CN218076425U - Device for separating and purifying caprylic/capric glyceride - Google Patents
Device for separating and purifying caprylic/capric glyceride Download PDFInfo
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- CN218076425U CN218076425U CN202221682612.XU CN202221682612U CN218076425U CN 218076425 U CN218076425 U CN 218076425U CN 202221682612 U CN202221682612 U CN 202221682612U CN 218076425 U CN218076425 U CN 218076425U
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Abstract
The utility model provides a be used for caprylic capric acid glyceride separation purification device, including the heat-preserving container, be equipped with stills in the heat-preserving container, be equipped with the liquid reserve tank on the stills, be equipped with the coil pipe in the liquid reserve tank, last inlet and the gas outlet of being equipped with of stills, gas outlet and coil pipe one end intercommunication, the inlet communicates with the liquid outlet of liquid reserve tank, and the coil pipe other end is equipped with the storage jar, through communicating pipe intercommunication between coil pipe and the storage jar, and the communicating pipe outside is equipped with cooling coil pipe. The raw materials lets in through the paddle stirring in the stills, carry out the constant temperature heating through the heater simultaneously, the raw materials forms in steam enters into the coil pipe in the liquid reserve tank, thereby the raw materials through in the liquid reserve tank cools down to the steam in the coil pipe, the raw materials can preheat simultaneously, reduce the energy consumption of heater, cooling coil can also cool off communicating pipe, guarantee that the liquefaction of steam enters into in the storage jar, reduce the energy consumption of condenser, make full use of used heat reduces the energy consumption, the purification efficiency is greatly improved.
Description
Technical Field
The utility model relates to a field of caprylic capric acid glyceride production, concretely relates to be used for caprylic capric acid glyceride separation and purification device.
Background
Caprylic/capric triglyceride is high-purity grease formed by esterifying caprylic/capric acid and glycerol, is excellent moisturizing grease, has good spreadability, makes skin have a smooth but not greasy feeling, is easy to be absorbed by skin, plays a good role in uniform and fine cosmetics, makes skin smooth and glossy, and can be used as a base material of moisturizing factors, a stabilizer, an antifreezing agent and a homogenizing agent of the cosmetics.
In the production process of caprylic/capric glyceride, impurities are often left in the caprylic/capric glyceride formed after esterification reaction, so that the purity of the caprylic/capric glyceride is influenced, the high-purity caprylic/capric glyceride needs to be separated and purified, the existing distillation and purification device is simpler in design structure, high in distillation and heating energy consumption, high in condenser energy consumption, incapable of well recovering steam liquefaction waste heat and wasting energy.
SUMMERY OF THE UTILITY MODEL
The main object of the utility model is to provide a be used for caprylic capric acid glyceride separation and purification device, solve the problem among the above-mentioned background art.
In order to solve the technical problem, the utility model discloses the technical scheme who adopts is: including the heat-preserving container, be equipped with stills in the heat-preserving container, be equipped with the liquid reserve tank on the stills, be equipped with the coil pipe in the liquid reserve tank, last inlet and the gas outlet of being equipped with of stills, gas outlet and coil pipe one end intercommunication, the inlet communicates with the liquid outlet of liquid reserve tank, and the coil pipe other end is equipped with storage jar, communicates through communicating pipe between coil pipe and the storage jar, and the communicating pipe outside is equipped with cooling coil pipe.
In the preferred scheme, be equipped with the heater in the heat-preserving container, the heater is used for heating it outside the stills, and the heater has temperature controller to be in invariable high temperature in making the stills.
In the preferred scheme, a motor is fixedly arranged on the distillation still, a rotating paddle is arranged in the distillation still, and the paddle is fixedly connected with the motor.
In a preferable scheme, two ends of the cooling coil are circularly communicated with the condenser.
In the preferred scheme, a temperature sensor is fixedly arranged in the liquid storage tank.
The utility model provides a be used for caprylic capric acid glyceride separation and purification device, the raw materials lets in the stills in through the paddle stirring, carry out the constant temperature heating through the heater simultaneously, the raw materials forms in the coil pipe that steam entered into in the liquid reserve tank, thereby the steam to the coil pipe in through the raw materials in the liquid reserve tank cools down, the raw materials can preheat simultaneously, reduce the energy consumption of heater, cooling coil can also cool off communicating pipe, guarantee that the liquefaction of steam enters into in the storage jar, reduce the energy consumption of condenser, make full use of used heat reduces the energy consumption, improve purification efficiency greatly.
Drawings
The invention will be further explained with reference to the following figures and examples:
FIG. 1 is a schematic view of the connection of the overall structure of the present invention;
FIG. 2 is a front sectional view of the overall structure of the present invention;
in the figure: a heat-preserving container 1; a distillation kettle 2; a motor 3; a liquid storage tank 4; a communicating pipe 5; a cooling coil 6; a storage tank 7; a heater 8; a paddle 9; a coil 10; a temperature sensor 11.
