CN218250247U

CN218250247U - Enamel reaction kettle for synthesis of 2-bromopropionic acid

Info

Publication number: CN218250247U
Application number: CN202222450905.1U
Authority: CN
Inventors: 徐建弟; 邹英伟
Original assignee: Changyi Fengrun Fine Chemical Co ltd
Current assignee: Changyi Fengrun Fine Chemical Co ltd
Priority date: 2022-09-16
Filing date: 2022-09-16
Publication date: 2023-01-10
Anticipated expiration: 2032-09-16

Abstract

The utility model relates to the technical field of enamel reaction kettles, in particular to an enamel reaction kettle for synthesizing 2-bromopropionic acid, which reduces the washing dead angle in a tank body and improves the cleaning effect of washing the interior of the tank body; including a jar body, water supply installation, the discharge valve, the steel pipe, the first stirring leaf of multiunit, the first shower nozzle of multiunit, the external member, multiunit straight tube and multiunit second shower nozzle, jar body top intercommunication is provided with the inlet pipe, the discharge valve intercommunication sets up in the inlet pipe bottom, jar body top is provided with water supply installation, steel pipe upper portion intercommunication and rotatory setting are in water supply installation, and the steel pipe passes through the water supply installation drive rotation, it is internal that the steel pipe lower part stretches into jar, the equal circumference of the first stirring leaf of multiunit is installed on the steel pipe lateral wall, the first shower nozzle of multiunit communicates the setting respectively on the steel pipe lateral wall, the external member top is connected with jar internal side wall top, and inside the steel pipe rotation passed the external member, the equal circumference of multiunit straight tube is installed on the external member lateral wall, the multiunit straight tube all communicates with water supply installation.

Description

Enamel reaction kettle for synthesis of 2-bromopropionic acid

Technical Field

The utility model relates to an enamel reactor's technical field especially relates to an enamel reactor is used in 2-bromopropionic acid synthesis.

Background

The enamel reactor is to contain the glass of the high silica dioxide, the lining is at the internal surface of steel container, burn and firmly adhere to the metal surface and become the combined material goods through the high temperature, at present the enamel reactor discovery when using when a kind of 2-bromopropionic acid synthetic processing, in prior art CN201820466126.1, this reation kettle includes the enamel reactor casing, the left side fixedly connected with feeding opening valve at enamel reactor casing top, the top swing joint of enamel reactor casing inner chamber has the agitator, but this reation kettle's spray pipe and sprinkler bead are fixed settings, produce the dead angle easily during washing, thereby reduce the inside clean effect of washing of reation kettle, consequently, propose one kind and reduce and wash the dead angle, improve and wash the enamel reactor of clean effect.

SUMMERY OF THE UTILITY MODEL

In order to solve the technical problem, the utility model provides a reduce the internal dead angle that washes of jar, improve the synthetic enamel reactor that uses of 2-bromopropionic acid of the clean effect that the internal portion of jar washed.

