CN216572602U - Preparation of mesoscopic structure carbon base nanometer cage is mixed machine with stirring - Google Patents
Preparation of mesoscopic structure carbon base nanometer cage is mixed machine with stirring Download PDFInfo
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- CN216572602U CN216572602U CN202122616974.0U CN202122616974U CN216572602U CN 216572602 U CN216572602 U CN 216572602U CN 202122616974 U CN202122616974 U CN 202122616974U CN 216572602 U CN216572602 U CN 216572602U
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Abstract
The utility model discloses a stirring mixer for preparing a mesoscopic carbon-based nano cage, which comprises an installation platform, wherein one side of the top end of the installation platform is fixedly provided with a muffle furnace, the other side of the top end of the installation platform is fixedly provided with a preparation box, the middle part of the top end of the installation platform is provided with a stirring mechanism, the stirring mechanism comprises a supporting column, a stirring cylinder, a support, a motor, a rotary disc, a magnetic stirring column, a stirring block and a discharge pipe, the stirring cylinder is fixed by fixing the supporting column at the top end of the installation platform, the motor is fixed by fixing the support at the top end of the stirring cylinder, the rotary disc is driven to rotate by the rotation of the motor, the magnetic stirring column is driven to rotate by the rotation of the rotary disc, so that raw materials in the stirring cylinder are stirred, the stirring block is fixedly arranged on the outer side of the magnetic stirring column, when the magnetic stirring column rotates, the raw materials are stirred more fully and are mixed, thereby improving the quality of the product.
Description
Technical Field
The utility model relates to the technical field of preparation of carbon-based nanocages, in particular to a stirring mixer for preparation of a mesoscopic carbon-based nanocage.
Background
The design and development of an energy storage device with high energy density and high power density are the pursuit targets, an electric double layer super capacitor (EDLCs) stores energy by rapidly adsorbing electrolyte ions on an electrode/electrolyte interface, and has the advantages of high power density, high charging and discharging speed, long cycle life and the like, sp2 nanocarbon has good conductivity, various morphologies and high physicochemical stability, and is the most commonly used EDLCs electrode material at present, the pore structure of a carbon material plays a key role in EDLCs performance, macropores can reduce diffusion distance as an ion buffer library, mesopores can provide a rapid channel and a large surface area for ion transportation and charge storage, and micropores can further increase charge storage, so the excellent EDLCs performance usually needs the balance among macropores, mesopores and micropores, and the 3D mesoscopic nanocarbon carbon has good pore structure and high specific surface area, electrode materials for EDLCs that are considered promising;
however, in the mesostructured carbon-based nanocage devices in the current market, raw materials are often required to be mixed when products are prepared, and insufficient mixing in the mixing process can cause the products to fail to meet the requirements, thereby affecting the product quality.
SUMMERY OF THE UTILITY MODEL
The utility model provides a stirring mixer for preparing a mesostructure carbon-based nanocage, which can effectively solve the problem that the prior mesostructure carbon-based nanocage device in the market is provided in the background art, raw materials are often required to be mixed when a product is prepared, and the product cannot meet the requirement due to insufficient mixing in the mixing process, so that the product quality is influenced.
In order to achieve the purpose, the utility model provides the following technical scheme: a stirring mixer for preparing a mesoscopic structure carbon-based nano cage comprises an installation table, wherein a muffle furnace is fixedly installed on one side of the top end of the installation table, a preparation box is fixedly installed on the other side of the top end of the installation table, and a stirring mechanism is arranged in the middle of the top end of the installation table;
the stirring mechanism comprises a supporting column, a stirring drum, a bracket, a motor, a turntable, a magnetic stirring column, a stirring block and a discharging pipe;
the utility model discloses a magnetic stirring device, including mount table, mount table top, support column, magnetic stirring post, agitator, stand, support, motor output shaft, carousel, magnetic stirring piece, stand top middle part fixed mounting has the support column, support column top fixed mounting has the churn, churn top fixed mounting has the support, support bottom middle part fixed mounting has the motor, motor output shaft bottom fixed mounting has the carousel, carousel bottom symmetry fixed mounting has the magnetic stirring post, magnetic stirring post outside fixed mounting has the stirring piece, churn bottom middle part fixed mounting has the discharging pipe.
