CN110270299A - A kind of system producing carbon nanometer roll - Google Patents
A kind of system producing carbon nanometer roll Download PDFInfo
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- CN110270299A CN110270299A CN201910587350.5A CN201910587350A CN110270299A CN 110270299 A CN110270299 A CN 110270299A CN 201910587350 A CN201910587350 A CN 201910587350A CN 110270299 A CN110270299 A CN 110270299A
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- reaction kettle
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- nanometer roll
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/28—Moving reactors, e.g. rotary drums
- B01J19/285—Shaking or vibrating reactors; reactions under the influence of low-frequency vibrations or pulsations
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/18—Nanoonions; Nanoscrolls; Nanohorns; Nanocones; Nanowalls
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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Abstract
The invention discloses a kind of system for producing carbon nanometer roll, including reaction kettle, reaction kettle is to being connected to material carbon storehouse, chemicals A tank, chemicals B tank, condenser system and carbon nanometer roll powder warehouse；Also to being equipped with weighing equipment between material carbon storehouse and reaction kettle；Chemicals A also is filled in chemicals tank A to the first metering pump is connected between chemicals A tank and reaction kettle；Chemicals B also is filled in chemicals tank B to the second metering pump is connected between chemicals B tank and reaction kettle；Reaction kettle includes autoclave body, and autoclave body is equipped with kettle cover, is equipped with hollow cavity in the kettle wall of autoclave body, hollow cavity is connected to vapour source, and hollow cavity bottom is equipped with drain valve, reaction kettle rotation setting, reaction kettle transmission is connected with the driving device for driving reaction kettle to swing, and reaction kettle inner wall is equipped with a plurality of strip bulge.Energy-saving and environmental protection, scale, low cost preparation high-purity.The present invention is applied to carbon nanometer roll production technical field.
Description
Technical field
The present invention relates to carbon nanometer roll production technical fields, and in particular to a kind of system for producing carbon nanometer roll.
Background technique
Graphene nano volume is a kind of novel one-dimensional carbon nano material, is crimped by two-dimensional graphene sheet layer.Stone
The basic construct unit of black alkene nanometer roll is graphene, therefore has some performances similar with graphene, such as high conductivity,
Fabulous electric conductivity and strong mechanical performance etc..Carbon nanometer roll is curled by graphene platelet, has typical stratiform
Hollow structure feature, wall spacing is adjustable, and this hollow structure can accommodate the atom or molecule of (absorption) other elements, to make
For energy storage material.Compared with carbon nanotube, graphene nano volume has open both ends, has by way of being inserted into or adulterating
Adjustable internal capacity and diameter, unique topological structure make graphene nano volume in energy storage (hydrogen storage), capacitor, catalysis, doctor
The various aspects such as drug carrier are with a wide range of applications.So far as is known, the common method that laboratory prepares carbon nanometer roll has electricity
Arc discharge, ultrasonic exfoliated graphite, isopropanol roll three kinds of methods such as single-layer graphene film.Only a small amount of production both at home and abroad, and
And at high cost, price.So far, the report of the commercial run of large-scale production carbon nanometer roll is had not yet seen.
Summary of the invention
The main object of the present invention is to provide a kind of system for producing carbon nanometer roll, energy-saving and environmental protection, scale, low cost
Prepare high-purity.
