CN218421078U - Molecular distiller - Google Patents
Molecular distiller Download PDFInfo
- Publication number
- CN218421078U CN218421078U CN202222397194.6U CN202222397194U CN218421078U CN 218421078 U CN218421078 U CN 218421078U CN 202222397194 U CN202222397194 U CN 202222397194U CN 218421078 U CN218421078 U CN 218421078U
- Authority
- CN
- China
- Prior art keywords
- sleeve
- glass main
- main part
- stainless steel
- glass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000011521 glass Substances 0.000 claims abstract description 71
- 229910001220 stainless steel Inorganic materials 0.000 claims abstract description 44
- 239000010935 stainless steel Substances 0.000 claims abstract description 44
- 239000000463 material Substances 0.000 claims abstract description 13
- 230000008878 coupling Effects 0.000 claims abstract description 4
- 238000010168 coupling process Methods 0.000 claims abstract description 4
- 238000005859 coupling reaction Methods 0.000 claims abstract description 4
- 239000010410 layer Substances 0.000 claims description 6
- 239000000110 cooling liquid Substances 0.000 claims description 3
- 238000000199 molecular distillation Methods 0.000 claims description 3
- 239000011229 interlayer Substances 0.000 claims description 2
- 238000000926 separation method Methods 0.000 abstract description 5
- 239000000126 substance Substances 0.000 abstract description 5
- 230000008859 change Effects 0.000 abstract description 3
- 239000007788 liquid Substances 0.000 description 15
- 239000011344 liquid material Substances 0.000 description 8
- 238000010438 heat treatment Methods 0.000 description 7
- 239000002826 coolant Substances 0.000 description 3
- 230000008676 import Effects 0.000 description 3
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000009835 boiling Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a molecular distiller belongs to chemical separation equipment technical field. It includes the evaporimeter body, the top region of evaporimeter body includes the motor from top to bottom, shaft coupling and closing cap, the middle part region of evaporimeter body is provided with glass main part, be provided with the intermediate layer that is used for the circulation heat source in glass main part's the regional lateral wall in middle part, the intercommunication has an inlet pipe on glass main part's the regional lateral wall in top, glass main part inner chamber top is provided with the knifing ware, the bottom region of evaporimeter body is provided with the base, the base is stainless steel, the base includes first sleeve and second sleeve, first sleeve and second sleeve are the drum structure. The utility model provides a molecular still, it is split type structure to adjust original full glass material is whole, dismantles convenient assembling, compares with the integral type structure, and it is littleer to take place broken change cost, and the structural glass main part of sectional type can also dispose the glass main part of equidimension not.
Description
Technical Field
The utility model relates to a molecular distiller belongs to chemical separation equipment technical field.
Background
Molecular distillation is a special liquid-liquid separation technology, which is different from traditional distillation and relies on the principle of difference in boiling point and difference in mean free path of molecular motion of different substances to realize separation. When the liquid mixture flows along the heating plate and is heated, light and heavy molecules can escape from the liquid surface and enter the gas phase, because of different free paths of the light and heavy molecules, the molecules of different substances move for different distances after escaping from the liquid surface, if a condensing plate can be properly arranged, the light molecules reach the condensing plate and are condensed and discharged, and the heavy molecules cannot reach the condensing plate and are discharged along mixed liquid, so that the aim of separating the substances is fulfilled.
However, the glass body and the base of the conventional molecular distillation apparatus are generally of an integral structure, and if the glass body and the base are broken, the replacement cost is high.
Disclosure of Invention
The utility model discloses the technical problem that will solve lies in: the utility model provides a molecular still, it has solved the glass main part of integral type molecular still and has taken place the breakage, changes the higher problem of cost.
The utility model discloses the technical problem that will solve takes following technical scheme to realize:
the utility model provides a molecular distiller, includes the evaporimeter body, the top region of evaporimeter body includes motor, shaft coupling and closing cap from top to bottom, the middle part region of evaporimeter body is provided with the glass main part, be provided with the intermediate layer that is used for circulating the heat source in the regional lateral wall in middle part of glass main part, the intercommunication has an inlet pipe on the regional lateral wall in top of glass main part, glass main part inner chamber top is provided with the knifing ware, the bottom region of evaporimeter body is provided with the base, the base is stainless steel material, the base includes first sleeve and second sleeve, first sleeve and second sleeve are the drum structure, the top department of drum structure all is provided with the opening, first sleeve with axis collineation and axis perpendicular to horizontal plane between the second sleeve, first telescopic inner chamber diameter is greater than the telescopic lateral wall diameter of second, the telescopic top inlay card of second is in first telescopic diapire middle part, first telescopic top lateral wall department is provided with the stainless steel flange, be provided with second glass flange on the bottom lateral wall of glass main part, the stainless steel flange with second glass flange carry out the telescopic diapire of second through the bolt and carry out fixed connection of second sleeve, second inner chamber bottom wall department is connected with stainless steel coil pipe and is connected with stainless steel coil pipe.
