CN220159956U - Reaction kettle for producing 5-chlorovaleryl chloride - Google Patents
Reaction kettle for producing 5-chlorovaleryl chloride Download PDFInfo
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- CN220159956U CN220159956U CN202321380659.5U CN202321380659U CN220159956U CN 220159956 U CN220159956 U CN 220159956U CN 202321380659 U CN202321380659 U CN 202321380659U CN 220159956 U CN220159956 U CN 220159956U
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- reaction kettle
- kettle device
- main body
- device main
- producing
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 124
- SVNNWKWHLOJLOK-UHFFFAOYSA-N 5-chloropentanoyl chloride Chemical compound ClCCCCC(Cl)=O SVNNWKWHLOJLOK-UHFFFAOYSA-N 0.000 title claims abstract description 18
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 34
- 238000003756 stirring Methods 0.000 claims abstract description 26
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 abstract description 19
- 229910052799 carbon Inorganic materials 0.000 abstract description 14
- 239000002351 wastewater Substances 0.000 abstract description 4
- 229910052801 chlorine Inorganic materials 0.000 abstract description 3
- 239000000460 chlorine Substances 0.000 abstract description 3
- 238000007599 discharging Methods 0.000 abstract 1
- 238000009434 installation Methods 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 description 5
- 230000007062 hydrolysis Effects 0.000 description 4
- 238000001179 sorption measurement Methods 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- XGISHOFUAFNYQF-UHFFFAOYSA-N pentanoyl chloride Chemical compound CCCCC(Cl)=O XGISHOFUAFNYQF-UHFFFAOYSA-N 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- JVSFQJZRHXAUGT-UHFFFAOYSA-N 2,2-dimethylpropanoyl chloride Chemical compound CC(C)(C)C(Cl)=O JVSFQJZRHXAUGT-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000011897 real-time detection Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a reaction kettle for producing 5-chlorovaleryl chloride, which comprises a reaction kettle device main body and a reaction mechanism. The utility model discloses a reaction kettle for producing chloropenta-chlorine, which can be used for pouring materials into the reaction kettle device body from a material inlet arranged above the reaction kettle device body, connecting a rotating shaft and a stirring rod to form a selective installation structure through a motor arranged in the center above the reaction kettle device body, driving the stirring rod to normally operate, rapidly heating through a heating rod arranged in the reaction kettle device body, thereby improving the reaction rate, and re-installing active carbon in the reaction kettle device body, realizing the treatment of waste water by adsorbing organic matters in the waste water through the active carbon bed layer, and discharging the filtered materials through a material outlet arranged below the reaction kettle device body.
Description
Technical Field
The utility model relates to the technical field of n-pentanoyl chloride, in particular to a reaction kettle for producing 5-chloropentanoyl chloride.
Background
The hydrolysis reaction is a reverse reaction of neutralization or esterification reaction, a hydrolysis kettle is used for hydrolysis of organic matters in industry, alcohol and phenol are mainly produced, the hydrolysis kettle is often needed in the production process of n-pentanoyl chloride, and a steam inlet and a discharge hole are generally arranged at the bottom of the hydrolysis kettle in a traditional structure.
Through searching, the patent with the publication number of CN204602196U discloses a reaction kettle used in a process of producing pivaloyl chloride, and the reaction kettle comprises a kettle body, wherein the top of the kettle body is provided with a feed inlet, the bottom of the kettle body is provided with a discharge outlet, the discharge outlet is connected with a discharge filtering device, the inner wall of the kettle body is provided with a guide groove, the inside of the kettle body is provided with a stirring device, the stirring device is connected with a driving motor, the stirring device comprises a stirring shaft, a sleeve and a telescopic rod for pushing and pulling the sleeve are slidably arranged in the middle of the stirring shaft, a main blade is arranged at the bottom of the stirring shaft, two auxiliary blades are respectively arranged at two ends of the main blade, the auxiliary blades are connected with the sleeve through an adjusting rod, and the right side of the kettle body is provided with a sampling device which comprises a delivery pipe and a sampling pipe. "although the stirring device in the apparatus described above can improve the stirring efficiency, the apparatus described above does not have a heating device and cannot detect and control the temperature inside the reaction vessel in real time.