To achieve the above object, the present invention proposes a kind of system for producing carbon nanometer roll, including reaction kettle, the reaction kettle
To being connected to material carbon storehouse, chemicals A tank, chemicals B tank, condenser system and carbon nanometer roll powder warehouse；
Also to being equipped with weighing equipment between the material carbon storehouse and reaction kettle；
Also to being connected to the first metering pump, filling in the chemicals tank A between the chemicals A tank and reaction kettle
Length of schooling agent A；
Also to being connected to the second metering pump, filling in the chemicals tank B between the chemicals B tank and reaction kettle
Length of schooling agent B；
The reaction kettle includes autoclave body, and the autoclave body is equipped with kettle cover, and hollow cavity is equipped in the kettle wall of the autoclave body, described
Hollow cavity is connected to vapour source, and the hollow cavity bottom is equipped with drain valve, the reaction kettle rotation setting, the reaction kettle transmission
It is connected with the driving device for driving reaction kettle to swing, the reaction kettle inner wall is equipped with a plurality of strip bulge；
First metering pump, the second metering pump respectively include two the first tube bodies and first actuator；
The feed end and discharge end of first tube body are respectively equipped with check valve in the same direction, the feed end of first tube body
It is docked with chemicals A tank or chemicals B tank, the discharge end of first tube body is docked with reaction kettle, first tube body
Middle part is connected with the second tube body, and the junction of second tube body and the first tube body is equipped with diaphragm, and the second pipe body activity is set
There is piston, forms confined space between the diaphragm and piston, be filled with fluid media (medium) in the confined space；
The output end of first actuator is equipped with two ratchets, and the gear teeth of two ratchets are contrary, and two ratchets are arranged respectively
There is corresponding transmission flywheel, is hollow in the middle part of the transmission flywheel, and the middle part hollow part for being driven flywheel is equipped with and corresponding ratchet
The gear teeth of cooperation, two transmission flywheels pass through the first drive rod respectively and are connected with two-piston, and one end of two first drive rods turns respectively
Dynamic to be connected on corresponding piston, the other end of two first drive rods rotates respectively to be connected on corresponding transmission flywheel；
Using the system of above-mentioned production carbon nanometer roll production method the following steps are included:
S1: material carbon is stored in material carbon storehouse；
S2: material carbon is weighed by weighing equipment, and weighed material carbon is put into reaction kettle；
First metering pump measures the chemicals A of corresponding amount according to the weight of material carbon, and the chemicals A of measurement is put
Enter in reaction kettle, at normal temperature, after material carbon impregnates one hour in chemicals A, the second metering pump is according to the weight of material carbon
Amount measures the chemicals B of corresponding amount, and the chemicals B of measurement is put into reaction kettle, then makes to keep temperature in reaction kettle
Degree is not higher than the reaction environment of 0.6MPa not higher than 400 DEG C, reaction pressure；
The Carbon Materials that material carbon obtains after reacting with chemicals A, chemicals B are stored in carbon nanometer roll powder warehouse, former
The carbon nanometer roll powder that material carbon generates after reacting with chemicals A, chemicals B is stored in condenser system after heating condensation
In.
It is further improved, agitating device is equipped in the autoclave body.
Further improved, the condenser system includes drainer, the drainer be located at the top of reaction kettle and with it is anti-
Kettle is answered to be connected to, the drainer is connected with cooling assembly and fluid reservoir, and the fluid reservoir is located at the lower section of drainer.
Further improved, the drainer includes tank body, is equipped with tube bank in the tank body and tube sheet, the tube sheet are located at
The top of tube bank, the tank base are equipped with end socket, and the tank body is connected with cooling assembly, and the end socket is connected with fluid reservoir.
Further improved, the strip bulge is arranged along reaction kettle length direction.
Further improved, each strip bulge is evenly distributed on reaction kettle inner wall.
Further improved, the vapour source is source of high pressure steam.
Further improved, the reaction kettle both ends are equipped with rotation axis, and the reaction kettle is erected at by rotation axis rotation
On two rotation seats, an at least rotation axis is equipped with gear；
The driving device includes the rack gear of the second actuator and sliding setting, and the output end of second actuator is equipped with
Turntable, transmission is connected with the second drive rod between the turntable and rack gear, and one end rotation of second drive rod is connected on turntable,
And second drive rod and turntable tie point not at the center of turntable, the other end rotation of second drive rod is connected in rack gear
On, the rack and pinion engagement.
Further improved, the rack gear sliding is set on the slide rail.
Further improved, second drive rod and turntable have multiple tie points.
Compared with prior art, technical solution of the present invention the utility model has the advantages that
A kind of system producing carbon nanometer roll of the invention is not higher than 400 DEG C in reaction temperature, and pressure is not higher than 0.6MPa
Temperate condition under chemically reacted to obtain carbon nanometer roll powder.During the preparation process, exhaust gas is not discharged, waste liquid is not discharged,
Waste residue is not discharged, process water is not consumed, does not generate strong noise.The present invention has energy-saving and environmental protection, scale, low cost preparation high
The features such as purity.
