CN215916519U - Organic synthesis extraction all-in-one - Google Patents

Organic synthesis extraction all-in-one Download PDF

Info

Publication number
CN215916519U
CN215916519U CN202122413070.8U CN202122413070U CN215916519U CN 215916519 U CN215916519 U CN 215916519U CN 202122413070 U CN202122413070 U CN 202122413070U CN 215916519 U CN215916519 U CN 215916519U
Authority
CN
China
Prior art keywords
synthesis
extraction
base
corners
workbench
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202122413070.8U
Other languages
Chinese (zh)
Inventor
牛学丽
张丽娜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jincheng Institute Of Technology
Original Assignee
Jincheng Institute Of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jincheng Institute Of Technology filed Critical Jincheng Institute Of Technology
Priority to CN202122413070.8U priority Critical patent/CN215916519U/en
Application granted granted Critical
Publication of CN215916519U publication Critical patent/CN215916519U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices For Use In Laboratory Experiments (AREA)

Abstract

The utility model discloses an organic synthesis and extraction integrated machine, which comprises a workbench, wherein a conical groove is arranged at the top of the workbench, a synthesis cylinder is arranged on the conical groove, rubber fixing parts of the synthesis cylinder are respectively arranged at two sides of the synthesis cylinder, spring storage cylinders are respectively arranged at four corners of the top of the workbench, a torsion spring is arranged inside the spring storage cylinder, the top of the torsion spring is connected with a connecting rod, the top of the connecting rod is provided with a top plate, a bearing is arranged in the middle of the top plate, and a stirring rod is arranged inside the bearing. The test personnel of being convenient for operate, simple structure, convenient to popularize and use.