As a preferable example, the top and the bottom of the outer side wall of the middle region of the glass main body are respectively provided with a heat-conducting medium inlet and outlet, and each heat-conducting medium inlet and outlet is communicated with the interlayer.
As a preferred example, the bottom end of the stainless steel coil is positioned right below the second sleeve, and the bottom end of the stainless steel coil is provided with two cooling liquid inlets and outlets.
As a preferred example, the bottom end faces of the first sleeve and the second sleeve are arranged obliquely, and the component interface is located at the bottommost part of the outer side wall of the first sleeve or the second sleeve connected with the component interface.
The utility model has the advantages that: the utility model discloses the glass main part adjustment that will original integral type is first glass main part, the lower half is the stainless steel base, pass through bolted connection in the dismouting, it is relatively convenient, and in case take place the breakage, the region of damage is only glass main part, from cost economic cost, the cost is reduced, and because be split type structure, can also select multiple specification (can also prepare multiple glass main part promptly, each glass main part height, outer of intermediate layer inner chamber variation in size, the glass flange homoenergetic of glass main part bottom can carry out fixed mounting with the stainless steel flange on the stainless steel base), the glass main part and the stainless steel base assemble, only need to be changed glass main part, the structure complexity is relatively less, it is relatively convenient to prepare, then when changing integral type glass main part originally, the cost is higher, and when considering actual use, collide with in the transportation handling, improper etc. all probably can lead to the breakage of integral type glass main part, the change cost is higher, and this application adopts split type structure, the base that stainless steel matter made, even if take place the breakage, only need to change the glass main part on the base can.
Drawings
Fig. 1 is a schematic structural view of the present invention;
FIG. 2 is a diagram of a prior art unitary glass body construction;
FIG. 3 is a schematic view of the glass body of the present invention;
FIG. 4 is a half-sectional view of the glass body of the present invention;
fig. 5 is a schematic structural view of the stainless steel base of the present invention.
In the figure: the device comprises a stainless steel coil 1, a stainless steel flange 2, a light component interface 3, a cooling liquid inlet and outlet 4, a cold trap connector 5, a heavy component interface 6, a first glass flange 7, a glass main body 8, a second glass flange 9, a heat-conducting medium inlet and outlet 10, a motor 11, a coupler 12 and a glass collecting bottle 13.
Detailed Description
In order to understand the technical means, creation features, achievement purposes and functions of the present invention easily, the present invention will be further explained by combining with the specific drawings.
As shown in fig. 1-5, a molecular distiller, including the evaporimeter body, the top region of evaporimeter body includes motor 11 from top to bottom, shaft coupling 12 and closing cap (the closing cap carries out fixed connection through bolt structure and the first glass flange 7 at glass main body 8's lateral wall top), the middle region of evaporimeter body is provided with glass main body 8, be provided with the intermediate layer that is used for circulating the heat source in the regional lateral wall in middle part of glass main body 8, the intercommunication has a inlet pipe on the regional lateral wall in top of glass main body 8, 8 inner chamber tops of glass main body are provided with the knifing ware, the bottom region of evaporimeter body is provided with the base, the base is stainless steel material, the base includes first sleeve and second sleeve, first sleeve and second sleeve are the drum structure, the top department of drum structure all is provided with the opening, the axis collineation of first sleeve and second sleeve both and axis perpendicular to the horizontal plane, the inner chamber diameter of first sleeve is greater than the telescopic lateral wall diameter of second sleeve, the telescopic top inlay card of second sleeve is in the diapire of first sleeve, the top lateral wall department of first sleeve is provided with stainless steel flange 2, the stainless steel flange bottom of glass main body 8 is provided with the second sleeve and the stainless steel flange is provided with the stainless steel flange middle part of the stainless steel flange and is connected with the stainless steel flange middle part of the stainless steel flange and is connected with the stainless steel coil pipe bottom of the stainless steel flange and is connected with the stainless steel flange middle part of stainless steel flange and is connected with stainless steel coil pipe.
