CN216224324U - Experimental device for be used for synthetic of fibre base magnetic response material - Google Patents
Experimental device for be used for synthetic of fibre base magnetic response material Download PDFInfo
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- CN216224324U CN216224324U CN202120599636.8U CN202120599636U CN216224324U CN 216224324 U CN216224324 U CN 216224324U CN 202120599636 U CN202120599636 U CN 202120599636U CN 216224324 U CN216224324 U CN 216224324U
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- motor
- oil bath
- bin
- reaction
- bath groove
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- 239000000463 material Substances 0.000 title claims abstract description 19
- 239000000835 fiber Substances 0.000 title claims abstract description 15
- 230000004044 response Effects 0.000 title claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 51
- 239000004020 conductor Substances 0.000 claims abstract description 21
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 11
- 230000002194 synthesizing effect Effects 0.000 claims abstract description 6
- 230000015572 biosynthetic process Effects 0.000 claims description 8
- 239000003814 drug Substances 0.000 claims description 4
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 229920002545 silicone oil Polymers 0.000 claims description 2
- 238000002474 experimental method Methods 0.000 abstract description 4
- 230000000149 penetrating effect Effects 0.000 abstract description 2
- 239000003921 oil Substances 0.000 description 25
- 238000003756 stirring Methods 0.000 description 6
- 239000011261 inert gas Substances 0.000 description 5
- 239000000696 magnetic material Substances 0.000 description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000010703 silicon Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000007810 chemical reaction solvent Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000001360 synchronised effect Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- Treatment Of Fiber Materials (AREA)
Abstract
The utility model discloses an experimental device for synthesizing a fiber-based magnetic response material, which comprises a control panel, a motor, an oil bath groove, a reaction chamber and a dosing chamber, wherein the control panel is arranged below the motor, the motor is arranged below the oil bath groove, the bottom of the oil bath groove is provided with a motor spiral, the oil bath groove is connected with the motor through the motor spiral, the reaction chamber is arranged in the oil bath groove and is connected with the motor spiral at the bottom of the oil bath groove through an extension sleeve penetrating through the reaction chamber, the inner pipe of the sleeve is provided with a columnar conductor, the dosing chamber is arranged at the top of the reaction chamber, and the top of the reaction chamber is also provided with an inlet and a pressure valve. The device has simple structure and simple and convenient operation, and can be widely applied to the synthesis reaction experiment of the magnetic response material.
Description
Technical Field
The utility model relates to the technical field of synthetic experimental equipment, and particularly belongs to an experimental device for synthesizing a fiber-based magnetic response material.
Background
The magnetic stirrer is a liquid mixing device commonly used in laboratories, is mainly used for stirring or simultaneously heating and stirring liquid or solid-liquid mixture with low viscosity, utilizes the principle that like poles repel and opposite poles attract of a magnetic field, and pushes a magnetic stirrer placed in a container to perform circumferential operation by continuously changing the polarities at two ends of a base, and the rotation of the magnetic stirrer drives a sample to rotate, so that the purpose of stirring the sample to accelerate the reaction process is achieved; the magnetic stirrer needs to drive the sample by the magnetic stirrer, when a synthesis experiment with a larger sample volume is carried out, the bottom sample is often fully stirred, the stirring of the upper sample is small, the effective collision times of particles in the reaction vessel are few, and the synthesis reaction efficiency is low. Therefore, in order to achieve more sufficient stirring, it is usually necessary to add a mechanical stirring paddle to assist the stirring of the sample. Therefore, the whole experimental device is complex to assemble, and integrated synchronous control is difficult to realize.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide an experimental device for synthesizing a fiber-based magnetic response material, which provides a solution for overcoming the technical defects of the existing experimental equipment, realizes the integrated synchronous control of the experimental device for synthesizing the magnetic material, improves the effective collision occurrence frequency of the synthetic reaction and further improves the reaction rate.
In order to achieve the purpose, the utility model adopts the following technical scheme:
the experimental device for synthesizing the fiber-based magnetic response material comprises a control panel, a motor, an oil bath groove, a reaction bin and a chemical adding bin, wherein the control panel is arranged below the motor, the motor is arranged below the oil bath groove, a motor spiral is arranged at the bottom of the oil bath groove, the oil bath groove is connected with the motor through the motor spiral, the reaction bin is arranged in the oil bath groove, an extension sleeve penetrating through the reaction bin is connected with the motor spiral at the bottom of the oil bath groove, a columnar conductor is arranged on an inner pipe of the sleeve, the chemical adding bin is arranged at the top of the reaction bin, and an inlet and a pressure valve are further arranged at the top of the reaction bin.
