CN220759216U - Acid halide aftertreatment device - Google Patents
Acid halide aftertreatment device Download PDFInfo
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- CN220759216U CN220759216U CN202322449538.8U CN202322449538U CN220759216U CN 220759216 U CN220759216 U CN 220759216U CN 202322449538 U CN202322449538 U CN 202322449538U CN 220759216 U CN220759216 U CN 220759216U
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- acid halide
- water washing
- reactor
- treatment
- filter
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- 239000002253 acid Substances 0.000 title claims abstract description 72
- 150000004820 halides Chemical class 0.000 title claims abstract description 66
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 37
- 238000004821 distillation Methods 0.000 claims abstract description 35
- 238000005406 washing Methods 0.000 claims abstract description 32
- 238000006386 neutralization reaction Methods 0.000 claims abstract description 30
- 239000000126 substance Substances 0.000 claims abstract description 23
- 238000002425 crystallisation Methods 0.000 claims abstract description 21
- 230000008025 crystallization Effects 0.000 claims abstract description 21
- 239000011541 reaction mixture Substances 0.000 claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 8
- 239000012535 impurity Substances 0.000 claims abstract description 8
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 4
- 230000001737 promoting effect Effects 0.000 claims abstract description 4
- 238000000926 separation method Methods 0.000 claims abstract description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 18
- 238000003860 storage Methods 0.000 claims description 18
- 239000002351 wastewater Substances 0.000 claims description 12
- 238000005086 pumping Methods 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims 2
- 239000000047 product Substances 0.000 abstract description 18
- 238000000034 method Methods 0.000 description 9
- 230000002378 acidificating effect Effects 0.000 description 6
- 239000004480 active ingredient Substances 0.000 description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000575 pesticide Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 230000000274 adsorptive effect Effects 0.000 description 1
- 229940035676 analgesics Drugs 0.000 description 1
- 239000000730 antalgic agent Substances 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000002260 anti-inflammatory agent Substances 0.000 description 1
- 229940121363 anti-inflammatory agent Drugs 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000004009 herbicide Substances 0.000 description 1
- -1 hydroxide ions Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 239000012264 purified product Substances 0.000 description 1
- 230000037072 sun protection Effects 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses an acid halide post-treatment device, which relates to the technical field of acid halide treatment equipment and comprises a reactor, a water washing device, a distillation tower, a neutralization reactor, a filter and a crystallization device, wherein the reactor is used for containing a reaction mixture containing acid halide, the reaction mixture is sequentially treated by the water washing device, the distillation tower, the neutralization reactor, the filter and the crystallization device, the water washing device is used for carrying out water washing treatment on the reaction mixture, the distillation tower is used for carrying out distillation separation on the acid halide after water washing and moisture, the neutralization reactor is used for carrying out reaction neutralization on the distilled acid halide and alkaline substances, the filter is used for further filtering impurities in the reaction product, and the crystallization device is used for promoting crystallization of the acid halide in the crystallizer. The acid halide post-treatment device provided by the utility model can improve the acid halide post-treatment efficiency and the product quality.
Description
Technical Field
The utility model relates to the technical field of acid halide treatment equipment, in particular to an acid halide post-treatment device.
Background
Acid halides are a compound containing halogen atoms and acid groups, an important chemical, they are widely used in chemistry and industry, they have wide biological activities, and they play an important role in different industries. In the agricultural field, acid halides are widely used as active ingredients of pesticides, as pesticides, bactericides and herbicides, which can effectively control pests, pathogens and weeds, and improve crop yield and quality; in the medical field, acid halides are important components of many drugs, as antibiotics, analgesics and anti-inflammatory agents, which are used in the treatment of various diseases and symptoms, playing a key role in maintaining human health; in the cosmetic industry, acid halides are used as active ingredients in products such as sun cream, toning lotion, emulsion and the like, which can provide functions of moisturizing, antioxidation, sun protection and the like and help to maintain the health and beauty of skin; in the food industry, acid halides are also active ingredients of some food additives, such as preservatives, antioxidants and emulsifiers, which can extend the shelf life of the food, improve the mouthfeel and stabilize the texture of the food; in addition, acid halides are also used as active ingredients in industrial chemicals, such as solvents, plastics and fuels. They play a key role in industrial production, supporting the manufacturing and production processes of various products. Acid halides may also present a certain risk of toxicity. Therefore, when acid halides are applied, safety regulations must be strictly followed, and appropriate safeguards must be taken to ensure the effectiveness of the application and the safety of the procedure. With proper use and handling, acid halides will continue to play an important role in various areas.
However, the work-up of acid halides generally has a number of problems such as low product purity, low processing efficiency, complex operation, etc. Thus, a new type of post-treatment system is needed to improve acid halide post-treatment efficiency and product quality.