Disclosure of Invention
The utility model aims to provide a reaction kettle for producing 5-chlorovaleryl chloride, which is used for solving the problems that in the prior art, a stirring device in the equipment can improve stirring efficiency, but the equipment in the content is not provided with a heating device and the temperature inside the reaction kettle cannot be detected and controlled in real time.
In order to solve the technical problems, the utility model provides a reaction kettle for producing 5-chlorovaleryl chloride, which comprises a reaction kettle device main body and a reaction mechanism, wherein an exhaust port is arranged above the reaction kettle device main body, a support column is arranged below the reaction kettle device main body, a feeding port is arranged above the reaction kettle device main body, a motor is arranged in the center of the upper part of the reaction kettle device main body, a rotating shaft is connected inside the motor, and the reaction mechanism is arranged inside the reaction kettle device main body.
Preferably, the exhaust port and the reaction kettle device body are welded, and the exhaust port and the reaction kettle device body form a fixed structure.
Preferably, the support column is welded with the main body of the reaction kettle device, and the support column is tightly attached to the main body of the reaction kettle device.
Preferably, the feed inlet is installed to the top of reation kettle device main part, the motor is installed to the top central authorities of reation kettle device main part, the internal connection of motor has the pivot, the stirring rod is installed in the outside of pivot, the internally mounted of reation kettle device main part has the stick that generates heat, the internally mounted of reation kettle device main part has the active carbon, the discharge gate is installed to the below of reation kettle device main part, the controller is installed to the top of reation kettle device main part.
Preferably, the motor is connected with the rotating shaft and the stirring rod to form a rotating structure, and the inner diameter size of the motor is matched with the outer diameter size of the rotating shaft.
Preferably, the heating rods are connected with the main body of the reaction kettle device through screws, and the heating rods are in one-to-one correspondence with the main body of the reaction kettle device.
Preferably, the discharge hole is welded with the main body of the reaction kettle device, and the discharge hole is arranged below the main body of the reaction kettle device.
Preferably, the controller is connected with the main body of the reaction kettle device through screws, and the controller is arranged above the main body of the reaction kettle device.
Compared with the related art, the reaction kettle for producing the 5-chlorovaleryl chloride has the following beneficial effects:
the utility model provides a reaction kettle for producing 5-chlorovaleryl chloride, which is characterized in that a material can be placed into the reaction kettle device body for reaction through a material inlet arranged above the reaction kettle device body, then a rotating structure is formed by connecting a rotating shaft and a stirring rod through a motor arranged in the center above the reaction kettle device body, so that the stirring rod is driven to normally operate, meanwhile, the material can be uniformly stirred, and then can be quickly heated through a heating rod arranged outside the rotating shaft, so that the reaction rate is improved, activated carbon arranged in the reaction kettle again can be utilized to separate a product from the reaction mixture through an activated carbon bed by utilizing the adsorption effect of the activated carbon on certain substances, the purity and quality of the product are improved, and the waste water can be adsorbed by passing through the activated carbon bed layer, so that the activated carbon has higher adsorption effect on pollutants, and the treatment of organic matters in the waste water can be realized.
Through the discharge gate of installing in reation kettle device main part below, can pass through this discharge gate with pure material after filtering and discharge, then through the controller of installing in reation kettle device main part top, can carry out real-time detection and control to the inside temperature of reation kettle device main part.
Drawings
FIG. 1 is a perspective view of a main body of a reaction kettle device of the present utility model;
FIG. 2 is a cross-sectional view of the main body of the reactor device of the present utility model;
FIG. 3 is a front view showing a cross section of the main body of the reactor apparatus of the present utility model;
FIG. 4 is a top view of the main body of the reactor device of the present utility model.
