CN216274456U - Special push rod for horizontal zone-melting graphite boat - Google Patents

Special push rod for horizontal zone-melting graphite boat Download PDF

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Publication number
CN216274456U
CN216274456U CN202122933815.3U CN202122933815U CN216274456U CN 216274456 U CN216274456 U CN 216274456U CN 202122933815 U CN202122933815 U CN 202122933815U CN 216274456 U CN216274456 U CN 216274456U
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push rod
graphite boat
fork head
horizontal
hook
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CN202122933815.3U
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房现阁
柯尊斌
王卿伟
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China Germanium Co ltd
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China Germanium Co ltd
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Abstract

The utility model discloses a special push rod for a horizontal zone-melting graphite boat, which comprises a push rod handle, a push rod, a fork head and a hook, wherein the push rod handle is connected with the fork head; one end of the push rod is connected with a push rod handle, the other end of the push rod is connected with the fork head, a horizontal bubble is arranged on the side wall of the push rod handle, which is connected with one end of the push rod, the push rod handle and the push rod are both straight rod-shaped and are arranged coaxially, and the axis of the push rod is collinear with the central line of the fork head; the hook is in a 1-shaped structure, the hook is vertically connected to the end part of the push rod connected with one end of the fork head, and the plane where the hook and the fork head are located is vertical to each other. The device is convenient to operate, reduces the difficulty of the operation technology, can quickly complete the charging operation, saves time and improves the production efficiency; the graphite boat containing the materials in each quartz tube can be ensured to be in a horizontal state, the thicknesses of the spindles discharged from the furnace are kept consistent, the probability of occurrence of defective products is reduced, and the product quality is guaranteed.