When material carbon, chemicals A, chemicals B react in a kettle, steam is passed through toward reaction kettle by vapour source
Heat source is provided for reaction kettle, the water that steam is formed is discharged the drain valve of hollow cavity bottom in time.Meanwhile reaction kettle is filled in driving
The drive lower swing set accelerates the mixing and stirring of material carbon, chemicals A, chemicals B, improves its contact area,
Convenient for the progress of reaction.The strip bulge of reaction kettle inner wall further improve material carbon, chemicals A, chemicals B it is mixed
Close stirring efficiency.
First metering pump of the invention, the second metering pump include two the first tube bodies and first actuator, and two first
Two check valves in the same direction are set in tube body, are added chemicals A or chemicals B in the second intracorporal movement of pipe by piston
Enter into reaction kettle, the power resources of piston make two spine by rotating and reverse for the first actuator in first actuator
Wheel drives two transmission flywheel turns respectively, and two transmission flywheels pass through the first drive rod respectively and push two-piston mobile, has saved sky
Between and components, easy to control, structure is simple.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this
Some embodiments of invention for those of ordinary skill in the art without creative efforts, can be with
The structure shown according to these attached drawings obtains other attached drawings.
Fig. 1 is the system schematic for producing carbon nanometer roll；
Fig. 2 is reaction kettle schematic diagram；
Fig. 3 is drainer structural schematic diagram；
Fig. 4 is that reaction kettle is erected at schematic diagram on rotation seat；
Fig. 5 is reaction kettle sectional view；
Fig. 6 is gear, rack gear, sliding rail, the second actuator, the second drive rod annexation figure；
Fig. 7 is the first metering pump and the second metering pump annexation figure.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiment is only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts it is all its
His embodiment, shall fall within the protection scope of the present invention.
It is to be appreciated that the directional instruction such as up, down, left, right, before and after ... of institute is only used in the embodiment of the present invention
Relative positional relationship, the motion conditions etc. in the case where a certain particular pose is as shown in the picture between each component are explained, if this is specific
When posture changes, then directionality instruction also correspondingly changes correspondingly.
In the present invention unless specifically defined or limited otherwise, term " connection ", " fixation " etc. shall be understood in a broad sense,
For example, " fixation " may be a fixed connection, it may be a detachable connection, or integral；It can be mechanical connection, be also possible to
Electrical connection；It can be directly connected, the connection inside two elements or two can also be can be indirectly connected through an intermediary
The interaction relationship of a element, unless otherwise restricted clearly.It for the ordinary skill in the art, can basis
Concrete condition understands the concrete meaning of above-mentioned term in the present invention.
It in addition, the technical solution between each embodiment of the present invention can be combined with each other, but must be general with this field
Based on logical technical staff can be realized, it will be understood that when the combination of technical solution appearance is conflicting or cannot achieve this
The combination of technical solution is not present, also not the present invention claims protection scope within.
Fig. 1 to Fig. 7 is please referred to, present embodiment discloses a kind of system for producing carbon nanometer roll, including reaction kettle 1, reactions
Kettle 1 is to being connected to material carbon storehouse 2, chemicals A tank 3, chemicals B tank 4, condenser system and carbon nanometer roll powder warehouse 5；
Also to being equipped with weighing equipment 7 between material carbon storehouse 2 and reaction kettle 1；
Chemical system also is filled in chemicals tank A to the first metering pump 8 is connected between chemicals A tank 3 and reaction kettle 1
Agent A；
Chemical system also is filled in chemicals tank B to the second metering pump 9 is connected between chemicals B tank 4 and reaction kettle 1
Agent B；
Reaction kettle 1 includes autoclave body 11, and autoclave body 11 is equipped with kettle cover 12, and hollow cavity 13 is equipped in the kettle wall of autoclave body 11, hollow
Chamber 13 is connected to vapour source, and 13 bottom of hollow cavity is equipped with drain valve, and the rotation setting of reaction kettle 1, it is anti-that the transmission of reaction kettle 1 is connected with drive
The driving device for answering kettle 1 to swing, 1 inner wall of reaction kettle are equipped with a plurality of strip bulge 14；Drain valve is a kind of valve for crossing water only gas
Door, the water in hollow cavity can be discharged.Strip bulge 14 stirs the material inside reaction kettle 1 when rotating convenient for reaction kettle 1
It mixes.Vapour source is passed through steam in hollow cavity 13, provides heat source to reaction kettle 1, the heat source provided is relatively stable, uniformly, is convenient for
Control.
