CN219398991U

CN219398991U - Fractionation device for terpinene-4-alcohol preparation

Info

Publication number: CN219398991U
Application number: CN202320326909.0U
Authority: CN
Inventors: 杨斌; 危景波; 苏江波
Original assignee: Fujian Nanping Longsheng Flavor And Fragrance Co ltd
Current assignee: Fujian Nanping Longsheng Flavor And Fragrance Co ltd
Priority date: 2023-02-27
Filing date: 2023-02-27
Publication date: 2023-07-25
Anticipated expiration: 2033-02-27

Abstract

The utility model discloses a fractionation device for terpinene-4-ol preparation, which belongs to the technical field of fractionation devices and aims at the problems that the fractionation efficiency of the fractionation device is not high enough and the use of the fractionation device is limited; according to the utility model, the fixed rod is driven to rotate by the driving motor, so that the stirring effect is realized, the fractionation efficiency of the fractionation device is improved, the hand wheel is rotated by manpower, the volume of the fractionation tank is conveniently adjusted, and the practicability of the fractionation device is improved.

Description

Fractionation device for terpinene-4-alcohol preparation

Technical Field

The utility model belongs to the technical field of fractionation devices, and particularly relates to a fractionation device for preparing terpinene-4-ol.

Background

Fractionation is a process of heating a certain mixture, cooling and separating different boiling points of each component in the mixture into relatively pure single substances, and in the process of preparing terpinen-4-ol, a fractionation tower is generally used for fractionating terpinen-4-ol raw material.

The publication number of the comparison patent document is: "CN 215609427U's a fractionation device for terpinene-4-ol preparation, including the base box, the four corners of the roof of base box all is fixed with vertical stable cover, the inner circle movable sleeve of stable cover is equipped with vertical transmission post, the top of four transmission posts extends to the upside of stable cover and is fixed with the fractionating tower body, the fixed cover of the outer lane of the transmission post that is located stable cover upside is equipped with horizontal backup pad, the diapire of backup pad is connected with vertical first buffer spring with the top of stable cover, the bottom of four transmission posts extends to the inside of base box and is fixed with horizontal flat board, the bottom of stable cover is connected with vertical second buffer spring with dull and stereotyped roof. The utility model has ingenious design, small vibration during working, small noise generated by vibration during working, and is beneficial to improving the comfort level of surrounding staff, preventing the damage of parts caused by vibration and reducing the failure rate, and the following problems still exist under the actual use condition: although this patent can carry out daily fractionation operation, in the in-service use, the fractionation device is inconvenient to evenly heat the raw materials for the speed of preparation terpinen-4-ol is slower, and then makes the fractionation efficiency of fractionation device not high enough, and the volume of fractionation device is comparatively fixed, makes the inconvenient volume of adjusting the fractionation jar according to staff's needs, makes the use of fractionation device have the limitation.

Therefore, there is a need for a fractionation device for terpinen-4-ol production that solves the problems of insufficient fractionation efficiency and limitations in the use of the fractionation device in the prior art.

Disclosure of Invention

The utility model aims to provide a fractionation device for preparing terpinen-4-ol, which aims to solve the problems in the prior art.

In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model provides a terpinene-4-alcohol preparation is with fractionation device, includes the base, the base upper end is fixed with the fractionation jar, the fractionation jar is inside to be seted up the fractionation jar, the fractionation jar upper end is fixed with driving motor, driving motor drive end is fixed with the dead lever, the dead lever middle part is fixed with three connecting rod, and is three the connecting rod both ends are fixed with two clearance boards, the base middle part rotates and is connected with the stabilizer bar, stabilizer bar one end is fixed with the hand wheel, the stabilizer bar other end is fixed with reciprocal double-screw bolt, the equal threaded connection of reciprocal double-screw bolt both sides surface has the screw block, two the screw block upside rotates and is connected with the articulated frame, the articulated frame upper end rotates and is connected with two sliders, two slider upside slides and is connected with the regulating plate.