Detailed Description
Example 1
As shown in fig. 1 to 2, a separation and purification device for caprylic/capric glyceride comprises a heat-preserving container 1, a distillation kettle 2 is arranged in the heat-preserving container 1, a liquid storage tank 4 is arranged on the distillation kettle 2, a coil pipe 10 is arranged in the liquid storage tank 4, a liquid inlet and a gas outlet are arranged on the distillation kettle 2, the gas outlet is communicated with one end of the coil pipe 10, the liquid inlet is communicated with the liquid outlet of the liquid storage tank 4, a storage tank 7 is arranged at the other end of the coil pipe 10, the coil pipe 10 is communicated with the storage tank 7 through a communicating pipe 5, and a cooling coil pipe 6 is arranged outside the communicating pipe 5. By this structure, the raw materials is stored in liquid reserve tank 4, lets in and heats the stirring in stills 2 to form the coil pipe 10 that steam entered into in the liquid reserve tank 4, cool down steam through microthermal raw materials, can preheat the raw materials simultaneously, cooling coil 6 can further cool down steam, guarantees that the raw materials after the distillation purification enters into storage jar 7.
In the preferred scheme, be equipped with heater 8 in heat-preserving container 1, heater 8 is used for heating it in stills 2 outside, and heater 8 has temperature controller to be in invariable high temperature in making stills 2. From this structure, the temperature of controller control heater 8 to heating stills 2, guaranteeing that the raw materials in stills 2 is in the required temperature of distillation.
In the preferred scheme, a motor 3 is fixedly arranged on the distillation still 2, a rotating paddle 9 is arranged in the distillation still 2, and the paddle 9 is fixedly connected with the motor 3. With the structure, the motor 3 drives the blades 9 to rotate, so that the heating of the raw materials is accelerated, the heating uniformity is ensured, and the distillation and purification efficiency is improved.
In a preferred scheme, both ends of the cooling coil 6 are in circulating communication with the condenser. With the structure, the cooling liquid in the condenser is circularly led into the cooling coil 6, so that the steam raw material circulating in the communicating pipe 5 is rapidly cooled and liquefied to enter the storage tank 7.
In a preferred scheme, a temperature sensor 11 is fixedly arranged in the liquid storage tank 4. With the structure, the temperature sensor 11 can monitor the temperature of the raw material in the liquid storage tank 4, so that the temperature reduction degree of the steam in the coil pipe 10 is judged, and the power of the condenser is regulated.
The above-mentioned embodiments are merely preferred embodiments of the present invention, and should not be considered as limitations of the present invention, and the protection scope of the present invention should be defined by the technical solutions described in the claims, and includes equivalent alternatives of technical features in the technical solutions described in the claims. I.e., equivalent alterations and modifications within the scope of the invention, are also intended to be covered by the scope of this invention.
Claims (5)
1. A device for separating and purifying caprylic capric acid glyceride is characterized in that: including heat-preserving container (1), be equipped with stills (2) in heat-preserving container (1), be equipped with liquid reserve tank (4) on stills (2), be equipped with coil pipe (10) in liquid reserve tank (4), be equipped with inlet and gas outlet on stills (2), gas outlet and coil pipe (10) one end intercommunication, the inlet communicates with the liquid outlet of liquid reserve tank (4), the coil pipe (10) other end is equipped with storage jar (7), communicate through communicating pipe (5) between coil pipe (10) and the storage jar (7), communicating pipe (5) outside is equipped with cooling coil (6).
2. The device for separating and purifying glyceryl caprylate-caprate according to claim 1, wherein the device comprises: a heater (8) is arranged in the heat-preserving barrel (1), the heater (8) is used for heating the distillation kettle (2) at the outer side of the distillation kettle, and the heater (8) is provided with a temperature controller so as to enable the distillation kettle (2) to be at a constant high temperature.
3. The device for separating and purifying the caprylic capric glyceride as claimed in claim 1, which is characterized in that: a motor (3) is fixedly arranged on the distillation still (2), a rotating paddle (9) is arranged in the distillation still (2), and the paddle (9) is fixedly connected with the motor (3).
4. The device for separating and purifying the caprylic capric glyceride as claimed in claim 1, which is characterized in that: two ends of the cooling coil (6) are circularly communicated with the condenser.
5. The device for separating and purifying the caprylic capric glyceride as claimed in claim 1, which is characterized in that: a temperature sensor (11) is fixedly arranged in the liquid storage tank (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221682612.XU CN218076425U (en) | 2022-07-02 | 2022-07-02 | Device for separating and purifying caprylic/capric glyceride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221682612.XU CN218076425U (en) | 2022-07-02 | 2022-07-02 | Device for separating and purifying caprylic/capric glyceride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218076425U true CN218076425U (en) | 2022-12-20 |
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ID=84478977
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202221682612.XU Active CN218076425U (en) | 2022-07-02 | 2022-07-02 | Device for separating and purifying caprylic/capric glyceride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218076425U (en) |
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2022
- 2022-07-02 CN CN202221682612.XU patent/CN218076425U/en active Active
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: Yaojiagang chemical industry park, Dongshi Town, Zhijiang City, Yichang City, Hubei Province Patentee after: Hubei Chuyi New Materials Co.,Ltd. Address before: Yaojiagang chemical industry park, Dongshi Town, Zhijiang City, Yichang City, Hubei Province Patentee before: ZHIJIANG CHUYI CHEMICAL CO.,LTD. |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A device for separating and purifying caprylic acid and decanoic acid glycerides Effective date of registration: 20230628 Granted publication date: 20221220 Pledgee: Hubei Science and Technology Financing Guarantee Co.,Ltd. Pledgor: Hubei Chuyi New Materials Co.,Ltd. Registration number: Y2023980046084 |