the technologies described above the technical scheme that is adopted: a kind of serialization process units of high-purity nano bronze body, comprise a temperature control heating device, described temperature control heating device comprises a calandria, described calandria is provided with and adds heat through-hole, described adding, be provided with helix tube in the heat through-hole, the entrance point of described helix tube is connected with the loading hopper pipe by first swivel, the port of export of described helix tube is connected with the blowing filler tube by second swivel, described first swivel is fixed on the fixing support rack, described second swivel is fixed on the transmission gear for electric motor, described first swivel is provided with first sealing ring, and described second swivel is provided with second sealing ring.
Described first swivel comprises one first connection chamber, one end of described first connection chamber is provided with first hickey, the other end of described first connection chamber is provided with first rotary connector, described loading hopper pipe is screwed onto on described first hickey, described helix tube is rotatably connected on described first rotary connector, described first sealing ring radially is arranged between described helix tube and described first rotary connector, described second swivel comprises one second connection chamber, one end of described second connection chamber is provided with second hickey, the other end of described second connection chamber is provided with second rotary connector, described helix tube is screwed onto on described second hickey, described blowing filler tube is rotatably connected on described second rotary connector, and described second sealing ring radially is arranged between described blowing filler tube and described second rotary connector.
The leading section of described loading hopper pipe is first tapering part, the leading section of the entrance point of described helix tube is the first horn opening part, described first tapering part and described first horn opening partly are arranged in described first connection chamber, described first tapering part stretches into the described first horn opening part, the leading section of described blowing filler tube is the second horn opening part, the leading section of the port of export of described helix tube is second tapering part, described second tapering part and described second horn opening partly are arranged in described second connection chamber, and described second tapering part stretches into the described second horn opening part.
Described helix tube is outer can be wound with insulation material.
Can also be filled with insulation material along axis direction in the helical cavity of described helix tube.
Described blowing filler tube is connected with closed container by gas outlet tube, be loaded with sodium hydroxide solution in the described closed container, described gas outlet tube stretches under the liquid level of sodium hydroxide solution, described closed container is connected with open-top receptacle by plastic tube, be loaded with deionized water in the described open-top receptacle, the entrance point of described plastic tube is positioned at the liquid level top of sodium hydroxide solution, and the port of export of described plastic tube is positioned under the liquid level of deionized water.
Production process of the present utility model is such: 1. will prepare, levigate nano gold powder is put in the helix tube by the loading hopper pipe, driving helix tube with motor and swivel rotates, nano gold powder enters in the temperature control heating device in helical rotation, thermally equivalent reaction in hot environment, can guarantee the time of staying of nano gold powder in temperature control heating device by the control velocity of rotation and the helix tube number of turn, high-purity nano bronze body behind the purifying is emitted and is collected by the valve on the blowing filler tube, the gas that reaction produces enters in the air after then entering into closed container and open-top receptacle processing successively by gas outlet tube and plastic tube.
Compared with prior art, it is easy to operate that advantage of the present utility model is to load raw material, powder material turnover serialization, and output is big, the nano gold powder purity height that makes; Helix tube can constantly rotate under the drive of transmission gear for electric motor, can guarantee that powder stirs, and the helix tube material can adopt quartz or stainless steel casing liner enamel inner container; Outside helix tube, twine insulation material, and in the helical cavity of helix tube along the axis direction fill insulant material, it is stable to guarantee better that nano gold powder is heated evenly, insulation material then can adopt asbestos or other refractory material; Tapering part stretches into the horn opening part can make nano gold powder can not hindered on progress path; Enter in the atmosphere after the gas treatment that closed container and open containers can produce reaction, reduce air pollution.
Description of drawings
Fig. 1 is a structural representation of the present utility model;
Fig. 2 is the partial enlarged drawing of the utility model first swivel;
Fig. 3 is the partial enlarged drawing of the utility model second swivel.
The specific embodiment
Embodiment describes in further detail the utility model below in conjunction with accompanying drawing.