In the scheme, the bottom of the adjusting plate is provided with a sliding groove, and the outer surfaces of the two sliding blocks are slidably connected with the inner walls at the left side and the right side of the sliding groove.

It is further worth to say that the stabilizer slot has been seted up at the base middle part, two screw thread piece surface sliding connection is at stabilizer slot left and right sides inner wall.

It should be further noted that the fixing rod penetrates through the middle of the fractionating tank, and the outer surface of the adjusting plate is slidably connected to the inner wall of the fractionating tank.

As a preferred embodiment, the outer surface of each cleaning plate is rotationally connected to the inner wall of the fractionating tank, and the cross section of each cleaning plate is arc-shaped.

As a preferred implementation mode, a feed inlet is arranged on one side of the fractionating tank, a discharge outlet is arranged on the other side of the fractionating tank, a condensing tube is arranged in the middle of the discharge outlet, and a collecting tank is arranged at the bottom of the discharge outlet.

As a preferred implementation mode, the four corners of the bottom of the base are fixedly provided with supporting legs, and the vertical section of each supporting leg is in T-shaped arrangement.

Compared with the prior art, the fractionation device for preparing terpinen-4-ol provided by the utility model at least has the following beneficial effects:

(1) The fixed rod is driven to rotate by the driving motor, so that the fixed rod, the connecting rod, the cleaning plate, the fractionating tank and the fractionating tank are mutually matched to realize the stirring effect, the raw materials are heated more uniformly, the fractionating speed of the fractionating device is higher, and the fractionating efficiency of the fractionating device is improved.

(2) The hand wheel is rotated by manpower, so that the hand wheel, the stabilizer bar, the reciprocating screw, the threaded block, the hinge bracket, the adjusting plate, the stabilizing groove, the sliding groove and the sliding block are mutually matched for operation, the effect of conveniently adjusting the volume of the fractionating tank is realized, the volume of the fractionating device can be adjusted according to the needs of workers, and the effect of improving the practicability of the fractionating device is further achieved.

Drawings

FIG. 1 is a perspective view of the present utility model;

FIG. 2 is a cross-sectional view of a fractionation tank of the present utility model;

FIG. 3 is a cross-sectional view of a base of the present utility model;

fig. 4 is a schematic view of the structure of the adjusting plate of the present utility model.

In the figure: 1. a base; 2. a fractionation tank; 3. a fractionation tank; 4. a driving motor; 5. a fixed rod; 6. a connecting rod; 7. a cleaning plate; 8. a stabilizer bar; 9. a hand wheel; 10. a reciprocating stud; 11. a screw block; 12. a hinge bracket; 13. a slide block; 14. an adjusting plate; 15. a chute; 16. a feed inlet; 17. a discharge port; 18. a condensing tube; 19. a collection tank; 20. a support leg; 21. a stabilizing trough.

Detailed Description

The utility model is further described below with reference to examples.

Referring to fig. 1-4, the utility model provides a fractionation device for preparing terpinene-4-ol, comprising a base 1, wherein the base 1 plays a role of connecting a fractionation tank 2 with a collection tank 19, the fractionation tank 2 is fixed at the upper end of the base 1, butanone and catalyst KGC can be added into a strong acid solution by the fractionation tank 2, the temperature is raised to thirty-seventy degrees, acetaldehyde is added, stirring is carried out for two to four hours, cooling is carried out to room temperature, the pH value is adjusted to be neutral, then the fractionation operation is carried out, the preparation operation of terpinene-4-ol can be carried out, a fractionation tank 3 is arranged in the fractionation tank 2, a driving motor 4 is fixed at the upper end of the fractionation tank 2, the driving motor 4 provides a driving force, a fixing rod 5 is fixed at the driving end of the driving motor 4, the fixing rod 5 is used for fixing the connecting rod 6, three connecting rods 6 are fixed at the middle part of the fixing rod 5, the connecting rod 6 is used for stirring raw materials, two cleaning plates 7 are fixed at two ends of the three connecting rods 6, the cleaning plates 7 can clean the inner wall of the fractionating tank 3 to prevent raw materials from corroding the fractionating tank 2, a stabilizer bar 8 is rotationally connected to the middle of the base 1, the stabilizer bar 8 is used for connecting a hand wheel 9 with a reciprocating stud 10, one end of the stabilizer bar 8 is fixedly provided with the hand wheel 9, the hand wheel 9 is convenient for workers to rotate, the other end of the stabilizer bar 8 is fixedly provided with the reciprocating stud 10, the reciprocating stud 10 drives two threaded blocks 11 to reversely slide, the outer surfaces of two sides of the reciprocating stud 10 are in threaded connection with the threaded blocks 11, the threaded blocks 11 drive a hinged frame 12 to fold, the upper sides of the two threaded blocks 11 are rotationally connected with the hinged frame 12 to adjust the volume of the fractionating tank 2, the upper end of the hinged frame 12 is rotationally connected with two sliding blocks 13, the slide blocks 13 are connected with the adjusting plates 14, the adjusting plates 14 are connected to the upper sides of the two slide blocks 13 in a sliding mode, and the adjusting plates 14 are used for adjusting the size of the fractionating tank 2.