It should be noted that, the output end axis of the motor 11 at the top of the evaporator body is perpendicular to the horizontal plane, the top end of the output end coupler 12 of the motor 11 is connected, the bottom end of the coupler 12 passes through the sealing cover to be connected with the film scraper in the inner cavity of the glass main body 8, the motor 11 drives the film scraper in the glass main body 8 through the coupler 12, the liquid material is input to the upper part of the inner cavity of the glass main body 8 through the feed pipe and flows onto the film scraper, the film scraper is a distributor, the top is a turntable structure, the axis is collinear with the glass main body 8, a certain gap is left between the turntable structure and the inner cavity side wall of the glass main body 8, the bottom end face of the film scraper is annularly provided with a plurality of rod bodies, the liquid material flows downwards along the inner cavity side wall of the glass main body 8 through the gap between the turntable structure and the glass main body 8, the rod bodies continuously and uniformly scrape the downward flowing liquid material on the inner cavity side wall of the glass main body 8 into a liquid film with uniform thickness, the uniform liquid film uniformly covering the inner cavity side wall of the glass main body 8, and the liquid material at this time is pushed downwards in a spiral shape.
Heat-conducting medium access & exit 10 has all been seted up to regional lateral wall top and the bottom in middle part of glass main part 8, and every heat-conducting medium access & exit 10 all is linked together with the intermediate layer, two heat-conducting medium access & exit 10, one as the import, another mouthful is as the export, and two heat-conducting medium access & exit 10 connect respectively the input and the output of the liquid material of circulation heating device (like electrical heating heat conduction oil circulation system), and the circulation heating device of here makes the liquid material evaporation on the inner chamber lateral wall of glass main part 8 through the heat-conducting medium.
The bottom of stainless steel coil 1 is located under the second sleeve, and stainless steel coil 1's bottom is provided with two coolant liquid and imports and exports 4, and two coolant liquid are imported and exported 4, and one is as the import, and another is as the export, and stainless steel coil 1 is located the second sleeve inner chamber and stretches to the part of glass main part inner chamber for the heliciform, and coolant liquid is imported and exported 4 and is connected the input and the output of the liquid material of circulation refrigerating plant (cold water machine).
The principle of the molecular distiller is as follows: liquid material is added from the top of evaporimeter (promptly the utility model provides an inlet pipe, material get into glass main part 8 in through the inlet pipe, and material liquid distributor (being the knifing ware) on the rotor distributes it on heating surface (8 inner chamber lateral walls of glass main part) evenly in succession, and the knifing ware is scraped the feed liquid into one deck extremely thin, is turbulent liquid film immediately to impel downwards with the heliciform. In the process, light molecules escaping from the heating surface are condensed into liquid on an internal condenser (namely the stainless steel coil 1) through a short route almost without collision, flow down along the condenser pipe and are discharged through a discharge pipe (component interface) positioned at the bottom of the evaporator, residual liquid, namely heavy molecules, are collected in a channel below the heating area (here, the light molecules flowing down along the condenser, namely light component materials, are collected by a second sleeve with a side wall relatively close to the stainless steel coil 1, and the heavy molecules, namely heavy component materials, are collected by a first sleeve with a side wall relatively far away from the stainless steel coil 1), and in addition, a cold trap connector 5 is arranged on the outer side wall of the bottom of the second sleeve and is used for transferring the escaping molecules but uncondensed materials (gas materials) to a next reaction device for further component separation or discharging as waste materials.
The slope of first sleeve and the telescopic bottom face of second sets up, the component interface is located the first sleeve that self connects or the telescopic lateral wall bottommost department of second, the slope of bottom face sets up, inner chamber diapire is not parallel to the horizontal plane in first sleeve and the second sleeve promptly, the material is convenient for concentrate on the inner chamber bottommost department, the component interface is a pipeline structure, the component interface on the second sleeve is light component interface 3, a material for collecting touching the condenser pipe and condensing the whereabouts, the component interface on the first sleeve is heavy component interface 6, a raffinate that is not heated to the effusion by the intermediate layer on being used for accepting 8 inner chamber lateral walls of glass main part, the bottom of light component interface 3 and heavy component structure all is connected with the glass receiving flask 13 that is used for collecting the material.
The working principle is as follows: replace into 8 lower half stainless steel bases of first glass main part with integral type glass main part 8 originally, during the removal transportation, the utility model discloses the molecular still mentioned can dismantle, and transportation pressure reduces, and can play reduce cost's effect to taking place the breakage, and in addition, stainless steel base still can dispose not equidimension glass main part 8.