The utility model discloses a synthetic enamel reactor that uses of 2-bromopropionic acid, which comprises a tank body, a water supply installation, arrange the material valve, the steel pipe, multiunit first stirring leaf, multiunit first shower nozzle, the external member, multiunit straight tube and multiunit second shower nozzle, tank body top intercommunication is provided with the inlet pipe, arrange the material valve intercommunication and set up in the inlet pipe bottom, tank body top is provided with water supply installation, steel pipe upper portion intercommunication and rotation setting are in water supply installation, and the steel pipe passes through water supply installation drive rotation, the steel pipe lower part stretches into in the tank body, multiunit first stirring leaf all circumference is installed on the steel pipe lateral wall, multiunit first shower nozzle communicates respectively to set up on the steel pipe lateral wall, the external member top is connected with jar body inside wall top, and the steel pipe rotation passes inside the external member, multiunit straight tube all circumference is installed on the external member lateral wall, multiunit straight tube all communicates with water supply installation, multiunit second shower nozzle communicates respectively to set up in multiunit straight tube bottom; the method comprises the steps that firstly, 2-bromopropionic acid to be synthetically processed is placed in a tank body through a feeding pipe, then a steel pipe is driven to rotate through a water supply device, the steel pipe rotates and then drives a plurality of groups of first stirring blades to rotate, so that the plurality of groups of first stirring blades can synthetically stir and process the 2-bromopropionic acid in the tank body, after the 2-bromopropionic acid in the tank body is synthetically processed, a discharge valve is opened, the 2-bromopropionic acid in the tank body is discharged outwards, then the water is conveyed into the steel pipe through the water supply device, the water entering the steel pipe is sprayed outwards through the plurality of groups of first spray nozzles, and meanwhile, the plurality of groups of first spray nozzles are driven to rotate through the steel pipe, so that the inner side wall of the tank body is rotationally sprayed and washed through the plurality of groups of first spray nozzles, washing dead corners in the tank body are reduced, meanwhile, the water supply device conveys the water to a plurality of groups of straight pipes, the plurality of groups of second spray nozzles can wash the steel pipe, the plurality of first stirring blades and the inner side wall of the tank body, and further improve the cleaning effect of the inner side wall of the tank body.

Preferably, the water supply device comprises a conveying box, connecting pipes, a first motor, a water tank, a pressurizing device and water pipes, wherein the conveying box is arranged in the middle of the top end of the tank body, the top end of each steel pipe is rotatably arranged at the top of the inner side wall of the conveying box, a plurality of groups of water inlets are formed in the upper portion of each steel pipe and communicated with the conveying box, sealing filler is arranged at the joint of each steel pipe and the inner side wall of the conveying box, the top ends of the plurality of groups of connecting pipes are communicated with the conveying box, the bottom ends of the plurality of groups of connecting pipes are respectively communicated with a plurality of groups of straight pipes, the first motor is arranged at the top end of the conveying box, the output end of the first motor is concentrically connected with the top end of each steel pipe, the top end of the water tank is communicated with a water inlet valve, the pressurizing device is communicated with the water tank, the input end of each water pipe is communicated with the bottom of the water tank, and the output end of each water pipe is communicated with the conveying box; open first motor and drive the steel pipe rotatory, make the rotatory back of the first stirring leaf of multiunit mix the stirring with the internal 2-bromopropionic acid of jar, place water inside the water tank through inlet valve with water, later with water tank internal seal, through supercharging device to ram air in the water tank, thereby make the water in the water tank receive air pressure to lead to pipe outside transport, water passes through the water pipe and gets into inside the delivery box, later the water in the delivery box passes through inside the multiunit water inlet gets into the steel pipe, simultaneously the water in the delivery box passes through inside the multiunit connecting pipe gets into the multiunit straight tube, thereby improve the convenience of the first shower nozzle of multiunit and multiunit second shower nozzle to the washing clearance of jar internal portion, improve the washing clearance effect of jar internal.

Preferably, the supercharging device comprises a barrel, a one-way air inlet valve, an air pipe, a second motor, a connecting arm, a piston and a one-way exhaust valve, the barrel is mounted on the outer side wall of the water tank, an opening is formed in the bottom end of the barrel, the one-way air inlet valve is communicated and arranged on the upper portion of the outer side wall of the barrel, the input end of the air pipe is communicated and arranged at the top end of the barrel, the output end of the air pipe is communicated and arranged at the top end of the water tank, a disc is arranged at the output end of the second motor, the bottom end of the connecting arm is rotatably mounted on the eccentric position of the outer side wall of the disc, the top end of the connecting arm is rotatably connected with the bottom end of the piston, the piston is arranged in the middle of the barrel in a vertical sliding mode, and the one-way exhaust valve is communicated and arranged on the air pipe; the second motor is started to drive the disc to rotate, the disc drives the piston to reciprocate up and down through the connecting arm after rotating, outdoor air is sucked into the upper portion of the cylinder through the one-way air inlet valve when the piston moves down, then the piston moves up, the air on the upper portion of the cylinder is conveyed into the water tank through the air pipe by the piston, the punching efficiency in the water tank is improved, and the convenience of conveying water in the water tank outwards is improved.