Further, as shown in fig. 1, 3 and 4, it is worth specifically explaining that the bottom of the adjusting plate 14 is provided with a sliding groove 15, the outer surfaces of the two sliding blocks 13 are slidably connected with the inner walls on the left side and the right side of the sliding groove 15, the middle of the base 1 is provided with a stabilizing groove 21, and the outer surfaces of the two threaded blocks 11 are slidably connected with the inner walls on the left side and the right side of the stabilizing groove 21.

Further, as shown in fig. 1 and fig. 2, it is worth specifically describing that the fixing rod 5 penetrates through the middle of the fractionating tank 2, the outer surface of the adjusting plate 14 is slidably connected to the inner wall of the fractionating tank 3, the outer surface of each cleaning plate 7 is rotatably connected to the inner wall of the fractionating tank 3, and the cross section of each cleaning plate 7 is arc-shaped.

The scheme comprises the following working processes: when using terpinene-4-alcohol preparation to use fractionation device, at first, drive dead lever 5 through driving motor 4 rotates, make a plurality of connecting rod 6 of dead lever 5 middle part fixed connection rotate, thereby make and the clearance board 7 of connecting rod 6 both ends fixed connection rotate, stir the operation to the raw materials that gets into by the pan feeding mouth, make under the stirring of connecting rod 6 the raw materials be heated more evenly, and under the rotation of clearance board 7, make the inner wall of fractionation tank 3 be cleared up more cleanly, make fractionation device's fractionation speed faster, and then reach the effect that improves fractionation device's fractionation efficiency, then rotate hand wheel 9 through the manpower, make and hand wheel 9 middle part fixed connection's stabilizer bar 8 rotate, thereby make and the reciprocal double-screw bolt 10 of stabilizer 8 one end fixed connection rotate, and then make and reciprocal double-screw bolt 10 left and right sides surface threaded connection's screw thread block 11 carry out reverse slip operation under the stability of stabilizer 21, thereby make with two screw block 11 upside rotate the articulated frame 12 of being connected fold operation, and then make and the articulated frame 12 carry out the regulation effect of height adjustment plate 14 at the side of stabilizer bar 12, and carry out the volume adjustment of the fractionation tank 2 is greatly, and thus the volume is greatly adjusted when the volume is greatly adjusted, the raw materials is greatly improved, the fractionation device is realized.

The working process can be as follows: the fixed rod 5 is driven to rotate through the driving motor 4, the connecting rod 6 fixedly connected with the middle part of the fixed rod 5 is rotated, the stirring effect is achieved, the raw materials are heated more uniformly, the fractionation speed of the fractionation device is higher, the fractionation efficiency of the fractionation device is improved, the hand wheel 9 is rotated through manpower, the stabilizer bar 8 fixedly connected with the middle part of the hand wheel 9 is rotated, the reciprocating stud 10 fixedly connected with one end of the stabilizer bar 8 is further used for driving the two threaded blocks 11 to carry out reverse sliding operation, the volume effect of the fractionation tank 2 is achieved, the volume of the fractionation device can be adjusted according to the needs of staff, and the practicability of the fractionation device is improved.