Furthermore, the reaction bin is divided into a bin cover and a bin body which are mutually meshed and sealed through threads, and the inlet and the pressure valve are arranged on the bin cover.
Furthermore, the reaction bin is made of nonmagnetic stainless steel materials, and the upper bottom surface and the lower bottom surface of the reaction bin are both in an arc shape protruding outwards.
Furthermore, the columnar conductor is arranged in the sleeve, the length of the columnar conductor is larger than that of the reaction bin, and two poles of a magnetic field generated when the columnar conductor is electrified are arranged outside the reaction bin.
Furthermore, the oil bath groove is filled with silicone oil.
Furthermore, the surface of control panel is equipped with digital display screen and control button, adjusts the electric current size in the cylindrical conductor and the rotational speed of motor through the control panel.
In summary, due to the adoption of the technical scheme, the utility model has the following technical effects:
the utility model comprises a control panel, a motor, an oil bath groove, a reaction chamber and a dosing chamber, wherein the reaction chamber is arranged in the oil bath groove and is connected with the motor through a sleeve outer pipe, a columnar conductor is arranged in the sleeve inner pipe, and an inert gas inlet and outlet and a pressure valve are arranged at the upper part of the columnar conductor. The device can generate a magnetic field in the reaction bin by adjusting the current of the inner pipe columnar conductor to enable the magnetic material to move along the direction of the magnetic field, and simultaneously, the reaction bin rotates in the opposite direction through the motor from the outside to enable the magnetic material in the reaction bin and the load material to move in opposite directions, so that the efficiency of synthetic reaction and the purity of products are improved.
Drawings
FIG. 1 is a schematic view of the structure of the apparatus of the present invention.
Fig. 2 is a schematic structural diagram of the epitaxial growth sleeve of the present invention.
In the drawing, a control panel 1, a motor 2, a motor screw 21, an oil bath 3, a reaction chamber 4, a medicine adding chamber 5, a sleeve 6, an outer tube 61, an inner tube 62, an inlet 7, a pressure valve 8 and a conductor 9.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail below with reference to the accompanying drawings by way of examples of preferred embodiments. It should be noted, however, that the numerous details set forth in the description are merely for the purpose of providing the reader with a thorough understanding of one or more aspects of the present invention, which may be practiced without these specific details.
Example 1
As shown in fig. 1 and 2, an experimental apparatus for synthesis of a fiber-based magnetic response material includes: control panel 1, motor 2, oil bath 3, reaction bin 4, add medicine storehouse 5, reaction bin 4 arranges in oil bath 3, is connected through the motor spiral 21 of the extension sleeve pipe 6 that runs through reaction bin 4 and 3 bottoms in oil bath, and sleeve pipe outer tube 61 is connected with motor 2, and a cylindrical conductor 9 is placed to sleeve pipe inner tube 62, and its upper portion is equipped with inert gas access & exit 7 and pressure valve 8. The control panel sets up in the motor below, the motor sets up in the below of oil bath groove, the bottom in oil bath groove is equipped with the motor spiral, and this oil bath groove passes through the motor spiral and is connected with the motor, the oil bath inslot is arranged in to the reaction bin, through setting up the motor spiral connection of the epitaxial sleeve pipe that runs through the reaction bin and oil bath groove bottom.
The columnar conductor 9 is arranged in the sleeve inner pipe 62, the length of the columnar conductor is larger than that of the reaction bin 4, and two poles of a magnetic field generated during electrification are arranged outside the reaction bin 4;
the reaction bin 4 is divided into a bin cover and a bin body, and the bin cover and the bin body are mutually meshed and sealed through threads;
the control panel 1 controls the synthesis reaction rate by adjusting the current in the columnar conductor 9 and the rotating speed of the motor 2;
the heating medium in the oil bath 3 is silicon oil which is not conductive and has good heat transfer performance;
the reaction chamber 4 is made of non-magnetic stainless steel material, and can isolate external magnetic field.
When the utility model is operated, the reaction chamber 4 of the device is firstly connected and tightly clamped with the motor screw 21 at the center of the bottom of the oil bath 3, the columnar conductor 9 is placed in the cavity of the sleeve inner pipe 62, the chamber cover is covered and screwed tightly for sealing, the firing pin in the chamber cover is contacted with the columnar conductor 9, and finally the hollow round cover of the oil bath 3 is covered to prevent the hot silicon oil from splashing.
After the device part is sequentially installed, a reaction solvent, a fiber-based material and a nano magnetic material are added into a reaction bin 4 through a chemical adding bin 5, inert gas is conveyed into the reaction bin through an inert gas inlet and outlet 7, then silicon oil is added into an oil bath groove 3, finally, a power switch of a control board 1 is turned on, the output current and the rotating speed of a motor 2 are adjusted, the heating temperature is set, and a synthesis experiment is started.
