CN2230617Y - Swinging high-pressure reactor - Google Patents

Abstract

The utility model discloses a swinging high pressure reactor. In the utility model, a reactor body (8) is installed on a supporting frame (1) and is supported by two supporting rods (9); a rotating shaft (6) which is installed on a belt pulley (5) in an eccentric way and a connecting rod (7) are driven via a motor; one end the connecting rod (7) is hinged with the rotating shaft (6), and the other end is hinged with a blind flange (10) on the top end of the reactor body (8); the reactor body (8) can be driven to swing up and down within the range of 10 to 80 DEG by taking the supporting rods as shafts, the swinging frequency is 10 to 60 times/min, and the action that reactant inside the swinging high pressure reactor can be mixed can be played. The swinging high pressure reactor can be used for various chemical reactions under the conditions that the room temperature is below 400DEG. C, and the ordinary pressure is 6.0 MPa. The utility model has the advantages that the structure of the equipment is simple, a rotating leakage point does not exist, and the temperature, the pressure, the swinging frequency, the mixing frequency, and the volume of the swinging high pressure reactor are all adjustable.

Description

The swing type autoclave

The utility model relates to stirring-type test autoclave, particularly relates to the autoclave that swings up and down the stirring reaction material with reactor.

The autoclave of transmission is a mechanical agitation type, or electromagnetism promotes stirring-type, easily produce in the course of the work to reveal and phenomenon such as stuck, and stirring efficiency is not high, and the volume of reactor immobilizes, and brings inconvenience to the user.

The purpose of this utility model provides a kind of simple in structure, and mixing effect is good, the small-sized swing type autoclave that easy operating uses.

Described autoclave is rack-mount, by an eccentric rotating shaft of adorning on motor and motor-driven reductor, belt pulley, the belt pulley, the hinged eccentrically weighted shaft of one end, the connecting rod of the hinged reactor end cap of one end flange drives, and making reactor serves as that axle swings up and down with the fulcrum on the support.Cause that by swing the material in the still mixes, the baffle plate fixing or activity that is installed in the still can further increase mixability.

This swing type autoclave number of oscillations 10-60 times/minutes, 10-80 ° of horizontal hunting angles, reaction kettle body is replaceable, its volume 300-5000ml.Reaction temperature is from room temperature to 400 ℃, withstand voltage 6.0 MPas.

This swing type autoclave has simple in structure, and nothing is rotated leakage point, and number of times is stirred in temperature, pressure, swing, reactor volume all can be regulated, and this reactor increases mixing of materials because the stirring that stops of swing stirring and Internal baffle is arranged, and benefit improves greatly.Through test, this reactor is increased the benefit 10-20 times than the autoclave of traditional approach, for the gas, liquid, solid phase reaction good result is arranged also.

The concrete structure of this swing type autoclave is provided by example and accompanying drawing:

Fig. 1 is the front view of this swing type autoclave.

Fig. 2 is the vertical view of this swing type autoclave.

Motor 2 is being fixed in figure medium-height trestle 1 bottom, its motor 2 drives decelerator 3 by shaft coupling, drive belt pulley 5 by belt 4, on the belt pulley 5 partially the center of belt pulley traditional thread binding rotating shaft 6, reaction kettle body 8 is installed on the support 1, the both sides of two cramp bar 9 supporting reactor kettlies 8, kettle 8 can cramp bar 9 be the axle rotation, one end of a connecting rod 7 is hinged on the eccentrically weighted shaft 6, one end is hinged on the end cap 10 of reactor kettle 8, drive decelerator 3 at motor 2, when driving belt pulley 5 and eccentrically weighted shaft 6 rotations, it is the loam cake end of drivening rod push-and-pull reaction kettle body 8 about in the of 7, making kettle serves as axle rotary oscillation up and down with cramp bar 9, and it is 10-60 times/minutes that the length of adjusting decelerator 3 and belt pulley 5 and connecting rod 7 makes the reaction kettle body number of oscillations, in 10-80 ° of scopes of the horizontal angle that swings up and down, perforated baffle 14 is housed, the mixed effect of still internal reaction material when swinging up and down in the reaction kettle body 8 to increase reactor 8.

The volume of reactor 8 can be 300ml-5000ml etc.The top is equiped with air inlet pipe 11, escape pipe 12, pressure-measuring pipe 13, also can establishes temperature tube.Reaction kettle body 8, and end cap, pipe 11,12,13 all make of stainless steel.

Claims (4)

1, a kind of swing type autoclave, its reaction kettle body (8) is installed on the support (1), (2) reductor (3) that drives that it is characterized in that motor is arranged, the eccentric rotating shaft of adorning (6) on the belt pulley (5) that drives by belt (4), the belt pulley, one end is hinged on the eccentrically weighted shaft (6), one end is hinged on the connecting rod (7) on the reaction kettle body end cap (10), and it serves as that axle swings up and down with the cramp bar (9) on the support (1) that eccentrically weighted shaft (6) rotates drivening rod (7) push-and-pull reaction kettle body (8).

2, swing type autoclave as claimed in claim 1 is characterized in that reaction kettle body (8) number of oscillations 10-60 times/minutes, 10-80 ° of horizontal hunting angles.

3, swing type autoclave as claimed in claim 1 is characterized in that being equipped with in the reaction kettle body (8) fixing or movable perforated baffle (14).

4, swing type autoclave as claimed in claim 1, the total measurement (volume) that it is characterized in that reactor (8) can be 300ml-5000ml.

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