Preferably, the tank also comprises a bracket, the bottom end of the bracket is connected with the bottom of the inner side wall of the tank body, and the upper part of the bracket is sleeved on the outer side wall of the steel pipe; through setting up the support, improve the rotatory stability of steel pipe, improve the use fastness of steel pipe.

Preferably, the device also comprises a sampling valve, and the sampling valve is communicated with and arranged at the lower part of the outer side wall of the tank body; by arranging the sampling valve, the convenience of sampling and detecting the 2-bromopropionic acid in the tank body is improved.

Preferably, the device also comprises a plurality of groups of scraping plates, wherein the scraping plates are respectively arranged at the front ends of the first stirring blades and are in contact with the inner side wall of the tank body; the first stirring leaf of multiunit drives multiunit scraper blade rotatory when rotatory, makes multiunit scraper blade scrape the adnexed 2-bromopropionic acid of jar internal side wall and clears up, improves the clearance convenience in the jar body.

Preferably, the device also comprises a plurality of groups of second stirring blades, and the plurality of groups of second stirring blades are all arranged at the lower part of the outer side wall of the steel pipe; the effect of mixing and stirring the bottom in the tank body is improved, and the condition of uneven synthesis caused by deposition of the 2-bromopropionic acid is reduced.

Compared with the prior art, the beneficial effects of the utility model are that: the method comprises the steps that firstly, 2-bromopropionic acid to be synthetically processed is placed in a tank body through a feeding pipe, then a steel pipe is driven to rotate through a water supply device, the steel pipe rotates and then drives a plurality of groups of first stirring blades to rotate, so that the plurality of groups of first stirring blades can synthetically stir and process the 2-bromopropionic acid in the tank body, after the 2-bromopropionic acid in the tank body is synthetically processed, a discharge valve is opened, the 2-bromopropionic acid in the tank body is discharged outwards, then the water is conveyed into the steel pipe through the water supply device, the water entering the steel pipe is sprayed outwards through the plurality of groups of first spray nozzles, and meanwhile, the plurality of groups of first spray nozzles are driven to rotate through the steel pipe, so that the inner side wall of the tank body is rotationally sprayed and washed through the plurality of groups of first spray nozzles, washing dead corners in the tank body are reduced, meanwhile, the water supply device conveys the water to a plurality of groups of straight pipes, the plurality of groups of second spray nozzles can wash the steel pipe, the plurality of first stirring blades and the inner side wall of the tank body, and further improve the cleaning effect of the inner side wall of the tank body.

Drawings

Fig. 1 is a schematic structural diagram of the present invention;

FIG. 2 is a partial structural view of the disk connected to a connecting arm or the like;

FIG. 3 is a partial structural view of the connection of the steel pipe with the first stirring vanes and the like;

FIG. 4 is a schematic view of a partial axial structure of a sleeve connected to a straight pipe or the like;

in the drawings, the reference numbers: 1. a tank body; 2. a feeding pipe; 3. a discharge valve; 4. a steel pipe; 5. a first stirring blade; 6. a first nozzle; 7. a kit; 8. a straight pipe; 9. a second spray head; 10. a delivery box; 11. a connecting pipe; 12. a first motor; 13. a water tank; 14. a water pipe; 15. a cylinder body; 16. a one-way intake valve; 17. an air tube; 18. a second motor; 19. a disc; 20. a connecting arm; 21. a support; 22. a sampling valve; 23. a squeegee; 24. a piston; 25. a one-way exhaust valve; 26. and a second stirring blade.

Detailed Description

In order to facilitate understanding of the present invention, the present invention will be described more fully hereinafter with reference to the accompanying drawings. The invention may be embodied in many different forms and is not limited to the embodiments described herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.

