CN219848270U - Oil-water separator for catalyst production - Google Patents
Oil-water separator for catalyst production Download PDFInfo
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- CN219848270U CN219848270U CN202320894788.XU CN202320894788U CN219848270U CN 219848270 U CN219848270 U CN 219848270U CN 202320894788 U CN202320894788 U CN 202320894788U CN 219848270 U CN219848270 U CN 219848270U
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- separation
- fixedly connected
- tower
- floating plate
- oil
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 53
- 239000003054 catalyst Substances 0.000 title claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 17
- 238000000926 separation method Methods 0.000 claims abstract description 89
- 238000006243 chemical reaction Methods 0.000 claims abstract description 30
- 238000007599 discharging Methods 0.000 claims abstract 2
- 238000003756 stirring Methods 0.000 claims description 23
- 238000001179 sorption measurement Methods 0.000 claims description 19
- 238000010521 absorption reaction Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 abstract description 31
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 abstract description 14
- 150000002148 esters Chemical class 0.000 abstract description 9
- 235000013773 glyceryl triacetate Nutrition 0.000 abstract description 7
- 239000001087 glyceryl triacetate Substances 0.000 abstract description 7
- 238000012545 processing Methods 0.000 abstract description 7
- 229960002622 triacetin Drugs 0.000 abstract description 7
- 238000012993 chemical processing Methods 0.000 abstract description 2
- 150000002632 lipids Chemical class 0.000 description 9
- 239000004519 grease Substances 0.000 description 5
- 239000012535 impurity Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Landscapes
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
The utility model relates to the technical field of chemical processing and discloses an oil-water separator for catalyst production, which comprises a reaction tower and a separation tower, wherein a condenser is fixedly connected to the outer surface of the reaction tower, a first pump body is fixedly connected to the outer surface of the separation tower, a first guide pipe is fixedly connected between the condenser and the first pump body, a discharging pipe is fixedly connected to the bottom surface of the separation tower, a negative pressure machine is fixedly connected to the upper end surface of the reaction tower, a motor is fixedly connected to the upper end surface of the separation tower, a second guide pipe is fixedly connected to the upper end surface of the negative pressure machine, a sliding pipe is slidingly connected to the outer side of the upper end surface of the separation tower, a filter plate is fixedly connected to the lower side of the inner wall of the separation tower, and a side guide groove is formed in the inner wall of the separation tower. The oil-water separator for catalyst production can be used for carrying out reaction processing on the glyceryl triacetate through a reaction tower, and can be used for carrying out high-efficiency separation on oil and water on the surface of ester liquid after ester water separation through a separation tower.
Description
Technical Field
The utility model relates to the technical field of chemical processing, in particular to an oil-water separator for catalyst production.
Background
In the process of processing the glyceryl triacetate, after the ester liquid with higher water content obtained at the top of the ester-water separation tower is condensed, oil-water separation is needed, so that an oil-water separator is used, and the existing oil-water separator is inconvenient to separate an oil layer from water efficiently and rapidly when separating the oil layer on the liquid surface, so that the processing efficiency of oil-water separation is reduced.
Disclosure of Invention
Aiming at the defects of the prior art, the utility model provides an oil-water separator for catalyst production, which solves the problem that an oil layer on a liquid surface is inconvenient to be separated from water efficiently and rapidly when glyceryl triacetate is processed.
In order to achieve the aim of conveniently and efficiently separating an oil layer on a liquid surface from water during processing of the glyceryl triacetate, the utility model provides the following technical scheme: the utility model provides an oil-water separator for catalyst production, includes reaction tower and knockout tower, the surface fixedly connected with condenser of reaction tower, the surface fixedly connected with first pump body of knockout tower, fixedly connected with first pipe between condenser and the first pump body, the bottom surface fixedly connected with row material pipe of knockout tower, the up end fixedly connected with negative pressure machine of reaction tower, the up end fixedly connected with motor of knockout tower, the up end fixedly connected with second pipe of negative pressure machine, the up end outside sliding connection of knockout tower has the downslide tube, and second pipe and downslide tube sliding connection, the inner wall downside fixedly connected with filter plate of knockout tower, the side guide slot has been seted up to the inner wall of knockout tower;
the inside sliding connection of separator has the separation floating plate, the inside of separation floating plate rotates and is connected with sealed cover that changes, the absorption chamber has been seted up to the inside of separation floating plate, the absorption hole has been seted up to the downside surface of separation floating plate, the output of motor is located the inside fixedly connected with drive shaft of separator, and the separation floating plate passes through sealed cover that changes to rotate with the drive shaft and be connected, the outer spring has been cup jointed in the outside of drive shaft, the lateral groove has been seted up to the surface of drive shaft, the inside fixedly connected with interior axle of lateral groove, interior axle's surface sliding connection has the puddler, interior spring has been cup jointed on interior axle's surface.