First metering pump 8, the second metering pump 9 respectively include two the first tube bodies 81 and first actuator 82；First
Actuator 82 is twin shaft stepper motor, which is electrically connected with switch and power supply.
The feed end and discharge end of first tube body 81 are respectively equipped with check valve 83 in the same direction, the feed end of the first tube body 81 with
Chemicals A tank 3 or chemicals B tank 4 dock, and the discharge end of the first tube body 81 is docked with reaction kettle 1,81 middle part of the first tube body
It is connected with the second tube body 84, the junction of the second tube body 84 and the first tube body 81 is equipped with diaphragm 85, is movably equipped in the second tube body 84
Piston 86 forms confined space, is filled with fluid media (medium) in confined space between diaphragm 85 and piston 86；
The output end of first actuator 82 is equipped with two ratchets 87, and the gear teeth of two ratchets 87 are contrary, two ratchets 87 difference
Be arranged with corresponding transmission flywheel 88, it is hollow for being driven in the middle part of flywheel 88, and the middle part hollow part for being driven flywheel 88 be equipped with it is right
The gear teeth for answering ratchet 87 to cooperate, two transmission flywheels 88 are connected by the first drive rod 89 with two-piston 86 respectively, two first transmissions
One end of bar 89 rotates respectively to be connected on corresponding piston 86, the other end of two first drive rods 89 rotate respectively be connected in it is corresponding
It is driven on flywheel 88；
Fig. 7 is please referred to, in practice, two ratchets 87 are attached separately to the output end of twin shaft stepper motor, for the ease of showing,
Two ratchets 87 are shown simultaneously in Fig. 7.The gear teeth of two ratchets 87 are sharp arc, and each gear teeth have directionality；
Corresponding, the gear teeth being driven in flywheel 88 are the sharp arc with the cooperation of the gear teeth of ratchet 87, mutually matched ratchet 87
It is only capable of that mutually rotation occurs toward a direction between transmission flywheel 88, when the first actuator 82 rotates forward, one of ratchet
87 can drive matched transmission flywheel 88 to rotate, and occur between another ratchet 87 and matched transmission flywheel 88
Relatively rotate, another transmission flywheel 88 will not be driven, transmission flywheel 88 drive for being driven rotation be attached thereto the
One drive rod, 89 eccentric rotary, the transmission flywheel 88 for being driven rotation pass through the first drive rod 89 being attached thereto and drive wherein
One piston 86 moves back and forth, and so as to make one of them first tube body 81 work, chemicals A or chemicals B is added
In reaction kettle 1.Similarly, when the first actuator 82 invert when, then make another transmission flywheel 88 rotate, thus make another first
Tube body 81 works.The advantage of doing so is that two pistons 86 can be driven mobile by one first driving 82, to control respectively
Make the first metering pump 8 and the work of the second metering pump 9.Twin shaft stepper motor can also be controlled by stepper motor driver and carry out unification
Control.As for scale or other modes are arranged on two first tube bodies 81 with calculate the first metering pump 8 and the second metering pump 9 into
To amount, has in this existing technology very much, be not described herein.
Piston 86 during reciprocating movement, make confined space compress or expand, confined space during compression,
Chemicals A or chemicals B can be made to enter in reaction kettle 1 from the first tube body 81；Confined space can make during expansion
Chemically preparation A tank 3 or chemicals B tank 4 enter in the first tube body 81 chemicals A or chemicals B.
Using the system of above-mentioned production carbon nanometer roll production method the following steps are included:
S1: material carbon is stored in material carbon storehouse 2；
S2: material carbon is weighed by weighing equipment 7, and weighed material carbon is put into reaction kettle 1, reaction kettle 1 is driving
The drive lower swing of dynamic device；
First metering pump 8 measures the chemicals A of corresponding amount according to the weight of material carbon, and by the chemicals A of measurement
It is put into reaction kettle 1, at normal temperature, after material carbon impregnates one hour in chemicals A, the second metering pump 9 is according to material carbon
Weight measure the chemicals B of corresponding amount, and the chemicals B of measurement is put into reaction kettle 1, is then made in reaction kettle 1
Temperature is kept to be not higher than the reaction environment of 0.6MPa not higher than 400 DEG C, reaction pressure；
The Carbon Materials that material carbon obtains after reacting with chemicals A, chemicals B are stored in carbon nanometer roll powder warehouse 5, former
The carbon nanometer roll powder that material carbon generates after reacting with chemicals A, chemicals B is stored in condenser system after heating condensation
In.