The basic principles and the main features of the invention and the advantages of the invention have been shown and described above. It should be understood by those skilled in the art that the present invention is not limited to the above embodiments, and that various changes and modifications may be made without departing from the spirit and scope of the invention, and such changes and modifications fall within the scope of the claimed invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (4)
1. The utility model provides a molecular distillation ware, includes the evaporimeter body, the top region of evaporimeter body includes motor (11), shaft coupling (12) and closing cap from top to bottom, the middle part region of evaporimeter body is provided with glass main part (8), be provided with the intermediate layer that is used for circulating the heat source in the regional lateral wall in middle part of glass main part (8), the intercommunication has an inlet pipe on the regional lateral wall in top of glass main part (8), glass main part (8) inner chamber top is provided with the knifing ware, its characterized in that: the bottom region of evaporimeter body is provided with the base, the base is stainless steel material, the base includes first sleeve and second sleeve, first sleeve and second sleeve are the drum structure, the top department of drum structure all is provided with the opening, first sleeve with axis collineation and axis perpendicular to horizontal plane between them of second sleeve, first telescopic inner chamber diameter is greater than the telescopic lateral wall diameter of second, the telescopic top inlay card of second is in first telescopic diapire middle part, first telescopic top lateral wall department is provided with stainless steel flange (2), be provided with second glass flange (9) on the bottom lateral wall of glass main part (8), stainless steel flange (2) with second glass flange (9) carry out fixed connection through the bolt, telescopic inner chamber diapire middle part fixedly connected with stainless steel coil (1) of second, stainless steel coil (1) upwards extend to in the sleeve inner chamber, first sleeve with the telescopic lateral wall bottom has all seted up the component interface.
2. A molecular still according to claim 1 wherein: and heat-conducting medium inlets and outlets (10) are formed in the top and the bottom of the outer side wall of the middle area of the glass main body (8), and each heat-conducting medium inlet and outlet (10) is communicated with the interlayer.
3. A molecular still according to claim 1 wherein: the bottom end of the stainless steel coil (1) is located under the second sleeve, and two cooling liquid inlets and outlets (4) are formed in the bottom end of the stainless steel coil (1).
4. A molecular still according to claim 1 wherein: the bottom end faces of the first sleeve and the second sleeve are obliquely arranged, and the component interface is located at the bottommost position of the outer side wall of the first sleeve or the second sleeve connected with the component interface.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222397194.6U CN218421078U (en) | 2022-09-09 | 2022-09-09 | Molecular distiller |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222397194.6U CN218421078U (en) | 2022-09-09 | 2022-09-09 | Molecular distiller |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218421078U true CN218421078U (en) | 2023-02-03 |
Family
ID=85103940
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202222397194.6U Active CN218421078U (en) | 2022-09-09 | 2022-09-09 | Molecular distiller |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218421078U (en) |
-
2022
- 2022-09-09 CN CN202222397194.6U patent/CN218421078U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103977592B (en) | The method of light naphtha is removed with the rectifier unit comprising two reboiler | |
| CN202724732U (en) | Circulating steam distillation device | |
| CN218421078U (en) | Molecular distiller | |
| CN106118707B (en) | Waste plastics innocent treatment equipment and method | |
| CN201658857U (en) | Rectifying tower for continuous rectification | |
| CN105567300A (en) | Solvent deasphalting extraction tower and method for solvent deasphalting | |
| CN206295742U (en) | A kind of dust-laden is pyrolyzed the full oil wash system of oil gas | |
| CN105126383A (en) | Traditional-Chinese-medicine efficient energy-saving automatic integrated extraction concentration technology and technological equipment | |
| CN110478930B (en) | Fractionating tower | |
| RU2466767C2 (en) | Heat-and-mass exchange vortex column | |
| CN106039750A (en) | Vacuum four-column differential pressure thermal coupling device and method for refining of crude phenol | |
| CN212090967U (en) | High boiling point heat-sensitive material distillation recovery system | |
| RU2683267C1 (en) | Installation for processing liquid hydrocarbons | |
| CN105694737A (en) | Distiller with corrugated surface for turpentine | |
| CN207126150U (en) | Vertical film evaporator is used in a kind of phosphatide processing | |
| CN2147500Y (en) | Heat-exchanger for fractional distillation, reaction and crystallizing | |
| CN207356608U (en) | A kind of return tank for MTBE devices | |
| CN208843995U (en) | A kind of condenser for naphtha processing | |
| CN102600627A (en) | Cyclone-flash cloth-film-reboiling-type heat-pipe distiller | |
| CN207738708U (en) | A kind of coal gas refrigerated separation device | |
| CN109758777A (en) | A kind of film flash rectifying column | |
| CN219630987U (en) | Internal steam removal device for screening | |
| CN111450561A (en) | Energy-saving carrier gas stripping system and stripping process | |
| CN202876405U (en) | Horizontal bi-shaft distillation device suitable for continuously separating sticky matters | |
| CN117398710B (en) | Rectifying column separator convenient to impurity separation |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: Building 5, No. 515 HSBC East Street, Jinshan District, Shanghai, 201518 Patentee after: Shanghai Yuanhuai Intelligent Technology Co.,Ltd. Address before: 201517 1st floor, building 16, Lane 691, Jianle Road, LvXiang Town, Jinshan District, Shanghai Patentee before: Shanghai Yuanhuai Industrial Co.,Ltd. |