Preferably, the stirring rods are axially provided with three groups along the driving shaft, the stirring rod at the lowest side is fixedly connected with the driving shaft, the stirring rods at the upper side are slidably connected with the side grooves, and an inner spring is arranged between every two adjacent stirring rods.
Preferably, the separation floating plate is in a shape of a circular truncated cone, and the upper end and the lower end of the outer spring are contacted with the separation tower and the separation floating plate.
Preferably, the sliding tube penetrates through the separation floating plate and extends to the inside of the adsorption cavity, the sliding tube is fixedly connected with the separation floating plate, and the sliding tube, the adsorption cavity and the adsorption hole are communicated.
Preferably, the two ends of the separation floating plate are fixedly connected with sliding blocks, and the separation floating plate is axially and slidably connected with the separation tower through the sliding blocks and the side guide grooves.
Preferably, the bottom surface of the inside of the separation tower is arc-shaped, and one end of the inner side of the first conduit penetrates through the separation tower and is positioned above the filter plate.
Compared with the prior art, the utility model provides the oil-water separator for catalyst production, which has the following beneficial effects:
1. the oil-water separator for catalyst production can be used for carrying out reaction processing on triacetin through a reaction tower, and can be used for conveying ester liquid after gas liquefaction in the reaction tower into a first guide pipe through a condenser, and can be used for conveying the ester liquid into a separation tower through a first pump body, a motor can drive a stirring rod to rotate through a driving shaft, so that the grease is dispersed, solid impurities in the grease are sunk and discharged through a discharge pipe, and when the stirring rod stirs the grease, the liquid level of the grease can be in a vortex shape, and an oil layer in the grease floats on the liquid level at the moment, so that the oil and water can be layered.
2. The oil-water separator for catalyst production is characterized in that along with the increase of the amount of fat water in a reaction tower, the liquid level of the fat water is raised and is contacted with the bottom surface of a separation floating plate, the liquid level has upward thrust to the separation floating plate, then a negative pressure machine can provide negative pressure for the inside of an adsorption cavity through a second conduit and a down slide pipe, an oil layer on the liquid level of the fat water can be adsorbed through an adsorption hole, and the oil layer on the upper layer of the liquid level can be conveyed into the reaction tower again through the second conduit and the down slide pipe, so that only water on the layer is left in the separation tower.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is a partial cross-sectional view of a structural separation column of the present utility model;
FIG. 3 is a partial cross-sectional view of a structural separation floating plate of the present utility model;
fig. 4 is a partial cross-sectional view of a drive shaft of the present utility model.
Wherein: 1. a reaction tower; 2. a separation tower; 3. a condenser; 4. a first pump body; 5. a first conduit; 6. a discharge pipe; 7. a negative pressure machine; 8. a motor; 9. a second conduit; 10. a down slide tube; 11. a filter plate; 12. a side guide groove; 13. separating the floating plate; 14. sealing the rotating sleeve; 15. an adsorption chamber; 16. adsorption holes; 17. a drive shaft; 18. an outer spring; 19. a side groove; 20. an inner fixed shaft; 21. a stirring rod; 22. an inner spring.
Description of the embodiments
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments.