The top end of the tank body 1 is communicated with a feeding pipe 2, a discharge valve 3 is communicated with the bottom end of the feeding pipe 2, the lower part of a steel pipe 4 extends into the tank body 1, a plurality of groups of first stirring blades 5 are circumferentially arranged on the outer side wall of the steel pipe 4, a plurality of groups of first spray nozzles 6 are respectively communicated with the outer side wall of the steel pipe 4, the top end of a suite 7 is connected with the top part of the inner side wall of the tank body 1, the steel pipe 4 rotates to penetrate through the inside of the suite 7, a plurality of groups of straight pipes 8 are circumferentially arranged on the outer side wall of the suite 7, a plurality of groups of second spray nozzles 9 are respectively communicated with the bottom ends of the plurality of groups of straight pipes 8, a conveying box 10 is arranged in the middle part of the top end of the tank body 1, the top end of the steel pipe 4 is rotatably arranged at the top part of the inner side wall of the conveying box 10, a plurality of groups of water inlets are arranged at the upper part of the steel pipe 4 and communicated with the conveying box 10, the sealing filler is arranged at the joint of the inner side wall of the steel pipe 4 and the conveying box 10, the top ends of a plurality of connecting pipes 11 are communicated with the conveying box 10, the bottom ends of a plurality of groups of connecting pipes 11 are respectively communicated with a plurality of groups of straight pipes 8, a first motor 12 is arranged at the top end of a conveying box 10, the output end of the first motor 12 is concentrically connected with the top end of a steel pipe 4, the top end of a water tank 13 is communicated with a water inlet valve, the input end of a water pipe 14 is communicated with the bottom of the water tank 13, the output end of the water pipe 14 is communicated with the conveying box 10, a cylinder body 15 is arranged on the outer side wall of the water tank 13, the bottom end of the cylinder body 15 is provided with an opening, a one-way air inlet valve 16 is communicated with the upper part of the outer side wall of the cylinder body 15, the input end of an air pipe 17 is communicated with the top end of the cylinder body 15, the output end of the air pipe 17 is communicated with the top end of the water tank 13, the output end of a second motor 18 is provided with a disc 19, the bottom end of a connecting arm 20 is rotatably arranged at the eccentric position of the outer side wall of the disc 19, the top end of the connecting arm 20 is rotatably connected with the bottom end of a piston 24, the piston 24 is rotatably arranged in the middle part of the cylinder body 15 in a vertical sliding way, the one-way exhaust valve 25 is communicated with and arranged on the air pipe 17, the bottom end of the support 21 is connected with the bottom of the inner side wall of the tank body 1, the upper part of the support 21 is sleeved on the outer side wall of the steel pipe 4, the sampling valve 22 is communicated and arranged at the lower part of the outer side wall of the tank body 1, the multiple groups of scraping plates 23 are respectively arranged at the front ends of the multiple groups of first stirring blades 5, the multiple groups of scraping plates 23 are all contacted with the inner side wall of the tank body 1, and the multiple groups of second stirring blades 26 are all arranged at the lower part of the outer side wall of the steel pipe 4; firstly, 2-bromopropionic acid to be synthesized and processed is placed inside a tank body 1 through a feeding pipe 2, then a steel pipe 4 is driven to rotate through a water supply device, the steel pipe 4 drives a plurality of groups of first stirring blades 5 to rotate after rotating, so that the plurality of groups of first stirring blades 5 synthesize and stir the 2-bromopropionic acid in the tank body 1, after the 2-bromopropionic acid in the tank body 1 is synthesized and processed, a discharge valve 3 is opened, so that the 2-bromopropionic acid in the tank body 1 is discharged outwards, then the water is conveyed into the steel pipe 4 through the water supply device, the water entering the steel pipe 4 is sprayed outwards through the plurality of groups of first spray heads 6, and meanwhile, the plurality of groups of first spray heads 6 drive the plurality of groups of first spray heads 6 to wash the inner side wall of the tank body 1 in a rotating mode, so as to reduce the washing dead angle in the tank body 1, meanwhile, the water supply device conveys the water to the plurality of groups of straight pipes 8, so that the plurality of groups of second spray heads 9 wash the steel pipe 4, the plurality of groups of first stirring blades 5 and the inner side wall of the tank body 1, and further improve the cleaning effect of the inner side wall of the tank body 1.