Description

Special push rod for horizontal zone-melting graphite boat
Technical Field
The utility model relates to a special push rod for a horizontal zone-melting graphite boat, and belongs to the technical field of zone-melting germanium ingot devices.
Background
The horizontal zone melting method is that according to different segregation coefficients of different materials, raw materials in a graphite boat are heated by high-frequency induction, the head raw materials are melted into liquid, a formed melting zone slowly moves from the head to the tail in a horizontal state, and impurities are melted into the melting zone and gradually brought to the tail in the process. The process is repeated for a plurality of times, and finally the high-purity material is obtained. The horizontal zone melting method is generally used for purifying materials such as germanium, gallium arsenide and the like. Taking the horizontal zone melting method for producing germanium ingots as an example, a graphite boat is usually used to zone-melt germanium material, and a semi-open graphite boat is placed in front of and behind the graphite boat (see fig. 1). During charging, the graphite boats are sequentially arranged in the quartz tube according to the figure 1, a push rod is used in the process, the push rod is used for pushing the graphite boat containing the germanium materials to a specified position in the quartz tube, and the head of the graphite boat containing the germanium materials is positioned in a right coil shown in the figure 1. The push rod (see figure 2) used at present is simple and has no horizontal calibration function, the material-containing graphite boat is pushed to a designated position horizontally by experience during use, and in order to keep the material-containing graphite boat horizontal, the push rod is required to be slow in operation, and the horizontal state of the material-containing graphite boat in the quartz tube needs to be continuously observed and timely adjusted. The process has higher requirement on an operator, not only consumes time, but also can not ensure that the graphite boat is in a horizontal state, and the problem of uneven thickness of the germanium ingot (influencing product test and quality) caused by the inclination of the pushed graphite boat often occurs at the same time.
SUMMERY OF THE UTILITY MODEL
Aiming at the problems of the existing push rod, the utility model provides a special push rod for a horizontal zone-melting graphite boat, which aims to solve the problems of inconvenient operation, uneven spindle thickness and low production efficiency in the production process.
In order to solve the technical problems, the technical scheme adopted by the utility model is as follows:
a special push rod for a horizontal zone-melting graphite boat comprises a push rod handle, a push rod, a fork head and a hook; one end of the push rod is connected with a push rod handle, the other end of the push rod is connected with the fork head, a horizontal bubble is arranged on the side wall of the push rod handle, which is connected with one end of the push rod, the push rod handle and the push rod are both straight rod-shaped and are arranged coaxially, and the axis of the push rod is collinear with the central line of the fork head; the hook is in a 1-shaped structure, the hook is vertically connected to the end part of the push rod connected with one end of the fork head, and the plane where the hook and the fork head are located is vertical to each other.
The use method of the special push rod for the horizontal zone-melting graphite boat comprises the following steps: firstly placing a half-open type graphite boat into a quartz tube, then placing a material-containing zone-melting graphite boat into the quartz tube, then using a fork head of a special push rod to fork the zone-melting graphite boat, quickly pushing the material-containing zone-melting graphite boat to a specified position in the quartz tube, then slightly swinging a push rod handle left and right to enable bubbles in a horizontal bubble to be located at a central position, namely, the material-containing graphite boat is located at a horizontal position, and finally placing the other half-open type graphite boat into the quartz tube and contacting the material-containing graphite boat, thereby completing furnace charging operation. When the graphite boat is taken out from the quartz tube, the hook of the push rod hooks the inner wall of the head of the graphite boat and is pulled outwards slightly.
In order to improve the stability of use, the fork head is in a U-shaped structure. The neutral line of the prong is also the line that bisects the prong into two halves.
The horizontal bubble is arranged on the side wall of the corresponding push rod handle when the fork head is horizontal, namely when the fork head is horizontal, the horizontal bubble is also in the horizontal position. This facilitates horizontal calibration. Horizontal bubble and hook are located the both sides of push rod respectively, and during the use, horizontal bubble is last all the time, can not influence the use of horizontal bubble because of the setting of hook.
The fork head is made of stainless steel or plastic. This ensures the structural strength and the stability of the device in use, and also ensures the low-cost property of manufacture.
In order to facilitate use and simultaneously give consideration to the use stability of propulsion, the width of the inner side of the fork head is 1 mm-2 mm larger than that of the zone-melting graphite boat. Therefore, the graphite boat can be conveniently forked in a district, and the stability of the propelling process can be ensured.
In order to meet the requirement of industrial production, the length of the push rod is twice that of the float-zone graphite boat.
The push rod is made of stainless steel or plastic. This ensures the structural strength and the stability of the device in use, and also ensures the low-cost property of manufacture.
The length of the push rod handle is 1/4-1/6 of the length of the push rod, so that the use is convenient, and the use stability is ensured.
In order to avoid the hand slip and improve the estimation stability, the push rod handle is provided with four parallel grooves, and the length direction of the grooves is mutually vertical to the axial direction of the push rod handle.
The prior art is referred to in the art for techniques not mentioned in the present invention.
The push rod special for the horizontal zone-melting graphite boat is convenient to operate, reduces the difficulty of operation technology, can quickly complete furnace charging operation, saves time and improves production efficiency; on the other hand, the material-containing graphite boats in the quartz tubes are ensured to be in a horizontal state, the thicknesses of the spindles discharged from the furnace are kept consistent, the probability of defective products is reduced, and the product quality is guaranteed.
Drawings
FIG. 1 is a schematic view of a horizontal zone-melting graphite boat;
FIG. 2 is a schematic view of a push rod of a conventional graphite boat;
FIG. 3 is a top view of the push rod dedicated for horizontal zone-melting graphite boat in accordance with the present invention;
FIG. 4 is a side view of the push rod for horizontal zone-melting graphite boat in accordance with the present invention
In the figure, 1 is a push rod handle, 2 is a horizontal bubble, 3 is a push rod, 4 is a fork head, 5 is a hook, 6 is a zone-melting graphite boat, 7 is a group of high-frequency coils, 8 is a half-open graphite boat, and 9 is the moving direction of a melting zone.
Detailed Description
In order to better understand the present invention, the following examples are further provided to illustrate the present invention, but the present invention is not limited to the following examples.
The terms "center," "longitudinal," "lateral," "length," "width," "thickness," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," "clockwise," "counterclockwise," and the like are used herein as terms of orientation or positional relationship with respect to one another as shown in the drawings or in use, and are used for convenience in describing the present application and do not indicate or imply that the referenced device or element must have a particular orientation, be constructed and operated in a particular orientation, and therefore should not be considered as limiting the present application.
Example 1
As shown in fig. 3, a special push rod for a horizontal zone-melting graphite boat comprises a push rod handle 1, a push rod 3, a fork 4 and a hook 5; one end of the push rod 3 is connected with a push rod handle 1, the other end of the push rod is connected with a fork head 4, a horizontal bubble 2 is arranged on the side wall of the end, connected with the push rod 3, of the push rod handle 1, the push rod handle 1 and the push rod 3 are both straight rod-shaped and arranged coaxially, and the axis of the push rod 3 is collinear with the central line of the fork head 4; the hook 5 is in a 1-shaped structure, the hook 5 is vertically connected to the end part of the push rod 3 connected with the fork head 4, and the plane where the hook 5 and the fork head 4 are located is vertical to each other.
The use method of the special push rod for the horizontal zone-melting graphite boat comprises the following steps: firstly placing a half-open type graphite boat into a quartz tube, then placing the material-containing graphite boat into the quartz tube, then using a fork head of a special push rod to fork the graphite boat, quickly pushing the material-containing graphite boat to a specified position in the quartz tube, then slightly swinging a push rod handle left and right to enable bubbles in the horizontal bubble to be located at a central position, namely indicating that the material-containing graphite boat is located at a horizontal position, and finally placing the other half-open type graphite boat into the quartz tube and contacting the material-containing graphite boat, thus completing furnace charging operation. When the graphite boat is taken out from the quartz tube, the hook of the push rod hooks the inner wall of the head of the graphite boat and is pulled outwards slightly. FIG. 1 is a top view of a graphite boat with an open top for easy hooking.
Example 2
On the basis of the embodiment 1, the following improvements are further made: in order to improve the stability of use, the fork head 4 is of a U-shaped structure. The horizontal bubble 2 is arranged on the side wall of the corresponding push rod handle 1 when the fork head 4 is horizontal, namely as shown in figure 3 (the use state is overlooked), when in use, the fork head 4 horizontally forks the graphite boat, and the horizontal bubble 2 is arranged above the graphite boat, so that the observation and the correction are convenient, and the horizontal calibration is convenient; horizontal bubble and hook are located the both sides of push rod respectively, and during the use, as shown in fig. 3, horizontal bubble is last all the time, can not influence the use of horizontal bubble because of the setting of hook.
Example 3
On the basis of the embodiment 2, the following improvements are further made: the fork head 4 is made of stainless steel or plastic. This ensures the structural strength and the stability of the device in use, and also ensures the low-cost property of manufacture. In order to facilitate the use and simultaneously consider the use stability of the propulsion, the width of the inner side of the fork head 4 is 1 mm-2 mm larger than that of the zone-melting graphite boat 6.
Example 4
On the basis of the embodiment 3, the following improvements are further made: the length of the push rod 3 is twice of the length of the zone-melting graphite boat 6. The push rod 3 is made of stainless steel or plastic. This ensures the structural strength and the stability of the device in use, and also ensures the low-cost property of manufacture.
Example 5
On the basis of the embodiment 4, the following improvements are further made: the length of the push rod handle 1 is 1/4-1/6 of the length of the push rod 3, so that the use is convenient and the use stability is ensured. In order to avoid the hand slip and improve the estimation stability, four parallel grooves are arranged on the push rod handle 1, and the length direction of each groove is perpendicular to the axial direction of the push rod handle 1.
The special push rod for the horizontal zone-melting graphite boat in each example is convenient to operate, reduces the difficulty of the operation technology, can quickly complete the charging operation, saves time and improves the production efficiency; on the other hand, the material-containing graphite boats in the quartz tubes are ensured to be in a horizontal state, the thicknesses of the spindles discharged from the furnace are kept consistent, the probability of defective products is reduced, and the product quality is guaranteed.