Disclosure of Invention
The utility model aims to provide an acid halide post-treatment device which solves the problems in the prior art and improves the acid halide post-treatment efficiency and the product quality.
In order to achieve the above object, the present utility model provides the following solutions:
the utility model provides an acid halide post-treatment device which comprises a reactor, a water washing device, a distillation tower, a neutralization reactor, a filter and a crystallization device, wherein the reactor is used for containing a reaction mixture containing acid halide, the reaction mixture is sequentially treated by the water washing device, the distillation tower, the neutralization reactor, the filter and the crystallization device, the water washing device is used for carrying out water washing treatment on the reaction mixture, the distillation tower is used for carrying out distillation separation on the acid halide after water washing and moisture, the neutralization reactor is used for carrying out reaction neutralization on the distilled acid halide and alkaline substances, the filter is used for further filtering impurities in a reaction product, and the crystallization device is used for promoting crystallization of the acid halide in the crystallizer.
Preferably, the distillation tower further comprises a vacuum pump for pumping out the gas in the distillation tower.
Preferably, the apparatus further comprises a waste water storage tank, and waste water generated by the reactor, the distillation tower, the filter and the neutralization reactor is discharged to the waste water storage tank for storage.
Preferably, the filter is an activated carbon filter.
Preferably, the reaction mixture washing device further comprises an alkaline substance storage tank, wherein the alkaline substance storage tank is used for storing alkaline substances, and the alkaline substances are added when the reaction mixture is subjected to washing treatment by the washing device.
Compared with the prior art, the utility model has the following technical effects:
the acid halide post-treatment device provided by the utility model effectively removes acid residues and organic impurities through multi-step treatment processes including water washing, distillation, neutralization reaction, filtration, crystallization purification and the like, and greatly improves the purity of the product. The system is reasonable in design, and the safety and stability of operation are ensured through measures such as distillation, neutralization and filtration. The operation flow is simple and easy, and the method is suitable for acid halide treatment with different scales and types, and is economical and practical. Therefore, the device provides an efficient, safe and economical solution for the acid halide post-treatment process, and ensures the high purity and high-quality chemical quality of the product.
Drawings
In order to more clearly illustrate the embodiments of the present utility model or the technical solutions in the prior art, the drawings that are needed in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present utility model, and other drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a block diagram of an acid halide post-treatment apparatus provided in an embodiment of the present utility model;
in the figure: 1-a reactor; 2-a water washing device; 3-a distillation column; 4-a vacuum pump; 5-a waste water storage tank; 6-a neutralization reactor; 7-an activated carbon filter; 8-a storage tank; 9-a crystallization device; 10-alkaline substance storage tank.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
The utility model aims to provide an acid halide post-treatment device which solves the problems in the prior art and improves the acid halide post-treatment efficiency and the product quality.
In order that the above-recited objects, features and advantages of the present utility model will become more readily apparent, a more particular description of the utility model will be rendered by reference to the appended drawings and appended detailed description.
The utility model provides an acid halide post-treatment device, which is shown in figure 1 and comprises a reactor 1, a water washing device 2, a distillation tower 3, a neutralization reactor 6, a filter and a crystallization device 9, wherein the reactor 1 is used for containing a reaction mixture containing acid halide, the reaction mixture is sequentially treated by the water washing device 2, the distillation tower 3, the neutralization reactor 6, the filter and the crystallization device 9, the water washing device 2 is used for carrying out water washing treatment on the reaction mixture, the distillation tower 3 is used for carrying out distillation separation on the acid halide after water washing and moisture, the neutralization reactor 6 is used for carrying out reaction neutralization on the distilled acid halide and alkaline substances, the filter is used for further filtering impurities in a reaction product, and the crystallization device 9 is used for promoting crystallization of the acid halide in the crystallizer.
The filter is an activated carbon filter 7, and other types of filters may be used in other embodiments.
The reaction mixture obtained after the reaction in the reactor 1 is passed to a water washing apparatus 2 for water washing for the purpose of removing acidic residues in the reaction mixture. When the acid halide is contacted with water, the acid groups in the acidic residue react with hydroxide ions (OH-) in the water to form a water soluble salt or acidic species. These water-soluble substances will dissolve from the mixture into the aqueous phase, thereby effecting the removal of the acidic residue, and the eluted mixture of the acid halide and the residual moisture is distilled off by the distillation column 3. Since the acid halide and water have different boiling points, the acid halide and water can be separated by heating the mixture and fractionating it in the distillation column 3. The purified acid halide is obtained after distillation, and the distilled acid halide is further subjected to neutralization reaction with an alkaline substance in a neutralization reactor 6, wherein the neutralization reaction aims at removing excessive acidic components in a distillation product, and in the neutralization reaction, the alkaline substance (such as sodium hydroxide or potassium hydroxide) reacts with acid groups in the acid halide to generate corresponding salt and water. Thus, the excess acidic component is neutralized to obtain a purer acid halide, and after the neutralization reaction, the product is further purified by the activated carbon filter 7. Activated carbon is a highly adsorptive material that adsorbs organics, including impurities of some acid halides. Residual organic impurities can be further removed by passing the product through an activated carbon filter 7, increasing the purity of the product- > finally, the product is purified by a crystallization device 9. By controlling the temperature and solvent conditions, the acid halide can be promoted to crystallize in a crystallizer, so that a purified product is separated, and crystallization is an effective purification method, and the purity and quality of the product can be further improved.