Preferably, the input end of the motor is electrically connected with the output end of an external power supply, and a valve is arranged on the outer side of the discharge pipe.
Preferably, a filtering mechanism is arranged inside the preparation box;
the filtering mechanism comprises a liquid inlet pipe, a pump, a liquid outlet pipe, a fixed block, a filtering box, a filtering screen and a guide pipe;
discharging pipe bottom fixed mounting has the feed liquor pipe, feed liquor pipe top fixed mounting has the pump machine, pump machine top middle part fixed mounting has the drain pipe, the inside symmetry fixed mounting of preparation case has the fixed block, two fixed mounting has the filter cartridge between the fixed block, the inside fixed mounting of filter cartridge has the filter screen, filter cartridge bottom fixed mounting has the pipe.
Preferably, filter cartridge middle part and drain pipe bottom coincidence, drain pipe and pipe run through fixed mounting respectively in preparation roof portion and one side, and all be provided with the sealing washer between the drain pipe and the pipe outside and preparation roof portion and one side, pipe one end is provided with collects the box, the input of pump machine and external power source's output electric connection.
Preferably, a heating mechanism is arranged inside the preparation box;
the heating mechanism comprises a heating box, a heat conduction pipe, a heating wire, an air suction pump and an air inlet pipe;
the heating box is symmetrically and fixedly arranged inside the preparation box, the heating pipes are fixedly arranged inside the heating box, heating wires are fixedly arranged inside the heating pipes, an air suction pump is fixedly arranged at the bottom of one side of the preparation box, and an air inlet pipe is fixedly arranged at the top of one side of the preparation box.
Preferably, the input of heater strip and aspiration pump all with external power source's output electric connection, the intake pipe all is provided with the check valve with the outside of pipe, aspiration pump bottom end fixed connection is in the mount table top.
Compared with the prior art, the utility model has the beneficial effects that: the utility model has scientific and reasonable structure and safe and convenient use:
1. the stirring mechanism is arranged, the stirring cylinder is fixed through the fixed supporting column at the top end of the mounting table, the motor is fixed through the fixed mounting support at the top end of the stirring cylinder, the rotating disc is driven to rotate through the rotation of the motor, the magnetic stirring column is driven to rotate through the rotation of the rotating disc, so that raw materials in the stirring cylinder are stirred, and the stirring block is fixedly mounted on the outer side of the magnetic stirring column, so that the raw materials are stirred more fully when the magnetic stirring column rotates, the raw materials are fully mixed, and the quality of a product is improved;
2. the filter mechanism is arranged, the pump is fixed through the liquid inlet pipe fixedly arranged at the bottom end of the discharge pipe, the mixed raw materials in the mixing drum are fed into the preparation box through the operation of the pump, the filter box is fixed inside the preparation box through the fixing block, the raw materials fall into the filter box after entering the preparation box, and the raw materials are filtered through the filter screen, so that components in the raw materials are convenient to extract, the subsequent processing is convenient, and the preparation efficiency is improved;
3. the heating mechanism is arranged, the heat pipe is fixed through the fixed mounting heating box in the preparation box, the heating is carried out through the heating wire fixedly mounted in the inner part of the heat pipe, the temperature of the heat pipe is increased through the heating of the heating wire, the temperature of the heating box is increased, the temperature in the inner part of the preparation box is increased, the preparation box is in a vacuum state through air suction of the air suction pump, the raw materials after filtration are dried conveniently, then argon is introduced into the preparation box through the air inlet pipe, the raw materials are continuously heated, the deposition of the carbon nano cage is completed, the heating of the product is more uniform, the product quality is improved, the product preparation is accelerated, and the preparation efficiency is improved.
