CN219091116U - Distilling device and distilling system beneficial to improving ethyl caproate solubility - Google Patents
Distilling device and distilling system beneficial to improving ethyl caproate solubility Download PDFInfo
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- CN219091116U CN219091116U CN202223089457.3U CN202223089457U CN219091116U CN 219091116 U CN219091116 U CN 219091116U CN 202223089457 U CN202223089457 U CN 202223089457U CN 219091116 U CN219091116 U CN 219091116U
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- raw material
- material cavity
- distillation
- solubility
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- SHZIWNPUGXLXDT-UHFFFAOYSA-N ethyl hexanoate Chemical compound CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 title claims abstract description 60
- 230000009286 beneficial effect Effects 0.000 title claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 47
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 38
- 238000004821 distillation Methods 0.000 claims abstract description 35
- 238000010438 heat treatment Methods 0.000 claims abstract description 22
- 238000003756 stirring Methods 0.000 claims abstract description 10
- 238000005485 electric heating Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 230000007423 decrease Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 9
- 238000009413 insulation Methods 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 125000003118 aryl group Chemical group 0.000 description 2
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 description 1
- 241000235342 Saccharomycetes Species 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000011491 glass wool Substances 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 239000003864 humus Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000015096 spirit Nutrition 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Images
Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model provides a distillation device and a distillation system which are beneficial to improving the solubility of ethyl caproate, relates to the field of white spirit distillation, and solves the problems that the solubility of ethyl caproate in ethanol is reduced and the distillation amount is reduced due to the fact that the concentration of alcohol in the existing distillation device is reduced along with the distillation process; an alcohol concentration sensor is arranged on the inner top wall of the raw material cavity; the side wall of the raw material cavity is provided with a feeding pipe; the feeding pipe is provided with an electric valve I; the inner wall of the raw material cavity is provided with a stirring device; the bottom wall of the raw material cavity is connected with the heating cavity. The utility model controls sectional feeding by the alcohol concentration sensor, controls the decline of alcohol concentration in the distillation device to a certain extent, and improves the distilling amount of ethyl caproate.
Description
Technical Field
The utility model relates to the field of white spirit distillation, in particular to a distillation device beneficial to improving the solubility of ethyl caproate.
Background
The main purpose of the distilled spirit distillation process is to concentrate alcohol and extract aroma substances. Ethyl caproate is one of the flavor components of white spirit. The ethyl caproate content is difficult to reach the standard of the high-grade wine, and the current common method for improving the ethyl caproate content is to improve pit mud, such as adding humus, electrodeless nutritive salt, caproic acid bacteria, methane bacteria and the like into the pit mud, namely improving in the initial fermentation process. There is no excessive concern about how to increase the extraction rate of ethyl caproate during the distillation process. The patent with publication number of CN106434240A discloses a method for improving the content of ethyl caproate in strong aromatic white spirit, which is to increase the concentration of thallus autolysate in fermented grains by improving the quantity of saccharomycetes so as to excite the function of pit mud to act as bacteria, and finally, the aim of improving the content of ethyl caproate is fulfilled on the premise of ensuring the quality of the wine. The patent with publication number of CN114231379A discloses a distillation method for increasing and reducing milk of strong aromatic Chinese spirits, which increases the concentration of alcohol in a device by intercepting initial alcohol vapor, is favorable for dissolving ethyl caproate in alcohol so as to increase the distilling amount of the ethyl caproate, but starts flowing the liquor by opening a valve, and in the subsequent distillation process, the concentration of alcohol is still lower and lower, so that the ethyl caproate is unfavorable for dissolving the ethyl caproate in alcohol.
Disclosure of Invention
The utility model aims to provide a distillation device beneficial to improving the solubility of ethyl caproate, and solves the problems that the solubility of ethyl caproate in ethanol is reduced and the distillation amount is reduced due to the fact that the concentration of alcohol in the existing distillation device is reduced along with the distillation process.
The embodiment of the utility model is realized by the following technical scheme:
a distilling device beneficial to improving the solubility of ethyl caproate comprises a heating cavity and a raw material cavity; an alcohol concentration sensor is arranged on the inner top wall of the raw material cavity; the side wall of the raw material cavity is provided with a feeding pipe; the feeding pipe is provided with an electric valve I; the inner wall of the raw material cavity is provided with a stirring device; the bottom wall of the raw material cavity is connected with the heating cavity.
Preferably, the side wall of the raw material cavity is provided with a temperature sensor.
Preferably, the bottom of the heating cavity is provided with an electric heating plate; and a water inlet is formed in the side wall of the heating cavity.