Reference numerals in the drawings: 1. a reaction kettle device main body; 2. an exhaust port; 3. a support column; 4. a reaction mechanism; 401. a feed inlet; 402. a motor; 403. a rotating shaft; 404. a stirring rod; 405. a heating rod; 406. activated carbon; 407. a discharge port; 408. and a controller.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and fully with reference to the accompanying drawings, in which it is evident that the embodiments described are only some, but not all embodiments of the utility model; all other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
An embodiment I, given by FIGS. 1-4, the present utility model provides a technical solution: the utility model provides a reation kettle is used in production of 5-chlorovaleryl chloride, includes reation kettle device main part 1 and reaction mechanism 4, and gas vent 2 is installed to reation kettle device main part 1's top, and support column 3 is installed to reation kettle device main part 1's below, and pan feeding mouth 401 is installed to reation kettle device main part 1's top, and motor 402 is installed to reation kettle device main part 1's top central authorities, and motor 402's internal connection has pivot 403, and reation kettle device main part 1's inside is equipped with reaction mechanism 4.
In the second embodiment, the exhaust port 2 and the reaction kettle device body 1 are welded, the exhaust port 2 and the reaction kettle device body 1 form a fixed structure, and the exhaust port 2 is installed to control the gas emission in the reaction process.
In the third embodiment, the support column 3 is welded with the main body 1 of the reaction kettle device, the support column 3 is tightly attached to the main body 1 of the reaction kettle device, and the main body 1 of the reaction kettle device can be supported and fixed by installing the support column 3.
In the fourth embodiment, the feed inlet 401 is installed above the reaction kettle device body 1, the motor 402 is installed in the center above the reaction kettle device body 1, the rotating shaft 403 is connected with the motor 402, the stirring rod 404 is installed on the outer side of the rotating shaft 403, the heating rod 405 is installed inside the reaction kettle device body 1, the activated carbon 406 is installed inside the reaction kettle device body 1, the discharge outlet 407 is installed below the reaction kettle device body 1, the controller 408 is installed above the reaction kettle device body 1, the materials can be poured into the reaction kettle device body 1 through the feed inlet 401, then the motor 402 is installed in the center above the reaction kettle device body 1, a rotating structure is formed by connecting the rotating shaft 403 with the stirring rod 404, so that the stirring rod 404 is driven to operate, meanwhile, the materials can be uniformly stirred under the driving of the rotating shaft 403, the heating rod 405 installed inside the reaction kettle device body 1 can be heated rapidly, the reaction kettle body 1 can be heated up again, the reaction kettle body can be installed at a high speed, the inner side of the reaction kettle body can be separated from the activated carbon 406 by the activated carbon 406, the quality of the reaction kettle body can be separated from the reaction kettle body 1 by the active carbon in the inside the reaction kettle device body 1 through the control of the controller, the quality of the reaction kettle device can be separated from the active carbon body 1, and the quality of the reaction kettle device can be separated from the active carbon can be discharged from the active carbon body by the active carbon in the active carbon body by the inside the device through the control of the device, and the active carbon body in the inside the reaction kettle device body 1 can be separated by the active carbon can be separated.
In the fifth embodiment, the motor 402 is connected to the rotating shaft 403 and the stirring rod 404 to form a rotating structure, the inner diameter of the motor 402 is matched with the outer diameter of the rotating shaft 403, and the motor 402 is installed to form a rotating structure by connecting the rotating shaft 403 and the stirring rod 404, so as to drive the stirring rod 404 to operate.
In the sixth embodiment, the heating rods 405 are connected with the reaction kettle device body 1 by screws, the heating rods 405 are in one-to-one correspondence with the reaction kettle device body 1, and rapid heating can be realized by installing the heating rods 405, so that the reaction rate is improved.
In the seventh embodiment, the material outlet 407 is welded to the reaction kettle device body 1, and the material outlet 407 is installed below the reaction kettle device body 1, so that the filtered material can be discharged by installing the material outlet 407.
In the eighth embodiment, the controller 408 is connected with the main body 1 of the reaction kettle device by screws, the controller 408 is installed above the main body 1 of the reaction kettle device, and the temperature inside the main body 1 of the reaction kettle device can be detected and controlled in real time by installing the controller 408.