Drawings
The accompanying drawings, which are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate embodiments of the utility model and together with the description serve to explain the principles of the utility model and not to limit the utility model.
In the drawings:
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of the stirring mechanism of the present invention;
FIG. 3 is a schematic view of the filter mechanism of the present invention;
FIG. 4 is a schematic view of the heating mechanism of the present invention;
reference numbers in the figures: 1. an installation table; 2. a muffle furnace; 3. preparing a box;
4. a stirring mechanism; 401. a support pillar; 402. a mixing drum; 403. a support; 404. a motor; 405. a turntable; 406. a magnetic stirring column; 407. stirring blocks; 408. a discharge pipe;
5. a filtering mechanism; 501. a liquid inlet pipe; 502. a pump machine; 503. a liquid outlet pipe; 504. a fixed block; 505. a filter cartridge; 506. filtering with a screen; 507. a conduit;
6. a heating mechanism; 601. a heating box; 602. a heat conducting pipe; 603. heating wires; 604. an air pump; 605. an air inlet pipe.
Detailed Description
The preferred embodiments of the present invention will be described in conjunction with the accompanying drawings, and it will be understood that they are described herein for the purpose of illustration and explanation and not limitation.
Example (b): as shown in fig. 1-4, the utility model provides a stirring mixer for preparing a mesoscopic carbon-based nano cage, which comprises an installation table 1, wherein one side of the top end of the installation table 1 is fixedly provided with a muffle furnace 2, the other side of the top end of the installation table 1 is fixedly provided with a preparation box 3, and the middle part of the top end of the installation table 1 is provided with a stirring mechanism 4 for fully mixing raw materials;
the stirring mechanism 4 comprises a supporting column 401, a stirring drum 402, a bracket 403, a motor 404, a turntable 405, a magnetic stirring column 406, a stirring block 407 and a discharge pipe 408;
the middle of the top end of the mounting table 1 is fixedly provided with a support column 401, the top end of the support column 401 is fixedly provided with a stirring barrel 402, the top end of the stirring barrel 402 is fixedly provided with a support 403, the middle of the bottom end of the support 403 is fixedly provided with a motor 404, the bottom end of an output shaft of the motor 404 is fixedly provided with a turntable 405, the bottom end of the turntable 405 is symmetrically and fixedly provided with magnetic stirring columns 406, the outer side of each magnetic stirring column 406 is fixedly provided with a stirring block 407, and the middle of the bottom end of the stirring barrel 402 is fixedly provided with a discharge pipe 408.
The input end of the motor 404 is electrically connected with the output end of the external power supply, and the outer side of the discharge pipe 408 is provided with a valve.
In order to filter the mixed raw materials, a filtering mechanism 5 is arranged inside the preparation box 3;
the filtering mechanism 5 comprises a liquid inlet pipe 501, a pump 502, a liquid outlet pipe 503, a fixed block 504, a filter box 505, a filter screen 506 and a guide pipe 507;
discharging pipe 408 bottom fixed mounting has feed liquor pipe 501, and feed liquor pipe 501 top fixed mounting has pump machine 502, and pump machine 502 top middle part fixed mounting has drain pipe 503, and the inside symmetry fixed mounting of preparation case 3 has fixed block 504, and fixed mounting has filter box 505 between two fixed blocks 504, and the inside fixed mounting of filter box 505 has filter screen 506, and filter box 505 bottom fixed mounting has pipe 507.
The middle part of the filter box 505 coincides with the bottom end of the liquid outlet pipe 503, the liquid outlet pipe 503 and the guide pipe 507 penetrate through and are fixedly installed at the top and one side of the preparation box 3 respectively, a sealing ring is arranged between the outer side of the liquid outlet pipe 503 and the outer side of the guide pipe 507 and the top and one side of the preparation box 3, one end of the guide pipe 507 is provided with a collection box, and the input end of the pump 502 is electrically connected with the output end of an external power supply.