Embodiment one: a kind of serialization process units of high-purity nano bronze body, comprise a temperature control heating device (not shown), temperature control heating device comprises a calandria 1, calandria 1 is provided with and adds heat through-hole 101, add and be provided with helix tube 2 in the heat through-hole 101, the helix tube 2 outer insulation material (not shown)s that are wound with, the entrance point of helix tube 2 is connected with loading hopper pipe 4 by first swivel 3, first swivel 3 is fixed on the fixing support rack 7, first swivel 3 comprises one first connection chamber 31, one end of first connection chamber 31 is provided with first hickey 32, the other end of first connection chamber 31 is provided with first rotary connector 33, loading hopper pipe 4 is screwed onto on first hickey 32, helix tube 2 is rotatably connected on first rotary connector 33, radially be provided with first sealing ring 34 between the helix tube 2 and first rotary connector 33, the leading section of loading hopper pipe 4 is first tapering part 41, the leading section of the entrance point of helix tube 2 is the first horn opening part 21, first tapering part 41 and the first horn opening part 21 are arranged in first connection chamber 31, first tapering part 41 stretches into the first horn opening part 21, the port of export of helix tube 2 is connected with blowing filler tube 6 by second swivel 5, second swivel 5 is fixed on the transmission gear for electric motor 8, second swivel 5 comprises one second connection chamber 51, one end of second connection chamber 51 is provided with second hickey 52, the other end of second connection chamber 51 is provided with second rotary connector 53, helix tube 2 is screwed onto on second hickey 52, blowing filler tube 6 is rotatably connected on second rotary connector 53, radially be provided with second sealing ring 54 between the blowing filler tube 6 and second rotary connector 53, the leading section of blowing filler tube 6 is the second horn opening part 61, the leading section of the port of export of helix tube 2 is second tapering part 22, second tapering part 22 and the second horn opening part 61 are arranged in second connection chamber 51, second tapering part 22 stretches into the second horn opening part 61, the bottom of blowing filler tube 6 is provided with baiting valve 62, blowing filler tube 6 is connected with closed container 11 by gas outlet tube 10, be loaded with sodium hydroxide solution 12 in the closed container 11, gas outlet tube 10 stretches under the liquid level of sodium hydroxide solution 12, closed container 11 is connected with open-top receptacle 14 by plastic tube 13, be loaded with deionized water 15 in the open-top receptacle 14, the entrance point of plastic tube 13 is positioned at the liquid level top of sodium hydroxide solution 12, and the port of export of plastic tube 13 is positioned under the liquid level of deionized water 15.
Embodiment two: other structure is identical with embodiment one, and difference is to be filled with insulation material 9 along axis direction in the helical cavity of helix tube 2.
Claims (8)
1, a kind of serialization process units of high-purity nano bronze body, comprise a temperature control heating device, it is characterized in that described temperature control heating device comprises a calandria, described calandria is provided with and adds heat through-hole, described adding, be provided with helix tube in the heat through-hole, the entrance point of described helix tube is connected with the loading hopper pipe by first swivel, the port of export of described helix tube is connected with the blowing filler tube by second swivel, described first swivel is fixed on the fixing support rack, described second swivel is fixed on the transmission gear for electric motor, described first swivel is provided with first sealing ring, and described second swivel is provided with second sealing ring.
2, the serialization process units of a kind of high-purity nano bronze body as claimed in claim 1, it is characterized in that described first swivel comprises one first connection chamber, one end of described first connection chamber is provided with first hickey, the other end of described first connection chamber is provided with first rotary connector, described loading hopper pipe is screwed onto on described first hickey, described helix tube is rotatably connected on described first rotary connector, described first sealing ring radially is arranged between described helix tube and described first rotary connector, described second swivel comprises one second connection chamber, one end of described second connection chamber is provided with second hickey, the other end of described second connection chamber is provided with second rotary connector, described helix tube is screwed onto on described second hickey, described blowing filler tube is rotatably connected on described second rotary connector, and described second sealing ring radially is arranged between described blowing filler tube and described second rotary connector.
3, the serialization process units of a kind of high-purity nano bronze body as claimed in claim 2, the leading section that it is characterized in that described loading hopper pipe is first tapering part, the leading section of the entrance point of described helix tube is the first horn opening part, described first tapering part and described first horn opening partly are arranged in described first connection chamber, described first tapering part stretches into the described first horn opening part, the leading section of described blowing filler tube is the second horn opening part, the leading section of the port of export of described helix tube is second tapering part, described second tapering part and described second horn opening partly are arranged in described second connection chamber, and described second tapering part stretches into the described second horn opening part.