Further, as shown in fig. 1, 2 and 3, it is worth specifically explaining that a feed inlet 16 is provided on one side of the fractionating tank 2, a discharge outlet 17 is provided on the other side of the fractionating tank 2, a condensation pipe 18 is provided in the middle of the discharge outlet 17, a collecting tank 19 is provided at the bottom of the discharge outlet 17, the condensation pipe 18 condenses, and the collecting tank 19 collects.

Further, as shown in fig. 1, fig. 2 and fig. 3, it is worth specifically explaining that the four corners of the bottom of the base 1 are all fixed with the supporting legs 20, the vertical section of each supporting leg 20 is T-shaped, the supporting legs 20 play a role in supporting the base 1, and the stability of the fractionation device is improved.

To sum up: the condensing effect is carried out through the condenser pipe 18 that sets up, and the collecting tank 19 that sets up is collected the effect, plays the effect of supporting base 1 through the landing leg 20 that sets up, improves the effect of fractionation plant stability.

The driving motor 4 can be purchased in the market, and the driving motor 4 is provided with a power supply, which belongs to the mature technology in the field and is fully disclosed, so that the description is not repeated.

Claims

1. The utility model provides a terpinene-4-alcohol preparation is with fractionation device, includes base (1), its characterized in that, base (1) upper end is fixed with fractionation tank (2), fractionation tank (2) inside has seted up fractionation tank (3), fractionation tank (2) upper end is fixed with driving motor (4), driving motor (4) drive end is fixed with dead lever (5), dead lever (5) middle part is fixed with three connecting rod (6), and is three connecting rod (6) both ends are fixed with two clearance boards (7), base (1) middle part rotation is connected with stabilizer bar (8), stabilizer bar (8) one end is fixed with hand wheel (9), the stabilizer bar (8) other end is fixed with reciprocal double-screw bolt (10), equal threaded connection in reciprocal double-screw bolt (10) both sides surface has screw thread piece (11), two screw thread piece (11) upside rotates and is connected with articulated frame (12), articulated frame (12) upper end rotation is connected with two slider (13), two slider (13) are gone up and are connected with regulating plate (14) sideslip.

2. The fractionation apparatus for producing terpinen-4-ol as defined in claim 1, wherein: a sliding groove (15) is formed in the bottom of the adjusting plate (14), and the outer surfaces of the two sliding blocks (13) are connected to the inner walls of the left side and the right side of the sliding groove (15) in a sliding mode.

3. The fractionation apparatus for producing terpinen-4-ol as defined in claim 1, wherein: the middle part of the base (1) is provided with a stabilizing groove (21), and the outer surfaces of the two threaded blocks (11) are connected with the inner walls of the left side and the right side of the stabilizing groove (21) in a sliding mode.

4. The fractionation apparatus for producing terpinen-4-ol as defined in claim 1, wherein: the fixed rod (5) penetrates through the middle of the fractionating tank (2), and the outer surface of the adjusting plate (14) is connected to the inner wall of the fractionating tank (3) in a sliding mode.

5. The fractionation apparatus for producing terpinen-4-ol as defined in claim 1, wherein: every clearance board (7) surface rotates to be connected at fractionating groove (3) inner wall, every clearance board (7) cross section all is the arc setting.

6. The fractionation apparatus for producing terpinen-4-ol as defined in claim 1, wherein: the utility model discloses a fractionating device, including fractionating jar (2), collecting tank (17), condenser pipe (18) are provided with feed inlet (16) in fractionating jar (2) one side, fractionating jar (2) opposite side is provided with discharge gate (17), discharge gate (17) middle part is provided with condenser pipe (18), discharge gate (17) bottom is provided with collecting tank (19).

7. The fractionation apparatus for producing terpinen-4-ol as defined in claim 1, wherein: the four corners of the bottom of the base (1) are respectively fixed with a supporting leg (20), and the vertical section of each supporting leg (20) is T-shaped.