CN221656584U - Be used for hydrazine ester hydrazine production of biphenyl reation kettle - Google Patents
Be used for hydrazine ester hydrazine production of biphenyl reation kettle Download PDFInfo
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- CN221656584U CN221656584U CN202420012629.7U CN202420012629U CN221656584U CN 221656584 U CN221656584 U CN 221656584U CN 202420012629 U CN202420012629 U CN 202420012629U CN 221656584 U CN221656584 U CN 221656584U
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- Prior art keywords
- fixedly connected
- kettle
- production
- kettle body
- wall
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- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 22
- 150000002148 esters Chemical class 0.000 title claims abstract description 15
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 title claims description 6
- 235000010290 biphenyl Nutrition 0.000 title claims description 3
- 239000004305 biphenyl Substances 0.000 title claims description 3
- 238000006243 chemical reaction Methods 0.000 claims abstract description 36
- 238000003756 stirring Methods 0.000 claims abstract description 25
- 238000004140 cleaning Methods 0.000 claims abstract description 17
- 230000007246 mechanism Effects 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 36
- 239000005653 Bifenazate Substances 0.000 claims description 11
- VHLKTXFWDRXILV-UHFFFAOYSA-N bifenazate Chemical compound C1=C(NNC(=O)OC(C)C)C(OC)=CC=C1C1=CC=CC=C1 VHLKTXFWDRXILV-UHFFFAOYSA-N 0.000 claims description 11
- 238000007790 scraping Methods 0.000 claims description 9
- 230000005540 biological transmission Effects 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims 1
- -1 biphenyl hydrazine ester Chemical class 0.000 abstract description 8
- 238000005406 washing Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 9
- 239000002994 raw material Substances 0.000 description 7
- 230000009471 action Effects 0.000 description 6
- 239000007921 spray Substances 0.000 description 6
- 229940067157 phenylhydrazine Drugs 0.000 description 5
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 4
- 235000017491 Bambusa tulda Nutrition 0.000 description 4
- 241001330002 Bambuseae Species 0.000 description 4
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 4
- 239000011425 bamboo Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000012295 chemical reaction liquid Substances 0.000 description 2
- 238000005984 hydrogenation reaction Methods 0.000 description 2
- HKOOXMFOFWEVGF-UHFFFAOYSA-N phenylhydrazine Chemical compound NNC1=CC=CC=C1 HKOOXMFOFWEVGF-UHFFFAOYSA-N 0.000 description 2
- ADYKPXIKPPZOQF-UHFFFAOYSA-N 1,1'-biphenyl;hydrazine Chemical compound NN.C1=CC=CC=C1C1=CC=CC=C1 ADYKPXIKPPZOQF-UHFFFAOYSA-N 0.000 description 1
- 230000000895 acaricidal effect Effects 0.000 description 1
- 239000000642 acaricide Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- OAKJQQAXSVQMHS-UHFFFAOYSA-O hydrazinium(1+) Chemical compound [NH3+]N OAKJQQAXSVQMHS-UHFFFAOYSA-O 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model provides a reaction kettle for hydrazinization production of biphenyl hydrazine ester, and relates to the technical field of reaction kettles for hydrazinization production of biphenyl hydrazine ester. This a reation kettle for production of biphenhydrazinate hydrazine ester hydrazine is through the cooperation setting between the cauldron body, axe lid, stirring wiper mechanism, ring gear, motor and the belt pulley two, can make the device have cleaning function, thereby effectually avoid people to need open the axe lid and wash the inner wall of the cauldron body and make people comparatively trouble condition, not only make people can comparatively convenient wash its inner wall after the cauldron body has used, and effectually reduced the staff and to the washing difficulty of the cauldron body, simultaneously can effectually avoided the lower condition of the cleaning efficiency of the cauldron body that leads to because of adopting manual abluent mode.
Description
Technical Field
The utility model relates to a reaction kettle for hydrazinization production of biphenyl hydrazine ester, in particular to a reaction kettle for hydrazinization production of biphenyl hydrazine ester, belonging to the technical field of reaction kettles for hydrazinization production of biphenyl hydrazine ester.
Background
Phenylhydrazine ester is a white solid crystal, and is usually used as acaricide, and the reaction liquid of phenylhydrazine ester needs to be subjected to hydrogenation reaction in the preparation process of the phenylhydrazine ester, and the hydrogenation reaction of the reaction liquid is generally carried out in a reaction kettle.