In order to dry the raw materials and prepare the products, a heating mechanism 6 is arranged inside the preparation box 3;
the heating mechanism 6 comprises a heating box 601, a heat conduction pipe 602, a heating wire 603, an air suction pump 604 and an air inlet pipe 605;
the heating boxes 601 are symmetrically and fixedly installed inside the preparation box 3, the heat conduction pipes 602 are fixedly installed inside the two heating boxes 601, the heating wires 603 are fixedly installed inside the heat conduction pipes 602, the air suction pump 604 is fixedly installed at the bottom of one side of the preparation box 3, and the air inlet pipe 605 is fixedly installed at the top of one side of the preparation box 3.
The input ends of the heating wire 603 and the air pump 604 are electrically connected with the output end of an external power supply, the air inlet pipe 605 and the outer side of the conduit 507 are provided with one-way valves, and the bottom end of the air pump 604 is fixedly connected to the top end of the mounting table 1.
The working principle and the using process of the utility model are as follows: in the practical application process, the power supply is turned on, the basic magnesium carbonate is put into the muffle furnace 2 to be heated to obtain the mesoscopic MgO, then the MgO is taken out and put into the stirring cylinder 402, and then the Zn (NO) is contained3)2·6H2The ethanol solution of O is poured into the mixing drum 402, the motor 404 is started, the rotating disc 405 is driven to rotate by the operation of the motor 404, the magnetic mixing column 406 is driven to rotate by the rotation of the rotating disc 405, and the mixing block 407 is fixedly arranged on the outer side of the magnetic mixing column 406, so that the mixing effect is improved, and the raw materials are fully and uniformly mixed;
after the raw materials are mixed, a valve on the outer side of a discharge pipe 408 is opened, a pump 502 is opened, the mixed solution in a stirring cylinder 402 is sent into a filter box 505 in a preparation box 3 from a liquid outlet pipe 503 through the pump 502, a one-way valve on the outer side of a guide pipe 507 is opened, the mixed solution is filtered through a filter screen 506, and the filtered solution is conveyed into a collection box through the guide pipe 507, so that the material waste is avoided;
after the raw materials are filtered, drying the filtered products, closing a one-way valve outside a conduit 507 and an air inlet pipe 605 to form a closed space in a preparation box 3, opening an air extraction pump 604 to extract air in the preparation box 3 to form vacuum in the preparation box 3, opening a switch of a heating wire 603, heating the heat conduction pipe 602 by the heating wire 603 to raise the temperature of a heating box 601 to raise the temperature in the preparation box 3 to dry the raw materials in the vacuum, after drying, closing the air extraction pump 604, opening the one-way valve of the air inlet pipe 605, conveying argon into the preparation box 3 by the air inlet pipe 605 to fill the argon into the preparation box 3 to form an argon inert atmosphere, then heating to a growth temperature at a rate of 5-10 ℃/min to perform carbon nano cage deposition, after the reaction is finished, naturally cooling to room temperature, and (3) obtaining a product sample, soaking the sample in dilute acid, washing to remove the MgO template, filtering, washing for multiple times, and drying to obtain the product.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the utility model. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (6)
1. The utility model provides a preparation of mesoscopic structure carbon base nanometer cage is with stirring machine, includes mount table (1), mount table (1) top one side fixed mounting has muffle furnace (2), mount table (1) top opposite side fixed mounting has preparation case (3), its characterized in that: a stirring mechanism (4) is arranged in the middle of the top end of the mounting table (1);
the stirring mechanism (4) comprises a supporting column (401), a stirring barrel (402), a bracket (403), a motor (404), a turntable (405), a magnetic stirring column (406), a stirring block (407) and a discharge pipe (408);
mounting table (1) top middle part fixed mounting has support column (401), support column (401) top fixed mounting has churn (402), churn (402) top fixed mounting has support (403), support (403) bottom middle part fixed mounting has motor (404), motor (404) output shaft bottom fixed mounting has carousel (405), carousel (405) bottom symmetry fixed mounting has magnetism stirring post (406), magnetism stirring post (406) outside fixed mounting has stirring piece (407), churn (402) bottom middle part fixed mounting has discharging pipe (408).