As shown in figures 1 to 4, the enamel reactor for synthesizing 2-bromopropionic acid of the present invention is operated by placing 2-bromopropionic acid to be synthesized and processed into the tank 1 through the inlet pipe 2, opening the first motor 12 to drive the steel pipe 4 to rotate, rotating the plurality of sets of first stirring blades 5 to mix and stir the 2-bromopropionic acid in the tank 1, placing water into the tank 13 through the inlet valve when the tank 1 is to be cleaned, sealing the tank 13, opening the second motor 18 to drive the disc 19 to rotate, driving the piston 24 to reciprocate up and down through the connecting arm 20 after the disc 19 rotates, sucking outdoor air into the upper part of the cylinder 15 through the one-way air inlet valve 16 when the piston 24 moves down, then the piston 24 upwards moves, make the piston 24 pass through trachea 17 with the air on barrel 15 upper portion and carry to inside water tank 13, make the water in the water tank 13 receive air pressure and lead to pipe 14 outwards to carry, water passes through pipe 14 and gets into inside transport box 10, later the water in transport box 10 gets into inside steel pipe 4 through the multiunit water inlet, the water that gets into in steel pipe 4 sprays through multiunit first shower nozzle 6 outwards, it is rotatory to drive multiunit first shower nozzle 6 through steel pipe 4 simultaneously, make multiunit first shower nozzle 6 wash jar internal side wall rotation water spray of body 1, multiunit connecting pipe 11 carries water to multiunit straight tube 8 simultaneously, make multiunit second shower nozzle 9 wash steel pipe 4, multiunit first stirring leaf 5 and jar internal side wall of body 1.

The utility model discloses the main function who realizes does: carry water to inside 4 steel pipes through water supply installation, the water that gets into in the steel pipe 4 outwards sprays through the first shower nozzle of multiunit 6, it is rotatory to drive the first shower nozzle of multiunit 6 through steel pipe 4 simultaneously, thereby make the first shower nozzle of multiunit 6 wash the rotatory water spray of 1 inside wall of the jar body, reduce the dead angle that washes in 1 jar body, water supply installation carries water to multiunit straight tube 8 simultaneously, make multiunit second shower nozzle 9 with steel pipe 4, the first stirring leaf of

multiunit

5 and 1 inside wall of the jar body wash, and then improve the clean effect that 1 inside of the jar body washed.

The installation mode, the connection mode or the arrangement mode of the enamel reaction kettle for synthesizing the 2-bromopropionic acid are common mechanical modes, and the enamel reaction kettle can be implemented as long as the beneficial effects can be achieved; the utility model discloses a synthetic enamel reation kettle's of using of 2-bromopropionic acid first motor 12 and second motor 18 for purchase on the market, this industry technical staff only need according to its subsidiary operating specification install and operate can, and need not the technical staff in this field and pay out creative work.

All technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.

The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, a plurality of modifications and variations can be made without departing from the technical principle of the present invention, and these modifications and variations should also be regarded as the protection scope of the present invention.

Claims

1. The utility model provides a synthetic enamel reactor that uses of 2-bromopropionic acid, a serial communication port, which comprises a tank body (1), water supply installation, discharge valve (3), steel pipe (4), the first stirring leaf of multiunit (5), multiunit first shower nozzle (6), external member (7), multiunit straight tube (8) and multiunit second shower nozzle (9), jar body (1) top intercommunication is provided with inlet pipe (2), discharge valve (3) intercommunication sets up in inlet pipe (2) bottom, jar body (1) top is provided with water supply installation, steel pipe (4) upper portion intercommunication and rotatory setting are in water supply installation, and steel pipe (4) are rotatory through the water supply installation drive, steel pipe (4) lower part stretches into in jar body (1), the equal circumference of the first stirring leaf of multiunit (5) is installed on steel pipe (4) lateral wall, multiunit first shower nozzle (6) intercommunication sets up respectively on steel pipe (4) lateral wall, external member (7) top is connected with jar body (1) inside wall top, and steel pipe (4) are rotatory to pass through inside external member (7), multiunit straight tube (8) all install on external member (7) lateral wall, multiunit straight tube (8) circumference, multiunit straight tube (8) all communicates with multiunit second shower nozzle (9) bottom.