In the present embodiment chemicals A and chemicals B in existing technology there are many, as long as can be realized above-mentioned side
The medicament of method.But the production carbon nanometer roll for focusing on being used by means of the medicament of the present invention and the present embodiment is
System, the system of the production carbon nanometer roll have having an unexpected effect compared with the existing technology, have substantive features and show
The progress of work.
Material carbon is not higher than 400 DEG C in reaction temperature by the present embodiment, and reaction pressure is not higher than the temperate condition of 0.6MPa
Under carry out being chemically reacted to obtain carbon nanometer roll powder.
In the present embodiment, agitating device 111 is equipped in autoclave body 11, agitating device 111 is anchor agitator, can also be used
The mixing plant of other models, various mixing plants are all many currently on the market.
In the present embodiment, condenser system includes drainer 10, drainer 10 be located at the top of reaction kettle 1 and with reaction kettle 1
Connection, drainer 10 are connected with cooling assembly 101 and fluid reservoir 102, and fluid reservoir 102 is located at the lower section of drainer 10.Cooling assembly
101 are mainly used for providing cold source for drainer 10, and the organic matter in reaction kettle 1 evaporates or distill after the heating cold to drainer 10
But, liquid after cooling is stored in fluid reservoir 102.
In the present embodiment, drainer 10 includes tank body 103, is equipped with tube bank 104 and tube sheet 105, tube sheet 105 in tank body 103
Positioned at the top of tube bank 104,103 bottom of tank body is equipped with end socket 106, and tank body 103 is connected with cooling assembly 101, end socket 106 and storage
Flow container 102 is connected.The design feature of the drainer 10 is that recirculated water cooling condenser, freezing water condenser, liquid trap, product are just store
Flow container is integrated in one.Such benefit has:
(1) valve, the pipe between recirculated water cooling condenser, freezing water condenser, liquid trap, the first receiver of product had both been greatly simplified
The high flowmeter that drops in price also is removed in the connection of line；
(2) equipment investment expense and occupation area of equipment is greatly saved；
(3) greatly reduce the leakage point of pipeline, valve etc.；
(4) safe handling of system is greatly increased.
In the present embodiment, strip bulge 14 is arranged along 1 length direction of reaction kettle.When reaction kettle 1 rotates, reaction kettle 1 passes through
Strip bulge 14 is stirred material, more preferable to material active force when strip bulge 14 is arranged along 1 length direction of reaction kettle.
In the present embodiment, each strip bulge 14 is evenly distributed on 1 inner wall of reaction kettle.
In the present embodiment, vapour source is source of high pressure steam, and it is anti-that general high steam temperature, which can reach 200 DEG C or more,
Kettle 1 is answered to provide enough heat sources.
In the present embodiment, 1 both ends of reaction kettle are equipped with rotation axis 15, and reaction kettle 1 is erected at two turns by the rotation of rotation axis 15
On dynamic seat 16, an at least rotation axis 15 is equipped with gear 17；
Driving device includes the rack gear 19 of the second actuator 18 and sliding setting, and the output end of the second actuator 18, which is equipped with, to be turned
Disk 20, transmission is connected with the second drive rod 21 between turntable 20 and rack gear 19, and one end rotation of the second drive rod 21 is connected in turntable 20
On, and the tie point 201 of the second drive rod 21 and turntable 20, or not the center of turntable 20, the other end of the second drive rod 21 rotates
It is connected on rack gear 19, rack gear 19 is engaged with gear 17.It is connected on turntable 20 by connecting rod 21, the second actuator 18 is with turn
21 eccentric rotary of connecting rod is driven when disk 20 rotates.The transmission of gear 17 and rack gear 19 is relatively stable, and driven load is larger, prolonged
It is durable, it can smoothly drive reaction kettle 1 to swing.
In the present embodiment, the sliding of rack gear 19 is located on sliding rail 22.