Claims (9)

1. The utility model provides a special push rod of horizontal zone-melting graphite boat which characterized in that: comprises a push rod handle (1), a push rod (3), a fork head (4) and a hook (5); one end of the push rod (3) is connected with a push rod handle (1), the other end of the push rod is connected with the fork head (4), a horizontal bubble (2) is arranged on the side wall of the push rod handle (1) at the end connected with the push rod (3), the push rod handle (1) and the push rod (3) are both straight rod-shaped and arranged coaxially, and the axis of the push rod (3) is collinear with the central line of the fork head (4); the hook (5) is in a 1-shaped structure, the hook (5) is vertically connected to the end part of one end, connected with the fork head (4), of the push rod (3), and the planes of the hook (5) and the fork head (4) are perpendicular to each other.
2. The special push rod for the horizontal zone-melting graphite boat as claimed in claim 1, wherein: the fork head (4) is of a U-shaped structure.
3. The special push rod for the horizontal zone-melting graphite boat as claimed in claim 2, wherein: the horizontal bubble (2) is arranged on the side wall of the push rod handle (1) corresponding to the fork head (4) when the fork head is horizontal, and the horizontal bubble (2) and the hook (5) are respectively positioned on two sides of the push rod (3).
4. The special push rod for the horizontal zone-melting graphite boat as claimed in any one of claims 1 to 3, wherein: the fork head (4) is made of stainless steel or plastic.
5. The special push rod for the horizontal zone-melting graphite boat as claimed in any one of claims 1 to 3, wherein: the width of the inner side of the fork head (4) is 1 mm-2 mm larger than that of the zone-melting graphite boat (6).
6. The special push rod for the horizontal zone-melting graphite boat as claimed in any one of claims 1 to 3, wherein: the length of the push rod (3) is twice of that of the zone-melting graphite boat (6).
7. The special push rod for the horizontal zone-melting graphite boat as claimed in any one of claims 1 to 3, wherein: the push rod (3) is made of stainless steel or plastic.
8. The special push rod for the horizontal zone-melting graphite boat as claimed in any one of claims 1 to 3, wherein: the length of the push rod handle (1) is 1/4-1/6 of the length of the push rod (3).
9. The special push rod for the horizontal zone-melting graphite boat as claimed in any one of claims 1 to 3, wherein: four parallel grooves are arranged on the push rod handle (1), and the length direction of the grooves is perpendicular to the axial direction of the push rod handle (1).
CN202122933815.3U 2021-11-26 2021-11-26 Special push rod for horizontal zone-melting graphite boat Active CN216274456U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202122933815.3U CN216274456U (en) 2021-11-26 2021-11-26 Special push rod for horizontal zone-melting graphite boat

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Application Number Priority Date Filing Date Title
CN202122933815.3U CN216274456U (en) 2021-11-26 2021-11-26 Special push rod for horizontal zone-melting graphite boat

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CN216274456U true CN216274456U (en) 2022-04-12

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115627371A (en) * 2022-10-24 2023-01-20 云南东昌金属加工有限公司 Cyclone type purification system for reduction and purification of germanium dioxide

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115627371A (en) * 2022-10-24 2023-01-20 云南东昌金属加工有限公司 Cyclone type purification system for reduction and purification of germanium dioxide

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