The utility model discloses a reation kettle for production of biphendrazide ester hydrazinization in chinese patent application publication CN218590464U, it includes the cauldron body and sets up the agitating unit on the cauldron body, and agitating unit is used for stirring the internal portion of cauldron, and the top of the cauldron body is connected with the depressurization pipe with the internal portion intercommunication of cauldron, is provided with the relief valve on the depressurization pipe, and then can reduce the potential safety hazard of reation kettle in the use.
In the process of carrying out reaction production on the phenylhydrazine ester hydrazine, we can know that after processing in the reaction kettle is finished, some raw materials generally remain in the reaction kettle, in order to ensure the accuracy of the proportioning of the raw materials added next time, the residual phenylhydrazine ester hydrazine raw materials on the inner wall of the reaction kettle are required to be cleaned after each use, but in the technical scheme of the comparison document, the reaction kettle inner wall is not required to be cleaned, so that a worker is required to open a cover to manually clean the inner wall of the reaction kettle, and meanwhile, the cover is arranged on the upper surface of the reaction kettle through a plurality of groups of bolts, so that people are more troublesome when opening the cover to flush the inner wall of the reaction kettle, the cleaning difficulty of the worker is increased, and the inner wall of the reaction kettle is manually cleaned with lower efficiency.
Disclosure of utility model
(One) solving the technical problems
The utility model aims to solve the problems and provide a reaction kettle for hydrazinization production of bifenazate, which solves the problem that the inner wall of the reaction kettle needs to be manually cleaned after the reaction kettle is used because the reaction kettle does not have a cleaning function.
(II) technical scheme
The utility model is realized by the following technical scheme: the reaction kettle for hydrazinization production of the bifenazate comprises a kettle body, wherein an axe cover is arranged on the upper surface of the kettle body, and a stirring and cleaning mechanism is arranged in the kettle body;
The stirring and cleaning mechanism comprises a rotating cylinder which is rotationally connected to the inner wall of the kettle body, a belt pulley I is fixedly connected to the outer surface of the rotating cylinder, a water pipe connector is fixedly connected to the outer surface of the rotating cylinder, a fixed disc is fixedly connected to the outer surface of the rotating cylinder, and the fixed disc can be driven to rotate along with the rotation of the rotating cylinder;
The bottom surface of the fixed disc is fixedly connected with three L-shaped connecting plates, the outer surface of each L-shaped connecting plate is fixedly connected with a scraping plate, the scraping plates are in contact with the inner wall of the kettle body, the outer surface of the fixed disc is fixedly connected with a group of fixed plates, the bottom surface of each fixed plate is fixedly connected with a connecting column, and the bottom end of each connecting column is rotationally connected with a first gear;
Every the equal fixedly connected with carrier bar in bottom surface of gear one, every the equal fixedly connected with of surface of carrier bar a set of stirring vane, the surface mounting of a set of one-way shower nozzle of rotation section of thick bamboo, along with the rotation of gear one, can drive stirring vane's rotation, and then realize stirring the biphendrazide ester hydrazine in the reaction process to accelerate its reaction effect, one-way shower nozzle belongs to prior art, and does not show the concrete details of one-way shower nozzle, and water can spray in the inner wall of the cauldron body through one-way shower nozzle in entering into the rotation section of thick bamboo.
Above-mentioned, the inner wall fixedly connected with ring gear of cauldron body, gear one meshes with the ring gear mutually, along with the circular motion of gear one, under the effect with the ring gear meshing, can realize gear one and rotation simultaneously at the circular motion.
Specifically, the upper surface mounting of axe lid has the motor, the output fixedly connected with belt pulley two, belt pulley two passes through the belt and is connected with belt pulley one transmission, and the motor belongs to prior art, and the motor passes through the support mounting in the upper surface of axe lid, along with the rotation of belt pulley two can be driven in the start-up of motor, and then can drive the rotation of belt pulley one under the effect of belt.
Specifically, the surface intercommunication of the cauldron body has the filling tube, the bottom surface intercommunication of the cauldron body has the row material pipe, and people can be through opening the lid on the filling tube to the internal filling raw materials of cauldron to can be discharged the biphendrazide ester hydrazine after the reaction processing through opening the valve on the row material pipe.
Further, the surface fixedly connected with brace table of the cauldron body, four supporting legs of bottom surface fixedly connected with of brace table can play the supporting role to the cauldron body through the brace table, can play the supporting role to the brace table through the supporting leg.