Referring to fig. 1-4, the utility model provides an oil-water separator for catalyst production, which comprises a reaction tower 1 and a separation tower 2, wherein the outer surface of the reaction tower 1 is fixedly connected with a condenser 3, the outer surface of the separation tower 2 is fixedly connected with a first pump body 4, a first guide pipe 5 is fixedly connected between the condenser 3 and the first pump body 4, the bottom surface of the separation tower 2 is fixedly connected with a discharge pipe 6, the upper end surface of the reaction tower 1 is fixedly connected with a negative pressure machine 7, the upper end surface of the separation tower 2 is fixedly connected with a motor 8, the upper end surface of the negative pressure machine 7 is fixedly connected with a second guide pipe 9, the outer side of the upper end surface of the separation tower 2 is slidingly connected with a downslide pipe 10, the second guide pipe 9 is slidingly connected with the downslide pipe 10, the lower side of the inner wall of the separation tower 2 is fixedly connected with a filter plate 11, and the inner wall of the separation tower 2 is provided with a side guide groove 12;
the inside sliding connection of separator 2 has separation floating plate 13, the inside rotation of separation floating plate 13 is connected with sealed cover 14, adsorption cavity 15 has been seted up to the inside of separation floating plate 13, adsorption hole 16 has been seted up to the downside surface of separation floating plate 13, the output of motor 8 and be located the inside fixedly connected with drive shaft 17 of separator 2, and separation floating plate 13 passes through sealed cover 14 and is connected with drive shaft 17 rotation, outer spring 18 has been cup jointed in the outside of drive shaft 17, lateral groove 19 has been seted up to the surface of drive shaft 17, the inside fixedly connected with interior jackshaft 20 of lateral groove 19, the surface sliding connection of interior jackshaft 20 has puddler 21, interior jackspring 22 has been cup jointed on the surface of interior jackshaft 20, can react the processing with triacetin through reactor 1, and can carry the ester liquid after the gas liquefaction in the reactor 1 to the first pipe in, and can carry the ester liquid to separator 2 by the first pump body 4, motor 8 can drive puddler 21 through drive shaft 17 rotation, make the fat water dispersion, and the solid impurity in the fat layer sunk bottom, and be discharged by drain tube 6, when the liquid level 21, the stirring like, the fat water can be layered on the fat water when stirring.
Further, the stirring rods 21 are axially provided with three groups along the driving shaft 17, the stirring rods 21 at the lowest side are fixedly connected with the driving shaft 17, the stirring rods 21 at the upper side are slidably connected with the side grooves 19, and inner springs 22 are arranged between the two adjacent stirring rods 21, namely, the stirring rods 21 at the upper side can axially slide the driving shaft 17 and compress the inner springs 22, so that the subsequent separation floating plate cannot interfere with the stirring rods 21 when moving up and down.
Further, the separation floating plate 13 is in a shape of a circular truncated cone, and the upper and lower ends of the outer spring 18 are in contact with the separation tower 2 and the separation floating plate 13, when the liquid level of the fat water rises, the separation floating plate 13 moves upwards at this time, and the outer spring 18 is compressed, so that the separation floating plate 13 can be closely attached to the liquid level, and an oil layer on the liquid level can be adsorbed.
Further, the down slide 10 penetrates the separation floating plate 13 and extends to the inside of the adsorption cavity 15, the down slide 10 is fixedly connected with the separation floating plate 13, the down slide 10, the adsorption cavity 15 and the adsorption hole 16 are communicated, the liquid level of the fat water is raised along with the increase of the fat water amount in the reaction tower 1 and contacts with the bottom surface of the separation floating plate 13, the liquid level has upward thrust to the separation floating plate 13, then the negative pressure machine 7 can provide negative pressure to the inside of the adsorption cavity 15 through the second conduit 9 and the down slide 10, an oil layer on the fat water liquid level can be adsorbed through the adsorption hole 16, and the upper oil layer on the liquid level can be conveyed into the reaction tower 1 again through the second conduit 9 and the down slide 10, and only water in the layer is left in the separation tower 2.
Further, the two ends of the separation floating plate 13 are fixedly connected with the sliding blocks, the separation floating plate 13 is axially and slidably connected with the separation tower 2 through the sliding blocks and the side guide grooves 12, and the separation floating plate 13 can be limited in the circumferential direction by sliding the sliding blocks in the vertical direction in the side guide grooves 12, so that the separation floating plate 13 can only move up and down along with the liquid level.
Further, the bottom surface of the inside of the separation tower 2 is arc-shaped, and one end of the inner side of the first conduit 5 penetrates through the separation tower 2 and is positioned above the filter plate 11, so that the first conduit 5 can convey the fat water in the reaction tower 1 into the separation tower 2.