Preferably, a heat exchanger is included; the outlet pipe of the raw material cavity is connected with the heat exchange medium inlet of the heat exchanger; the raw material outlet of the heat exchanger is connected with the feeding pipe of the raw material cavity.
Preferably, a heat exchange medium outlet of the heat exchanger is connected with the storage tank.
Preferably, the outer walls of the raw material cavity and the outlet pipe of the raw material cavity are both provided with heat insulation layers.
Preferably, the outlet pipe of the raw material cavity is provided with an electric valve II.
The technical scheme of the embodiment of the utility model has at least the following advantages and beneficial effects:
the utility model controls sectional feeding by the alcohol concentration sensor, controls the decline of alcohol concentration in the distillation device to a certain extent, and improves the distilling amount of ethyl caproate.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present utility model, the drawings that are needed in the embodiments will be briefly described below, it being understood that the following drawings only illustrate some embodiments of the present utility model and therefore should not be considered as limiting the scope, and other related drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a schematic diagram of a distillation apparatus for facilitating enhanced ethyl hexanoate solubility provided by the present utility model;
FIG. 2 is a flow chart of a distillation system provided in the present utility model;
icon: 1-heating cavity, 11-electric heating plate, 12-water inlet, 2-raw material cavity, 21-alcohol concentration sensor, 22-feeding pipe, 221-electric valve I, 23-stirring device, 24-temperature sensor, 25-outlet pipe, 251-electric valve II, 26-material door, 3-distillation device, 4-heat exchanger and 5-storage tank.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the embodiments of the present utility model more apparent, the technical solutions of the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model, and it is apparent that the described embodiments are some embodiments of the present utility model, but not all embodiments of the present utility model. The components of the embodiments of the present utility model generally described and illustrated in the figures herein may be arranged and designed in a wide variety of different configurations.
Example 1
As shown in fig. 1, a distillation device which is beneficial to improving the solubility of ethyl caproate comprises a heating cavity 1 and a raw material cavity 2; an alcohol concentration sensor 21 is arranged on the inner top wall of the raw material cavity 2; the side wall of the raw material cavity 2 is provided with a feeding pipe 22; the feeding pipe 22 is provided with an electric valve I221; the inner wall of the raw material cavity 2 is provided with a stirring device 23; the bottom wall of the raw material cavity 2 is connected with the heating cavity 1.
In the specific implementation process, the prior art is one-time feeding, and the material is fed again after distillation is completed. The conventional singlechip is used as a control module to control the opening and closing of the first electric valve 221, when the value measured by the alcohol concentration sensor 21 is lower than the set minimum threshold value, the first electric valve 221 is opened, new fermented grains are added, the alcohol content of the new fermented grains is higher, the alcohol concentration in the device can be improved to a certain extent, so that the solubility of ethyl caproate in alcohol is improved, and the distilling quantity of ethyl caproate is increased. The stirring device 23 is mainly used for uniformly mixing the newly added raw material and the old raw material, and the positions of the stirring device are not specially set, and the stirring device can be used for inner top wall, bottom wall, side wall and the like. The stirring device 23 may be formed by connecting stirring blades using a conventional rotating shaft and driven by a rotating motor. An openable and closable material gate 26 can be arranged on the side wall of the raw material cavity 2 for a discharge hole after distillation is completed.
In this embodiment, the side wall of the raw material chamber 2 is provided with a temperature sensor 24. In the specific implementation process, the boiling point of the alcohol is lower than that of water, so that the temperature is controlled between the alcohol and the water, the water is not evaporated, the alcohol is evaporated, the alcohol concentration is higher, and the ethyl caproate is more beneficial to being dissolved in the alcohol. The temperature can be controlled between 80 degrees and 90 degrees using existing thermostats, such as ZWK heat treatment thermostats manufactured by electric heating equipment limited, su. If the alcohol concentration measured by the alcohol concentration sensor 21 exceeds the set upper threshold, the heating temperature may be increased so that the water evaporates to reduce the alcohol concentration. After the temperature controller detects the temperature through the temperature sensor 21, the numerical value is transmitted to the temperature controller to compare the temperature and calculate and output deviation, and finally the heating degree of the electric heating plate is controlled, even the electric heating plate is opened and closed, so as to make up the deviation. Such as the temperature is lower than the threshold value, the heating power of the electric heating plate is controlled to be increased.
In this embodiment, an electric heating plate 11 is disposed at the bottom of the heating chamber 1; the side wall of the heating cavity 1 is provided with a water inlet 12.
In the specific implementation process, the heating mode can also adopt conventional direct electric heating or open fire heating. The utility model preferably uses steam heating, because the steam heating is more uniform, the degradation of starch and protein in malt is more ideal, and the phenomenon of electric heating paste pot can not occur.