Further, the below of the cauldron body is provided with the water pump, the output intercommunication of water pump has the raceway, the raceway rotates the inner wall of being connected in the water pipe connector, and the water pump belongs to prior art, and the input of water pump is linked together with outside water source, through rotating the raceway with the water pipe connector and being connected, can make the raceway can not cause the interference to the rotation of rotating the section of thick bamboo, can pour into the outside water source into through the raceway in the section of thick bamboo through starting the water pump.
The utility model provides a reaction kettle for hydrazinization production of bifenazate, which has the following beneficial effects:
1. This a reation kettle for production of biphenhydrazinate hydrazine ester hydrazine is through the cauldron body, axe lid, stirring wiper mechanism, the cooperation setting between ring gear, motor and the belt pulley two, can make the device have cleaning function, thereby effectually avoided people to need open the axe lid and wash the inner wall of the cauldron body and make people comparatively trouble condition, not only make people can be comparatively convenient wash its inner wall after the cauldron body has used, and effectually reduced the staff and to the washing difficulty of the cauldron body, simultaneously can effectually avoided the lower condition of the cleaning efficiency to the cauldron body that leads to because of adopting manual abluent mode.
2. This a reation kettle for production of biphendrazide ester hydrazinization is through the cooperation setting between fixed disk, the fixed plate, the spliced pole, gear one, the carrier bar, stirring vane and the ring gear, stirring effect when can further improve the reaction of biphendrazide ester hydrazinization, along with the rotation of fixed disk can drive fixed plate circular motion, can drive gear one's circular motion under the connected action of spliced pole, under gear one and ring gear meshing's effect, can drive gear one in circular motion and the rotation, and then drive the carrier bar rotation in circular motion, thereby stirring effect when the reaction of biphendrazide ester hydrazinium can be further guaranteed under stirring vane's effect.
Drawings
FIG. 1 is a schematic elevation view of a three-dimensional structure of the present utility model;
FIG. 2 is a schematic view of a portion of the structure of the present utility model;
FIG. 3 is a schematic view of the internal structure of the kettle body of the present utility model;
Fig. 4 is a schematic perspective view of the stirring and cleaning mechanism of the present utility model.
Description of the reference numerals
1. A kettle body;
2. An axe cover;
3. A stirring and cleaning mechanism; 301. a rotating cylinder; 302. a first belt pulley; 303. a water pipe connector; 304. a fixed plate; 305. an L-shaped connecting plate; 306. a scraper; 307. a fixing plate; 308. a connecting column; 309. a first gear; 310. a carrier bar; 311. stirring blades; 312. a unidirectional spray head;
4. a toothed ring; 5. a motor; 6. a belt pulley II; 7. a feeding tube;
8. A discharge pipe; 9. a support table; 10. support legs; 11. a water pump; 12. a water pipe.
Detailed Description
The embodiment of the utility model provides a reaction kettle for hydrazinization production of bifenazate.
Referring to fig. 1, 2, 3 and 4, the kettle comprises a kettle body 1, wherein the kettle body 1 belongs to the prior art, the kettle body 1 does not belong to the main innovation direction of the application, so specific details of the kettle body 1 are not shown in the drawings, a control panel is arranged on the outer surface of the kettle body 1, an axe cover 2 is arranged on the upper surface of the kettle body 1, the axe cover 2 is arranged on the upper surface of the kettle body 1 through bolts, and a stirring and cleaning mechanism 3 is arranged in the kettle body 1;
The stirring and cleaning mechanism 3 comprises a rotating cylinder 301 which is rotationally connected to the inner wall of the kettle body 1, the top end of the rotating cylinder 301 extends to the upper part of the axe cover 2, a belt pulley I302 is fixedly connected to the outer surface of the rotating cylinder 301, the rotating of the rotating cylinder 301 can be driven by the rotation of the belt pulley I302, a water pipe connector 303 is fixedly connected to the outer surface of the rotating cylinder 301, a fixed disc 304 is fixedly connected to the outer surface of the rotating cylinder 301, and the fixed disc 304 can be driven to rotate along with the rotation of the rotating cylinder 301;
The bottom surface of the fixed disk 304 is fixedly connected with three L-shaped connecting plates 305, along with the rotation of the fixed disk 304, the rotation of the L-shaped connecting plates 305 can be driven, the outer surface of each L-shaped connecting plate 305 is fixedly connected with a scraping plate 306, the rotation of the scraping plate 306 can be driven through the rotation of the L-shaped connecting plates 305, the scraping plate 306 is contacted with the inner wall of the kettle body 1, along with the circular motion of the scraping plate 306, the cleaning of the raw materials of the residual dihydrazide ester in the inner wall of the kettle body 1 can be realized, the outer surface of the fixed disk 304 is fixedly connected with a group of fixed plates 307, the number of the fixed plates 307 is three, the bottom surface of each fixed plate 307 is fixedly connected with a connecting column 308, the circular motion of the connecting column 308 can be driven through the circular motion of the fixed plates 307, the bottom end of each connecting column 308 is rotationally connected with a first gear 309, and the first gear 309 can rotate at the bottom end of the connecting column 308;
The bottom surface of every gear one 309 all fixedly connected with carrier bar 310, the equal fixedly connected with of surface of every carrier bar 310 is a set of stirring vane 311, a set of one-way shower nozzle 312 is installed to the surface of rotating cylinder 301, along with the rotation of gear one 309, can drive the rotation of stirring vane 311, and then realize stirring the biphenhydralazine in the reaction process, thereby accelerate its reaction effect, one-way shower nozzle 312 belongs to prior art, and not demonstrate the concrete details of one-way shower nozzle 312, water can spray in the inner wall of cauldron body 1 through one-way shower nozzle 312 in entering into rotating cylinder 301.