When the device is used, glyceryl triacetate can be subjected to reaction processing through the reaction tower 1, ester liquid after gas liquefaction in the reaction tower 1 can be conveyed into the first guide pipe through the condenser 3, the ester liquid can be conveyed into the separation tower 2 through the first pump body 4, the motor 8 can drive the stirring rod 21 to rotate through the driving shaft 17, so that the lipid water is dispersed, solid impurities in the lipid water sink and are discharged through the discharge pipe 6, when the stirring rod 21 stirs the lipid water, the liquid level of the lipid water can be made to be vortex-shaped, an oil layer in the lipid water floats on the liquid level at the moment, so that oil and water can be layered, the liquid level of the lipid water rises and contacts with the bottom surface of the separation floating plate 13 along with the increase of the lipid water amount in the reaction tower 1, the liquid level of the lipid water has upward thrust at the moment, then the negative pressure is provided for the inside the adsorption cavity 15 through the second guide pipe 9 and the lower slide pipe 10, the oil layer on the lipid water level can be adsorbed through the adsorption hole 16, the oil layer on the liquid level can be conveyed into the reaction tower 2 again through the second guide pipe 9 and the lower slide pipe 10, and the water layer is left in the reaction tower 2.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides an oil-water separator for catalyst production, includes reaction tower (1) and separator (2), its characterized in that: the device comprises a reaction tower (1), wherein a condenser (3) is fixedly connected to the outer surface of the reaction tower (1), a first pump body (4) is fixedly connected to the outer surface of a separation tower (2), a first guide pipe (5) is fixedly connected between the condenser (3) and the first pump body (4), a discharging pipe (6) is fixedly connected to the bottom surface of the separation tower (2), a negative pressure machine (7) is fixedly connected to the upper end surface of the reaction tower (1), a motor (8) is fixedly connected to the upper end surface of the separation tower (2), a second guide pipe (9) is fixedly connected to the upper end surface of the negative pressure machine (7), a lower slide pipe (10) is slidingly connected to the outer side of the upper end surface of the separation tower (2), a filter plate (11) is fixedly connected to the lower side of the inner wall of the separation tower (2), and a side guide groove (12) is formed in the inner wall of the separation tower (2);
the inside sliding connection of knockout drum (2) has separation floating plate (13), the inside of separation floating plate (13) rotates and is connected with sealed cover (14), absorption chamber (15) have been seted up to the inside of separation floating plate (13), absorption hole (16) have been seted up to the downside surface of separation floating plate (13), the output of motor (8) is located inside fixedly connected with drive shaft (17) of knockout drum (2), and separation floating plate (13) rotate through sealed cover (14) and drive shaft (17) to be connected, outer spring (18) have been cup jointed in the outside of drive shaft (17), lateral groove (19) have been seted up to the surface of drive shaft (17), the inside fixedly connected with interior axle (20) of lateral groove (19), the surface sliding connection of interior axle (20) has puddler (21), interior spring (22) have been cup jointed on the surface of interior axle (20).
2. The oil-water separator for catalyst production according to claim 1, wherein: the stirring rods (21) are axially arranged along the driving shaft (17) in three groups, the stirring rods (21) at the lowest side are fixedly connected with the driving shaft (17), the stirring rods (21) at the upper side are slidably connected with the side grooves (19), and an inner spring (22) is arranged between every two adjacent stirring rods (21).
3. The oil-water separator for catalyst production according to claim 1, wherein: the separation floating plate (13) is in a round table shape, and the upper end and the lower end of the outer spring (18) are in contact with the separation tower (2) and the separation floating plate (13).
4. The oil-water separator for catalyst production according to claim 1, wherein: the lower sliding tube (10) penetrates through the separation floating plate (13) and extends to the inside of the adsorption cavity (15), the lower sliding tube (10) is fixedly connected with the separation floating plate (13), and the lower sliding tube (10), the adsorption cavity (15) and the adsorption hole (16) are communicated.
5. The oil-water separator for catalyst production according to claim 1, wherein: the two ends of the separation floating plate (13) are fixedly connected with sliding blocks, and the separation floating plate (13) is axially and slidably connected with the separation tower (2) through the sliding blocks and the side guide grooves (12).
6. The oil-water separator for catalyst production according to claim 1, wherein: the inner bottom surface of the separation tower (2) is arc-shaped, and one end of the inner side of the first conduit (5) penetrates through the separation tower (2) and is positioned above the filter plate (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320894788.XU CN219848270U (en) | 2023-04-20 | 2023-04-20 | Oil-water separator for catalyst production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320894788.XU CN219848270U (en) | 2023-04-20 | 2023-04-20 | Oil-water separator for catalyst production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219848270U true CN219848270U (en) | 2023-10-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320894788.XU Active CN219848270U (en) | 2023-04-20 | 2023-04-20 | Oil-water separator for catalyst production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219848270U (en) |
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- 2023-04-20 CN CN202320894788.XU patent/CN219848270U/en active Active
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