2. The enamel reactor for synthesizing 2-bromopropionic acid as claimed in claim 1, wherein the water supply device comprises a delivery box (10), a plurality of sets of water inlets (11), a first motor (12), a water tank (13), a pressurizing device and a water pipe (14), the delivery box (10) is installed in the middle of the top end of the tank body (1), the top end of the steel pipe (4) is rotatably installed at the top of the inner side wall of the delivery box (10), the upper portion of the steel pipe (4) is provided with a plurality of sets of water inlets which are communicated with the interior of the delivery box (10), a sealing filler is arranged at the joint of the inner side wall of the delivery box (10) and the steel pipe (4), the top ends of the plurality of sets of connection pipes (11) are communicated with the interior of the delivery box (10), the bottom ends of the plurality of sets of connection pipes (11) are respectively communicated with a plurality of straight pipes (8), the first motor (12) is installed at the top end of the delivery box (10), the output end of the first motor (12) is concentrically connected with the top end of the steel pipe (4), the top end of the water tank (13) is communicated with a water inlet valve, the pressurizing device is communicated with the water pipe (13), the input end of the water pipe (14) is arranged at the bottom of the water tank (13), and the output end of the delivery box (10).

3. The enamel reactor for synthesizing 2-bromopropionic acid as claimed in claim 2, wherein the pressurizing device comprises a cylinder (15), a one-way air inlet valve (16), an air pipe (17), a second motor (18), a connecting arm (20), a piston (24) and a one-way exhaust valve (25), the cylinder (15) is installed on the outer side wall of the water tank (13), an opening is formed in the bottom end of the cylinder (15), the one-way air inlet valve (16) is communicated and arranged on the upper portion of the outer side wall of the cylinder (15), the input end of the air pipe (17) is communicated and arranged on the top end of the cylinder (15), the output end of the air pipe (17) is communicated and arranged on the top end of the water tank (13), a disc (19) is arranged at the output end of the second motor (18), the bottom end of the connecting arm (20) is rotatably installed on the eccentric position of the outer side wall of the disc (19), the top end of the connecting arm (20) is rotatably connected with the bottom end of the piston (24), the piston (24) is vertically slidably arranged in the middle of the cylinder (15), and the one-way exhaust valve (25) is communicated and arranged on the air pipe (17).

4. The enamel reactor for synthesizing 2-bromopropionic acid as claimed in claim 1, further comprising a bracket (21), wherein the bottom end of the bracket (21) is connected with the bottom of the inner side wall of the tank body (1), and the upper part of the bracket (21) is sleeved on the outer side wall of the steel pipe (4).

5. The enamel reactor for synthesizing 2-bromopropionic acid as claimed in claim 1, further comprising a sampling valve (22), wherein the sampling valve (22) is communicated with and arranged at the lower part of the outer side wall of the tank body (1).

6. An enamel reactor for synthesizing 2-bromopropionic acid as claimed in claim 1, further comprising a plurality of sets of scrapers (23), wherein the sets of scrapers (23) are respectively installed at the front ends of the sets of first stirring blades (5), and the sets of scrapers (23) are all in contact with the inner side wall of the tank body (1).

7. An enamel reactor for synthesizing 2-bromopropionic acid as claimed in claim 1, further comprising a plurality of sets of second stirring vanes (26), wherein the plurality of sets of second stirring vanes (26) are installed at the lower portion of the outer side wall of the steel tube (4).