The inner wall of the kettle body 1 is fixedly connected with a toothed ring 4, the first gear 309 is meshed with the toothed ring 4, and along with the circular motion of the first gear 309, the first gear 309 can realize the rotation and the simultaneous circular motion of the first gear 309 under the action of meshing with the toothed ring 4.
The upper surface mounting of axe lid 2 has motor 5, and motor 5's output fixedly connected with belt pulley two 6, belt pulley two 6 pass through the belt and are connected with belt pulley one 302 transmission, and motor 5 belongs to prior art, and motor 5 passes through the support mounting in axe lid 2's upper surface, along with motor 5's start-up can drive the rotation of belt pulley two 6, and then can drive the rotation of belt pulley one 302 under the effect of belt.
The surface intercommunication of the cauldron body 1 has charging tube 7, and the bottom surface intercommunication of the cauldron body 1 has row material pipe 8, and people can be through opening the lid on the charging tube 7 and annotate the raw materials in to the cauldron body 1 to can discharge the biphendrazide ester hydrazine after the reaction processing through opening the valve on row material pipe 8.
The surface fixedly connected with supporting bench 9 of cauldron body 1, the bottom surface fixedly connected with four supporting legs 10 of supporting bench 9 can play the supporting role to the cauldron body 1 through supporting bench 9, can play the supporting role to supporting bench 9 through supporting leg 10.
The below of cauldron body 1 is provided with water pump 11, and the output intercommunication of water pump 11 has raceway 12, and raceway 12 rotates the inner wall of being connected in water pipe connector 303, and water pump 11 belongs to prior art, and the input of water pump 11 is linked together with outside water source, through rotating raceway 12 and water pipe connector 303 to be connected, can make raceway 12 can not cause the interference to the rotation of rotating cylinder 301, can pour into the water source of outside into through raceway 12 in rotating cylinder 301 through starting water pump 11.
The utility model is used when in use: firstly, raw materials are filled into a kettle body 1 through a charging pipe 7, then the kettle body 1 and a motor 5 are started through a control panel on the kettle body 1, along with the starting of the motor 5, a belt pulley II 6 is driven to rotate, and then a rotating cylinder 301 is driven to rotate, so that the rotation of a fixed disk 304 is driven, along with the rotation of the fixed disk 304, a fixed plate 307 is driven to move circularly, a first gear 309 is driven to move circularly under the connection action of a connecting column 308, the first gear 309 is driven to move circularly and rotate under the action of meshing of the first gear 309 and a toothed ring 4, a carrier rod 310 is driven to rotate while moving circularly, stirring of the bifenazate hydrazine in the reaction process can be realized under the action of a stirring blade 311, after the bifenazate hydrazine is processed, after the discharge, when the inner wall of the kettle body 1 needs to be cleaned, the worker can start the water pump 11, inject external water source into the rotating cylinder 301 through the water pipe 12, spray water into the inner wall of the kettle body 1 through the one-way spray nozzle 312, then drive the rotating cylinder 301 to rotate along with the starting of the motor 5 through the starting motor 5, further drive the fixed disc 304 to rotate, drive the circular motion of the L-shaped connecting plate 305 along with the rotation of the fixed disc 304, scrape the residual biphenyl hydrazine on the inner wall of the kettle body 1 under the contact action of the scraping plate 306 and the inner wall of the kettle body 1, flush the inner wall of the kettle body 1 through the water source sprayed by the one-way spray nozzle 312, thereby completing the cleaning of the inner wall after the kettle body 1 is used, thereby effectually avoided people to need open axe's lid 2 come to wash the inner wall of the cauldron body 1 and make the comparatively trouble condition of people, not only make people can comparatively convenient wash its inner wall after the cauldron body 1 has used to effectually reduced the staff and to the washing degree of difficulty of the cauldron body 1, simultaneously can effectually avoided the lower condition of the cleaning efficiency of the cauldron body 1 that leads to owing to adopting manual abluent mode, after the inner wall to the cauldron body 1 washs to accomplish, the staff can be through opening the control valve on the discharge pipe 8 with wasing the waste water discharge after.