In the present embodiment, the second drive rod 21 has multiple tie points 201, the different tie point of connecting rod 21 with turntable 20
When 201, the amplitude of fluctuation of reaction kettle 1 is different, and the reciprocating movement of rack gear 19 is displaced different.
The above description is only a preferred embodiment of the present invention, is not intended to limit the scope of the invention, all at this
Under the inventive concept of invention, using equivalent structure transformation made by description of the invention and accompanying drawing content, or directly/use indirectly
It is included in other related technical areas in scope of patent protection of the invention.
Claims (10)
1. a kind of system for producing carbon nanometer roll, which is characterized in that including reaction kettle (1), the reaction kettle (1) is to being connected to raw material
Carbon storehouse (2), chemicals A tank (3), chemicals B tank (4), condenser system and carbon nanometer roll powder warehouse (5)；
Also to being equipped with weighing equipment (7) between the material carbon storehouse (2) and reaction kettle (1)；
Also to being connected to the first metering pump (8) between the chemicals A tank (3) and reaction kettle (1), in the chemicals tank A
Fill chemicals A；
Also to being connected to the second metering pump (9) between the chemicals B tank (4) and reaction kettle (1), in the chemicals tank B
Fill chemicals B；
The reaction kettle (1) includes autoclave body (11), and the autoclave body (11) is equipped with kettle cover (12), in the kettle wall of the autoclave body (11)
Equipped with hollow cavity (13), the hollow cavity (13) is connected to vapour source, and hollow cavity (13) bottom is equipped with drain valve, described anti-
Kettle (1) rotation setting is answered, reaction kettle (1) transmission is connected with the driving device for driving reaction kettle (1) to swing, the reaction kettle
(1) inner wall is equipped with a plurality of strip bulge (14)；
First metering pump (8), the second metering pump (9) include two the first tube bodies (81) and first actuator (82)；
The feed end and discharge end of two first tube bodies (81) are respectively equipped with check valve in the same direction (83), first tube body (81)
Feed end is docked with chemicals A tank (3) or chemicals B tank (4), the discharge end and reaction kettle of first tube body (81)
(1) it docks, is connected with the second tube body (84) in the middle part of first tube body (81), second tube body (84) and the first tube body (81)
Junction is equipped with diaphragm (85), is movably equipped with piston (86) in second tube body (84), the diaphragm (85) and piston (86)
Between form confined space, fluid media (medium) is filled in the confined space；
The output end of first actuator (82) is equipped with two ratchets (87), and the gear teeth of two ratchets (87) are contrary, two ratchets
(87) it is arranged with corresponding transmission flywheel (88) respectively, is hollow in the middle part of the transmission flywheel (88), and be driven flywheel (88)
Middle part hollow part is equipped with the gear teeth that cooperates with corresponding ratchet (87), two transmissions flywheel (88) pass through respectively the first drive rod (89) and
Two-piston (86) is connected, and one end of two first drive rods (89) rotates respectively to be connected on corresponding piston (86), two first transmissions
The other end of bar (89) rotates respectively to be connected on corresponding transmission flywheel (88)；
Using the system of above-mentioned production carbon nanometer roll production method the following steps are included:
S1: material carbon is stored in material carbon storehouse (2)；
S2: material carbon is weighed by weighing equipment (7), and weighed material carbon is put into reaction kettle (1), reaction kettle (1) exists
The drive lower swing of driving device；
First metering pump (8) measures the chemicals A of corresponding amount according to the weight of material carbon, and the chemicals A of measurement is put
Enter in reaction kettle (1), at normal temperature, after material carbon impregnates one hour in chemicals A, the second metering pump (9) is according to raw material
The weight of carbon measures the chemicals B of corresponding amount, and the chemicals B of measurement is put into reaction kettle (1), then makes reaction kettle
(1) temperature is kept to be not higher than the reaction environment of 0.6MPa not higher than 400 DEG C, reaction pressure in；
The Carbon Materials that material carbon obtains after reacting with chemicals A, chemicals B are stored in carbon nanometer roll powder warehouse (5), raw material
The carbon nanometer roll powder that carbon generates after reacting with chemicals A, chemicals B is stored in condenser system after heating condensation.
2. the system of production carbon nanometer roll according to claim 1, which is characterized in that be equipped with stirring in the autoclave body (11)
Device (111).