After the experiment is finished, the reaction bin 4 and the motor screw 21 are separated and then integrally taken out, the reaction bin is cooled to room temperature, the inert gas inlet and outlet 7 is adjusted according to the indication of the pressure valve 8 to slowly deflate and reduce the pressure until the air pressure in the bin body is equal to the outside, the bin cover of the reaction bin 4 is unscrewed, the sample is poured out and collected, and the reaction solvent is washed away by deionized water, so that the magnetic fiber-based magnetic response sample is obtained. .
The foregoing is only a preferred embodiment of the present invention, and it should be noted that those skilled in the art can make various improvements and modifications without departing from the principle of the present invention, and these improvements and modifications should also be construed as the protection scope of the present invention.
Claims (6)
1. An experimental device for synthesizing a fiber-based magnetic response material is characterized in that: including control panel, motor, oil bath groove, reaction chamber, add the medicine storehouse, the control panel sets up in the motor below, the motor sets up the below in the oil bath groove, the bottom in oil bath groove is equipped with the motor spiral, and this oil bath groove passes through the motor spiral and is connected with the motor, the oil bath inslot is arranged in to the reaction chamber, through setting up the motor spiral connection of the extension sleeve pipe that runs through the reaction chamber and oil bath groove bottom, sheathed tube inner tube sets up a column conductor, add the medicine storehouse setting at the top in the reaction chamber, the top in this reaction chamber still is provided with entry and pressure valve.
2. The experimental device for the synthesis of the fiber-based magnetic response material according to claim 1, wherein: the reaction bin is divided into a bin cover and a bin body, the bin cover and the bin body are mutually meshed and sealed through threads, and the inlet and the pressure valve are arranged on the bin cover.
3. An experimental device for the synthesis of fiber-based magnetic response materials according to claim 2, characterized in that: the reaction bin is made of nonmagnetic stainless steel materials, and the upper bottom surface and the lower bottom surface of the reaction bin are both in an arc shape protruding outwards.
4. The experimental device for the synthesis of the fiber-based magnetic response material according to claim 1, wherein: the columnar conductor is arranged in the sleeve, the length of the columnar conductor is larger than that of the reaction bin, and two poles of a magnetic field generated when the columnar conductor is electrified are arranged outside the reaction bin.
5. The experimental device for the synthesis of the fiber-based magnetic response material according to claim 1, wherein: and silicone oil is filled in the oil bath groove.
6. The experimental device for the synthesis of the fiber-based magnetic response material according to claim 1, wherein: the surface of control panel is equipped with digital display screen and control button, adjusts the electric current size and the rotational speed of motor in the columnar conductor through the control panel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120599636.8U CN216224324U (en) | 2021-03-24 | 2021-03-24 | Experimental device for be used for synthetic of fibre base magnetic response material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120599636.8U CN216224324U (en) | 2021-03-24 | 2021-03-24 | Experimental device for be used for synthetic of fibre base magnetic response material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN216224324U true CN216224324U (en) | 2022-04-08 |
Family
ID=80938171
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202120599636.8U Active CN216224324U (en) | 2021-03-24 | 2021-03-24 | Experimental device for be used for synthetic of fibre base magnetic response material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN216224324U (en) |
-
2021
- 2021-03-24 CN CN202120599636.8U patent/CN216224324U/en active Active
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Address after: 242300 intersection of Dongcheng Avenue and Dongcheng Road, heli Park, Ningguo Economic and Technological Development Zone, Ningguo City, Xuancheng City, Anhui Province Patentee after: Anhui Boshike Environmental Protection Technology Co.,Ltd. Country or region after: China Address before: No. 12, Kexing Road, high tech Zone, Nanning, Guangxi 530000 Patentee before: GUANGXI BOSSCO ENVIRONMENTAL PROTECTION TECHNOLOGY Co.,Ltd. Country or region before: China |
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| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240428 Address after: 242300 intersection of Dongcheng Avenue and Dongcheng Road, heli Park, Ningguo Economic and Technological Development Zone, Ningguo City, Xuancheng City, Anhui Province Patentee after: Anhui Boshike Environmental Protection Technology Co.,Ltd. Country or region after: China Patentee after: Guangxi Boshike Environmental Technology Co.,Ltd. Address before: 242300 intersection of Dongcheng Avenue and Dongcheng Road, heli Park, Ningguo Economic and Technological Development Zone, Ningguo City, Xuancheng City, Anhui Province Patentee before: Anhui Boshike Environmental Protection Technology Co.,Ltd. Country or region before: China |