The foregoing has shown and described the basic principles and main features of the present utility model and the advantages of the present utility model. It will be understood by those skilled in the art that the present utility model is not limited to the embodiments described above, and that the above embodiments and descriptions are merely illustrative of the principles of the present utility model, and various changes and modifications may be made without departing from the spirit and scope of the utility model, which is defined in the appended claims. The scope of the utility model is defined by the appended claims and equivalents thereof.
Claims (6)
1. Be used for hydrazine ester hydrazine production of biphenyl to use reation kettle, including the cauldron body (1), its characterized in that: an axe cover (2) is arranged on the upper surface of the kettle body (1), and a stirring and cleaning mechanism (3) is arranged in the kettle body (1);
The stirring and cleaning mechanism (3) comprises a rotating cylinder (301) which is rotatably connected to the inner wall of the kettle body (1), a belt pulley I (302) is fixedly connected to the outer surface of the rotating cylinder (301), a water pipe connector (303) is fixedly connected to the outer surface of the rotating cylinder (301), and a fixed disc (304) is fixedly connected to the outer surface of the rotating cylinder (301);
The bottom surface of the fixed disc (304) is fixedly connected with three L-shaped connecting plates (305), the outer surface of each L-shaped connecting plate (305) is fixedly connected with a scraping plate (306), the scraping plates (306) are in contact with the inner wall of the kettle body (1), a group of fixed plates (307) are fixedly connected with the outer surface of the fixed disc (304), connecting columns (308) are fixedly connected with the bottom surface of each fixed plate (307), and gears (309) are rotatably connected with the bottom ends of the connecting columns (308);
The bottom surface of every gear one (309) all fixedly connected with carrier bar (310), every the surface of carrier bar (310) all fixedly connected with a set of stirring vane (311), the surface mounting of rotary cylinder (301) has a set of one-way shower nozzle (312).
2. The reaction kettle for hydrazinization production of bifenazate according to claim 1, which is characterized in that: the inner wall of the kettle body (1) is fixedly connected with a toothed ring (4), and the first gear (309) is meshed with the toothed ring (4).
3. The reaction kettle for hydrazinization production of bifenazate according to claim 1, which is characterized in that: the upper surface of axe cover (2) is equipped with motor (5), the output of motor (5) fixedly connected with belt pulley two (6), belt pulley two (6) are connected with belt pulley one (302) transmission through the belt.
4. The reaction kettle for hydrazinization production of bifenazate according to claim 1, which is characterized in that: the outer surface of the kettle body (1) is communicated with a feeding pipe (7), and the bottom surface of the kettle body (1) is communicated with a discharging pipe (8).
5. The reaction kettle for hydrazinization production of bifenazate according to claim 1, which is characterized in that: the outer surface of the kettle body (1) is fixedly connected with a supporting table (9), and the bottom surface of the supporting table (9) is fixedly connected with four supporting legs (10).
6. The reaction kettle for hydrazinization production of bifenazate according to claim 1, which is characterized in that: the kettle is characterized in that a water pump (11) is arranged below the kettle body (1), the output end of the water pump (11) is communicated with a water delivery pipe (12), and the water delivery pipe (12) is rotationally connected to the inner wall of the water pipe connector (303).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202420012629.7U CN221656584U (en) | 2024-01-03 | 2024-01-03 | Be used for hydrazine ester hydrazine production of biphenyl reation kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202420012629.7U CN221656584U (en) | 2024-01-03 | 2024-01-03 | Be used for hydrazine ester hydrazine production of biphenyl reation kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN221656584U true CN221656584U (en) | 2024-09-06 |
Family
ID=92582712
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202420012629.7U Active CN221656584U (en) | 2024-01-03 | 2024-01-03 | Be used for hydrazine ester hydrazine production of biphenyl reation kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN221656584U (en) |
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2024
- 2024-01-03 CN CN202420012629.7U patent/CN221656584U/en active Active
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