The acid halide post-treatment device provided by the utility model effectively removes acid residues and organic impurities through multi-step treatment processes including water washing, distillation, neutralization reaction, filtration, crystallization purification and the like, and greatly improves the purity of the product. The system is reasonable in design, and the safety and stability of operation are ensured through measures such as distillation, neutralization and filtration. The operation flow is simple and easy, and the method is suitable for acid halide treatment with different scales and types, and is economical and practical. Therefore, the device provides an efficient, safe and economical solution for the acid halide post-treatment process, and ensures the high purity and high-quality chemical quality of the product.
In some embodiments, in order to improve distillation efficiency and stability of materials, the embodiment further includes a vacuum pump 4, where the vacuum pump 4 is used to pump out gas in the distillation tower 3, and is used to provide vacuum conditions during distillation, reduce reaction temperature, and avoid decomposition of products. When the acid halide is distilled and separated from the water, the water is first converted into steam and then distilled, and the acid halide distillation product is introduced into the neutralization reactor 6.
In some embodiments, in order to uniformly collect and post-treat the wastewater, the embodiment further comprises a wastewater storage tank 5, and the wastewater generated by the reactor 1, the distillation tower 3, the filter and the neutralization reactor 6 is discharged to the wastewater storage tank 5 for storage.
The activated carbon in the activated carbon filter 7 can be recovered and used for wastewater treatment in the wastewater tank 5. In some embodiments, the reaction vessel further comprises an alkaline substance storage tank 10, the alkaline substance storage tank 10 is used for storing alkaline substances, and the alkaline substances are added when the reaction mixture is subjected to water washing treatment by the water washing device 2.
The principles and embodiments of the present utility model have been described in detail with reference to specific examples, which are provided to facilitate understanding of the method and core ideas of the present utility model; also, it is within the scope of the present utility model to be modified by those of ordinary skill in the art in light of the present teachings. In view of the foregoing, this description should not be construed as limiting the utility model.
Claims (5)
1. An acid halide aftertreatment device, characterized in that: the acid halide acid and alkali reaction device comprises a reactor, a water washing device, a distillation tower, a neutralization reactor, a filter and a crystallization device, wherein the reactor is used for containing a reaction mixture containing the acid halide, the reaction mixture is sequentially treated by the water washing device, the distillation tower, the neutralization reactor, the filter and the crystallization device, the water washing device is used for carrying out water washing treatment on the reaction mixture, the distillation tower is used for carrying out distillation separation on the acid halide after water washing and moisture, the neutralization reactor is used for carrying out reaction neutralization on the distilled acid halide and alkali substances, the filter is used for further filtering impurities in a reaction product, and the crystallization device is used for promoting crystallization of the acid halide in the crystallizer.
2. The acid halide post-treatment device according to claim 1, wherein: and a vacuum pump for pumping out the gas in the distillation column.
3. The acid halide post-treatment device according to claim 1, wherein: the device also comprises a waste water storage tank, wherein waste water generated by the reactor, the distillation tower, the filter and the neutralization reactor is discharged into the waste water storage tank for storage.
4. The acid halide post-treatment device according to claim 1, wherein: the filter is an activated carbon filter.
5. The acid halide post-treatment device according to claim 1, wherein: the device is characterized by further comprising an alkaline substance storage tank, wherein the alkaline substance storage tank is used for storing alkaline substances, and the alkaline substances are added when the water washing device carries out water washing treatment on the reaction mixture.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322449538.8U CN220759216U (en) | 2023-09-08 | 2023-09-08 | Acid halide aftertreatment device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322449538.8U CN220759216U (en) | 2023-09-08 | 2023-09-08 | Acid halide aftertreatment device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220759216U true CN220759216U (en) | 2024-04-12 |
Family
ID=90599925
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202322449538.8U Active CN220759216U (en) | 2023-09-08 | 2023-09-08 | Acid halide aftertreatment device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220759216U (en) |
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2023
- 2023-09-08 CN CN202322449538.8U patent/CN220759216U/en active Active
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