As shown in fig. 2, in the present embodiment, a heat exchanger 4 is included; the outlet pipe 25 of the raw material cavity 2 is connected with the heat exchange medium inlet of the heat exchanger 4; the raw material outlet of the heat exchanger 4 is connected with a feeding pipe 22 of the raw material cavity 2.
In the specific implementation process, the alcohol vapor is required to be additionally cooled into the liquid wine in the prior art, the heat of the alcohol vapor is fully utilized, the alcohol vapor is used as a heat exchange medium to preheat the raw material, the heat consumption in the subsequent distillation process is reduced, and the vapor is liquefied.
In this embodiment, the heat exchange medium outlet of the heat exchanger 4 is connected to the storage tank 5.
In a specific implementation, the storage tank 5 is used for storing liquid wine.
In this embodiment, the outer walls of the raw material cavity 2 and the outlet pipe 25 of the raw material cavity 2 are both provided with heat insulation layers.
In the specific implementation process, the heat insulation layer can adopt glass wool, so that heat dissipation is effectively reduced.
In this embodiment, the outlet pipe 25 of the raw material chamber 2 is provided with an electric valve II 251.
In the specific implementation process, when the alcohol concentration is reduced to the set lower threshold, the second electric valve 251 can be closed, so that the continuous outward transportation of the alcohol in the device is avoided, the first electric valve 221 is opened, and new fermented grains are added, so that the alcohol concentration in the device is quickly increased.
A distillation system of a distillation device which is beneficial to improving the solubility of ethyl caproate comprises a heat exchanger; the outlet pipe of the raw material cavity 2 is connected with the heat exchange medium inlet of the heat exchanger; the raw material outlet of the heat exchanger is connected with the feeding pipe of the raw material cavity 2.
The heat exchange medium outlet of the heat exchanger is connected with the storage tank 5.
The outer walls of the raw material cavity 2 and the outlet pipe of the raw material cavity are both provided with heat insulation layers.
An outlet pipe of the raw material cavity 2 is provided with an electric valve II 251.
The above is only a preferred embodiment of the present utility model, and is not intended to limit the present utility model, but various modifications and variations can be made to the present utility model by those skilled in the art. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present utility model should be included in the protection scope of the present utility model.
Claims (7)
1. A distilling device beneficial to improving the solubility of ethyl caproate is characterized by comprising a heating cavity and a raw material cavity; an alcohol concentration sensor is arranged on the inner top wall of the raw material cavity; the side wall of the raw material cavity is provided with a feeding pipe; the feeding pipe is provided with an electric valve I; the inner wall of the raw material cavity is provided with a stirring device; the bottom wall of the raw material cavity is connected with the heating cavity.
2. The distillation apparatus for facilitating the enhancement of ethyl hexanoate solubility according to claim 1, wherein the feedstock chamber side wall is provided with a temperature sensor.
3. The distillation apparatus for facilitating the improvement of ethyl caproate solubility according to claim 1, wherein an electric heating plate is provided at the bottom of the heating chamber; and a water inlet is formed in the side wall of the heating cavity.
4. A distillation system comprising the distillation apparatus of any one of claims 1-3, wherein the distillation apparatus is configured to increase the solubility of ethyl hexanoate, comprising a heat exchanger; the outlet pipe of the raw material cavity is connected with the heat exchange medium inlet of the heat exchanger; the raw material outlet of the heat exchanger is connected with the feeding pipe of the raw material cavity.
5. The distillation system according to claim 4, wherein the heat exchange medium outlet of the heat exchanger is connected to a storage tank.
6. The distillation system according to claim 4, wherein the feed chamber and the feed chamber outlet tube outer wall are each provided with a heat insulating layer.
7. The distillation system according to claim 4, wherein the outlet pipe of the feed chamber is provided with an electrically operated valve II.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223089457.3U CN219091116U (en) | 2022-11-17 | 2022-11-17 | Distilling device and distilling system beneficial to improving ethyl caproate solubility |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223089457.3U CN219091116U (en) | 2022-11-17 | 2022-11-17 | Distilling device and distilling system beneficial to improving ethyl caproate solubility |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219091116U true CN219091116U (en) | 2023-05-30 |
Family
ID=86467701
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202223089457.3U Active CN219091116U (en) | 2022-11-17 | 2022-11-17 | Distilling device and distilling system beneficial to improving ethyl caproate solubility |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219091116U (en) |
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2022
- 2022-11-17 CN CN202223089457.3U patent/CN219091116U/en active Active
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| Date | Code | Title | Description |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Lv Gaoqi Inventor after: Lv Sirui Inventor before: Lv Gaoqi Inventor before: Lv Sirui |