2. The stirring mixer for preparing the mesostructured carbon-based nanocage as claimed in claim 1, wherein the input end of the motor (404) is electrically connected with the output end of an external power supply, and the outer side of the discharge pipe (408) is provided with a valve.
3. The mixing mixer for the preparation of mesostructured carbon-based nanocages according to claim 1, wherein a filtering mechanism (5) is arranged inside the preparation box (3);
the filtering mechanism (5) comprises a liquid inlet pipe (501), a pump (502), a liquid outlet pipe (503), a fixing block (504), a filtering box (505), a filter screen (506) and a guide pipe (507);
discharging pipe (408) bottom fixed mounting has feed liquor pipe (501), feed liquor pipe (501) top fixed mounting has pump machine (502), pump machine (502) top middle part fixed mounting has drain pipe (503), preparation case (3) inside symmetry fixed mounting has fixed block (504), two fixed mounting has filter cartridge (505) between fixed block (504), filter cartridge (505) inside fixed mounting has filter screen (506), filter cartridge (505) bottom fixed mounting has pipe (507).
4. The stirring mixer for preparing the mesostructured carbon-based nanocage as claimed in claim 3, wherein the middle part of the filter box (505) coincides with the bottom end of the liquid outlet pipe (503), the liquid outlet pipe (503) and the guide pipe (507) are respectively fixedly installed at the top and one side of the preparation box (3) in a penetrating manner, sealing rings are respectively arranged between the outer sides of the liquid outlet pipe (503) and the guide pipe (507) and the top and one side of the preparation box (3), one end of the guide pipe (507) is provided with a collection box, and the input end of the pump (502) is electrically connected with the output end of an external power supply.
5. The mixing mixer for preparation of mesostructured carbon-based nanocages according to claim 1, wherein a heating mechanism (6) is arranged inside the preparation box (3);
the heating mechanism (6) comprises a heating box (601), a heat conduction pipe (602), a heating wire (603), an air suction pump (604) and an air inlet pipe (605);
the inside symmetry fixed mounting of preparation case (3) has heating cabinet (601), two inside equal fixed mounting of heating cabinet (601) has heat pipe (602), the inside fixed mounting of heat pipe (602) has heater strip (603), preparation case (3) one side bottom fixed mounting has aspiration pump (604), preparation case (3) one side top fixed mounting has intake pipe (605).
6. The stirring mixer for preparing the mesostructured carbon-based nanocage according to claim 5, wherein the input ends of the heating wire (603) and the air pump (604) are electrically connected with the output end of an external power supply, the outer sides of the air inlet pipe (605) and the conduit (507) are respectively provided with a one-way valve, and the bottom end of the air pump (604) is fixedly connected to the top end of the mounting table (1).
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122616974.0U CN216572602U (en) | 2021-10-29 | 2021-10-29 | Preparation of mesoscopic structure carbon base nanometer cage is mixed machine with stirring |
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| CN202122616974.0U CN216572602U (en) | 2021-10-29 | 2021-10-29 | Preparation of mesoscopic structure carbon base nanometer cage is mixed machine with stirring |
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| CN216572602U true CN216572602U (en) | 2022-05-24 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2024011401A1 (en) * | 2022-07-11 | 2024-01-18 | 南京延长反应技术研究院有限公司 | Carbon nanocage preparation system and preparation method |
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2021
- 2021-10-29 CN CN202122616974.0U patent/CN216572602U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2024011401A1 (en) * | 2022-07-11 | 2024-01-18 | 南京延长反应技术研究院有限公司 | Carbon nanocage preparation system and preparation method |
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