3. the system of production carbon nanometer roll according to claim 1, which is characterized in that the condenser system includes drainer
(10), the drainer (10) is located at the top of reaction kettle (1) and is connected to reaction kettle (1), and the drainer (10) is connected with system
Cold component (101) and fluid reservoir (102), the fluid reservoir (102) are located at the lower section of drainer (10).
4. the system of production carbon nanometer roll according to claim 3, which is characterized in that the drainer (10) includes tank body
(103), tube bank (104) and tube sheet (105) are equipped in the tank body (103), the tube sheet (105) is located at the upper of tube bank (104)
Side, tank body (103) bottom are equipped with end socket (106), and the tank body (103) is connected with cooling assembly (101), the end socket
(106) it is connected with fluid reservoir (102).
5. the system of production carbon nanometer roll according to claim 1, which is characterized in that the strip bulge (14) is along reaction
The setting of kettle (1) length direction.
6. the system of production carbon nanometer roll according to claim 5, which is characterized in that each strip bulge (14) is uniformly distributed
In reaction kettle (1) inner wall.
7. the system of production carbon nanometer roll according to claim 1, which is characterized in that the vapour source is high steam
Source.
8. the system of production carbon nanometer roll according to claim 1, which is characterized in that reaction kettle (1) both ends are equipped with
Rotation axis (15), the reaction kettle (1) are erected on two rotation seats (16) by rotation axis (15) rotation, an at least rotation axis
(15) gear (17) are equipped with；
The driving device include the second actuator (18) and sliding be arranged rack gear (19), second actuator (18) it is defeated
Outlet is equipped with turntable (20), and transmission is connected with the second drive rod (21) between the turntable (20) and rack gear (19), and described second passes
One end rotation of lever (21) is connected on turntable (20), and the second drive rod (21) and the tie point (201) of turntable (20) do not exist
The other end rotation at the center of turntable (20), second drive rod (21) is connected on rack gear (19), the rack gear (19) and tooth
Take turns (17) engagement.
9. the system of production carbon nanometer roll according to claim 8, which is characterized in that rack gear (19) sliding is located at cunning
On rail (22).
10. it is according to claim 8 production carbon nanometer roll system, which is characterized in that second drive rod (21) with
Turntable (20) has multiple tie points (201).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910587350.5A CN110270299A (en) | 2019-07-02 | 2019-07-02 | A kind of system producing carbon nanometer roll |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910587350.5A CN110270299A (en) | 2019-07-02 | 2019-07-02 | A kind of system producing carbon nanometer roll |
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| Publication Number | Publication Date |
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| CN110270299A true CN110270299A (en) | 2019-09-24 |
Family
ID=67963883
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910587350.5A Withdrawn CN110270299A (en) | 2019-07-02 | 2019-07-02 | A kind of system producing carbon nanometer roll |
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| Country | Link |
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| CN (1) | CN110270299A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2230617Y (en) * | 1995-07-07 | 1996-07-10 | 华中理工大学 | Swinging high-pressure reactor |
| WO2006021249A1 (en) * | 2004-08-19 | 2006-03-02 | Lurgi Ag | Device for removing ammonia or amines from reaction solutions |
| CN205517753U (en) * | 2016-04-12 | 2016-08-31 | 深圳市通产丽星股份有限公司 | Reaction unit of functional graphite alkene of industrialization preparation |
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| CN108236889A (en) * | 2018-02-27 | 2018-07-03 | 任永飞 | A kind of system of coal aromatic hydrocarbons |
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2019
- 2019-07-02 CN CN201910587350.5A patent/CN110270299A/en not_active Withdrawn
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|---|---|---|---|---|
| CN2230617Y (en) * | 1995-07-07 | 1996-07-10 | 华中理工大学 | Swinging high-pressure reactor |
| WO2006021249A1 (en) * | 2004-08-19 | 2006-03-02 | Lurgi Ag | Device for removing ammonia or amines from reaction solutions |
| CN205517753U (en) * | 2016-04-12 | 2016-08-31 | 深圳市通产丽星股份有限公司 | Reaction unit of functional graphite alkene of industrialization preparation |
| CN206359787U (en) * | 2016-12-20 | 2017-07-28 | 宁国佩特恩电器科技有限公司 | A kind of two-chamber piston pump |
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