Working principle: for a reaction kettle for producing 5-chlorovaleryl chloride, firstly, the material can be poured into the reaction kettle device body 1 through a feed inlet 401 arranged above the reaction kettle device body 1, then the material can be separated from the reaction mixture through the adsorption of the active carbon 406 to certain substances by a motor 402 arranged in the center above the reaction kettle device body 1, the purity and the quality of the product are improved by a discharge port 407 arranged below the reaction kettle device body 1, the filtered material can be discharged from the reaction kettle device body by a stirring rod 404 arranged outside the rotating shaft 403, the material can be uniformly stirred under the driving of the rotating shaft 403, and then the rapid heating can be realized by a heating rod 405 arranged inside the reaction kettle device body 1, so that the reaction rate is improved, and then the active carbon 406 is arranged inside the reaction kettle device body 1 again, the product purity and the quality of the product are improved by the adsorption of the active carbon 406, and finally the filtered material can be discharged by the discharge port 407 arranged below the reaction kettle device body 1, and finally the temperature of the reaction kettle device can be controlled by a controller arranged above the reaction kettle device body 1, so that the inside of the reaction kettle can be controlled to produce the chlorine, and the reaction kettle 1 can be used for producing the chlorine in real time.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the spirit and scope of the utility model as defined by the appended claims and their equivalents.
Claims (8)
1. The utility model provides a reaction kettle for 5-chlorovaleryl chloride production, includes reation kettle device main part (1) and reaction mechanism (4), its characterized in that: the reactor comprises a reactor device body (1), wherein an exhaust port (2) is arranged above the reactor device body (1), a support column (3) is arranged below the reactor device body (1), a feeding port (401) is arranged above the reactor device body (1), a motor (402) is arranged in the center of the upper part of the reactor device body (1), a rotating shaft (403) is connected to the motor (402), and a reaction mechanism (4) is arranged inside the reactor device body (1).
2. The reaction kettle for producing 5-chlorovaleryl chloride according to claim 1, wherein the exhaust port (2) and the reaction kettle device main body (1) are welded, and the exhaust port (2) and the reaction kettle device main body (1) form a fixed structure.
3. The reaction kettle for producing 5-chlorovaleryl chloride according to claim 1, wherein the support column (3) is welded with the reaction kettle device main body (1), and the support column (3) is tightly attached with the reaction kettle device main body (1).
4. The reaction kettle for producing 5-chlorovaleryl chloride according to claim 1, wherein a feed inlet (401) is arranged above the reaction kettle device main body (1), a motor (402) is arranged in the center above the reaction kettle device main body (1), a rotating shaft (403) is connected to the motor (402), a stirring rod (404) is arranged on the outer side of the rotating shaft (403), a heating rod (405) is arranged inside the reaction kettle device main body (1), activated carbon (406) is arranged inside the reaction kettle device main body (1), a discharge outlet (407) is arranged below the reaction kettle device main body (1), and a controller (408) is arranged above the reaction kettle device main body (1).
5. The reaction kettle for producing 5-chlorovaleryl chloride of claim 4, wherein the motor (402) is connected with a rotating shaft (403) and a stirring rod (404) to form a rotating structure, and the inner diameter size of the motor (402) is matched with the outer diameter size of the rotating shaft (403).
6. The reaction kettle for producing 5-chlorovaleryl chloride according to claim 4, wherein the heating rods (405) are connected with the reaction kettle device main body (1) by screws, and the heating rods (405) are in one-to-one correspondence with the reaction kettle device main body (1).
7. The reaction kettle for producing 5-chlorovaleryl chloride of claim 4, wherein the discharge port (407) is welded with the reaction kettle device main body (1), and the discharge port (407) is installed below the reaction kettle device main body (1).
8. The reaction kettle for producing 5-chlorovaleryl chloride of claim 4, wherein the controller (408) is connected with the reaction kettle device main body (1) by screws, and the controller (408) is arranged above the reaction kettle device main body (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321380659.5U CN220159956U (en) | 2023-06-01 | 2023-06-01 | Reaction kettle for producing 5-chlorovaleryl chloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321380659.5U CN220159956U (en) | 2023-06-01 | 2023-06-01 | Reaction kettle for producing 5-chlorovaleryl chloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220159956U true CN220159956U (en) | 2023-12-12 |
Family
ID=89067583
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321380659.5U Active CN220159956U (en) | 2023-06-01 | 2023-06-01 | Reaction kettle for producing 5-chlorovaleryl chloride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220159956U (en) |
-
2023
- 2023-06-01 CN CN202321380659.5U patent/CN220159956U/en active Active
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