4,, it is characterized in that described helix tube is wound with insulation material outward as the serialization process units of claim 1 or 2 or 3 described a kind of high-purity nano bronze bodies.
5, the serialization process units of a kind of high-purity nano bronze body as claimed in claim 4 is characterized in that being filled with insulation material along axis direction in the helical cavity of described helix tube.
6, serialization process units as claim 1 or 2 or 3 described a kind of high-purity nano bronze bodies, it is characterized in that described blowing filler tube is connected with closed container by gas outlet tube, be loaded with sodium hydroxide solution in the described closed container, described gas outlet tube stretches under the liquid level of sodium hydroxide solution, described closed container is connected with open-top receptacle by plastic tube, be loaded with deionized water in the described open-top receptacle, the entrance point of described plastic tube is positioned at the liquid level top of sodium hydroxide solution, and the port of export of described plastic tube is positioned under the liquid level of deionized water.
7, the serialization process units of a kind of high-purity nano bronze body as claimed in claim 4, it is characterized in that described blowing filler tube is connected with closed container by gas outlet tube, be loaded with sodium hydroxide solution in the described closed container, described gas outlet tube stretches under the liquid level of sodium hydroxide solution, described closed container is connected with open-top receptacle by plastic tube, be loaded with deionized water in the described open-top receptacle, the entrance point of described plastic tube is positioned at the liquid level top of sodium hydroxide solution, and the port of export of described plastic tube is positioned under the liquid level of deionized water.
8, the serialization process units of a kind of high-purity nano bronze body as claimed in claim 5, it is characterized in that described blowing filler tube is connected with closed container by gas outlet tube, be loaded with sodium hydroxide solution in the described closed container, described gas outlet tube stretches under the liquid level of sodium hydroxide solution, described closed container is connected with open-top receptacle by plastic tube, be loaded with deionized water in the described open-top receptacle, the entrance point of described plastic tube is positioned at the liquid level top of sodium hydroxide solution, and the port of export of described plastic tube is positioned under the liquid level of deionized water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200520013538 CN2805996Y (en) | 2005-07-22 | 2005-07-22 | Continuous preparation apparatus for high-purity gold nano-powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200520013538 CN2805996Y (en) | 2005-07-22 | 2005-07-22 | Continuous preparation apparatus for high-purity gold nano-powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2805996Y true CN2805996Y (en) | 2006-08-16 |
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ID=36920299
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200520013538 Expired - Fee Related CN2805996Y (en) | 2005-07-22 | 2005-07-22 | Continuous preparation apparatus for high-purity gold nano-powder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2805996Y (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106735306A (en) * | 2017-01-22 | 2017-05-31 | 武汉璟泓万方堂医药科技股份有限公司 | A kind of continuous reaction unit for preparing collaurum |
| CN106795471A (en) * | 2014-10-27 | 2017-05-31 | 弗门尼舍有限公司 | The apparatus and method that product is hydrolyzed |
-
2005
- 2005-07-22 CN CN 200520013538 patent/CN2805996Y/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106795471A (en) * | 2014-10-27 | 2017-05-31 | 弗门尼舍有限公司 | The apparatus and method that product is hydrolyzed |
| CN106795471B (en) * | 2014-10-27 | 2021-04-06 | 弗门尼舍有限公司 | Apparatus and method for hydrolyzing products |
| CN106735306A (en) * | 2017-01-22 | 2017-05-31 | 武汉璟泓万方堂医药科技股份有限公司 | A kind of continuous reaction unit for preparing collaurum |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: SHANGHAI HUASHI NANO MATERIALS CO., LTD. Free format text: FORMER OWNER: HUANG DEHUAN Effective date: 20080606 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20080606 Address after: Block A, Xin Mei Industrial Zone, 260 Cao Cao Road, Shanghai, Minhang District, China: 201108 Patentee after: Shanghai Huashi Nano Material Co., Ltd. Address before: Room 13, No. 288, Lane 301, Macao Road, Shanghai, Putuo District, 200060 Patentee before: Huang Dehuan |
|
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20060816 Termination date: 20120722 |