Description

Organic synthesis extraction all-in-one
Technical Field
The utility model relates to the field of chemistry, in particular to an organic synthesis and extraction integrated machine.
Background
Organic synthesis refers to a process of chemically preparing simple substances, simple inorganic substances or simple organic substances into more complex organic substances. For example, methanol from hydrogen and carbon dioxide, vinyl chloride from acetylene, and polymerization to give polyvinyl chloride resin, adipic acid and hexamethylenediamine from phenol through a series of reactions, and condensation of the two to form polyamide fibers. At present, most organic substances such as resin, rubber , fiber, dye, medicine, fuel, perfume, etc. can be prepared by organic synthesis. Some require extraction after synthesis, which is also called solvent extraction or liquid-liquid extraction, also called extraction, is a unit operation that separates mixtures by utilizing the different solubilities of components in the system in a solvent. That is, a method of transferring a solute substance from one solvent to another solvent by utilizing the difference in solubility or partition coefficient of the substance in two solvents which are not soluble in each other, and extraction is one of the means used in organic chemistry laboratories for purifying and purifying compounds. The desired substance can be extracted from the solid or liquid mixture by extraction. However, the existing synthesis equipment can only carry out synthesis tests, cannot carry out extraction tests, needs separate operations of synthesis and extraction, is very inconvenient, has low synthesis efficiency, is fixed and cannot be adjusted in the height of a workbench, is inconvenient for collecting liquid by measuring cylinders with different heights, needs other lighting facilities for lighting, and is inconvenient for operation of testers; therefore, the organic synthesis and extraction integrated machine is provided.
Disclosure of Invention
The utility model aims to provide an organic synthesis and extraction integrated machine aiming at the defects of the prior art so as to solve the problems in the background technology.
In order to achieve the purpose, the utility model provides the following technical scheme: an organic synthesis extraction all-in-one machine comprises a workbench, wherein a conical groove is formed in the top of the workbench, a synthesis cylinder is arranged on the conical groove, synthesis cylinder rubber fixing parts are arranged on two sides of the synthesis cylinder, spring storage cylinders are arranged at four corners of the top of the workbench, a torsion spring is arranged inside the spring storage cylinders, a connecting rod is connected to the top of the torsion spring, a top plate is arranged at the top of the connecting rod, a bearing is arranged in the middle of the top plate, a stirring rod is arranged inside the bearing, a crank is connected to the top of the stirring rod, a sealing plate is arranged at the bottom of the top plate, illuminating lamp panels are arranged on two sides of the sealing plate, a liquid outlet pipe is connected to the bottom of the synthesis cylinder, a hand valve is arranged on the liquid outlet pipe, a separating funnel is arranged at the bottom of the liquid outlet pipe, and is arranged on a separating funnel fixing frame, the bottom of separating funnel is equipped with the graduated flask, electric telescopic handle is all installed to four corners of workstation bottom, electric telescopic handle installs four corners at the base top, the side-mounting of base has switch, the rubber pad is all installed to four corners of base bottom, be connected with the power cord on the base.
As a preferred technical solution of the present invention, the electric telescopic rod is installed at four corners of the top of the base through bolts, the work table is installed at the top of the electric telescopic rod through bolts, and the spring storage cylinders are installed at four corners of the top of the work table through bolts.
As a preferred technical scheme of the present invention, the torsion spring is fixed in the spring storage cylinder through a connection block, the connection rod is fixedly connected to a top end of the torsion spring through the connection block, and the top plate is mounted on a top portion of the connection rod through a bolt.
As a preferable technical scheme of the utility model, the sealing plate and the illuminating lamp plate are both arranged on the bottom of the top plate through bolts, the bearing is arranged on the middle part of the top plate through bolts, the stirring rod is fixed in the bearing, and the crank is connected with the top of the stirring rod in a welding manner.
As a preferable technical scheme of the utility model, the synthetic cylinder rubber fixing piece is installed on the top of the workbench through a bolt, the separating funnel fixing frame is installed on the bottom of the workbench through a bolt, and the rubber pad is installed on the bottom of the base through a bolt.
As a preferred technical scheme of the utility model, the power switch is mounted on the side surface of the base through a bolt, and the power switch is respectively electrically connected with the lighting lamp panel and the electric telescopic rod.
The utility model has the beneficial effects that: this equipment not only can carry out the synthetic experiment of organic matter, also can extract the experiment, combines synthetic and extraction together, and people need not separately operate, and easy operation is convenient, can stir simultaneously and improve synthetic efficiency, and the height degree that can the automatically regulated workstation in addition, the measuring cylinder of the co-altitude not of being convenient for collects liquid, can provide the illumination, and the experimenter of being convenient for operates simple structure, convenient to popularize and use.
Drawings
FIG. 1 is a schematic structural view of the present invention;
fig. 2 is a top view of the inventive table.
In the figure: the device comprises a workbench 1, a spring storage barrel 2, a connecting rod 3, a top plate 4, a bearing 5, a sealing plate 6, a crank 7, a stirring rod 8, a lighting lamp plate 9, a synthesis barrel 10, a synthesis barrel rubber fixing part 11, a torsion spring 12, a conical groove 13, a liquid outlet pipe 14, a hand valve 15, a separating funnel 16, a separating funnel fixing frame 17, a measuring cylinder 18, an electric telescopic rod 19, a base 20, a power switch 21, a power line 22 and a rubber pad 23.
Detailed Description
The following detailed description of the preferred embodiments of the present invention, taken in conjunction with the accompanying drawings, will make the advantages and features of the utility model more readily understood by those skilled in the art, and thus will more clearly and distinctly define the scope of the utility model.
Example (b): referring to fig. 1-2, the present invention provides a technical solution: an organic synthesis extraction all-in-one machine comprises a workbench 1, wherein a conical groove 13 is arranged at the top of the workbench 1, a synthesis cylinder 10 is arranged on the conical groove 13, synthesis cylinder rubber fixing parts 11 are respectively arranged at two sides of the synthesis cylinder 10, spring storage cylinders 2 are respectively arranged at four corners of the top of the workbench 1, a torsion spring 12 is arranged inside the spring storage cylinders 2, a connecting rod 3 is connected to the top of the torsion spring 12, a top plate 4 is arranged at the top of the connecting rod 3, a bearing 5 is arranged in the middle of the top plate 4, a stirring rod 8 is arranged inside the bearing 5, a crank 7 is connected to the top of the stirring rod 8, a sealing plate 6 is arranged at the bottom of the top plate 4, illumination lamp plates 9 are respectively arranged at two sides of the sealing plate 6, a liquid outlet pipe 14 is connected to the bottom of the synthesis cylinder 10, a hand valve 15 is arranged on the liquid outlet pipe 14, a separating funnel 16 is arranged at the bottom of the liquid outlet pipe 14, the liquid separating funnel 16 is arranged on a liquid separating funnel fixing frame 17, separating funnel 16's bottom is equipped with graduated flask 18, and electric telescopic handle 19 is all installed to four corners of workstation 1 bottom, and electric telescopic handle 19 installs four corners at base 20 top, and base 20's side-mounting has switch 21, and rubber pad 23 is all installed to four corners of base 20 bottom, is connected with power cord 22 on the base 20.
Electric telescopic handle 19 passes through the bolt and installs four corners at base 20 top, and workstation 1 passes through the bolt and installs on electric telescopic handle 19's top, and spring storage cylinder 2 passes through the bolt and installs four corners at workstation 1 top, can drive workstation 1 through electric telescopic handle 19 circular telegram work and reciprocate.
Torsion spring 12 passes through the connecting block to be fixed in spring storage cylinder 2, and connecting rod 3 passes through the connecting block and is fixed continuous with torsion spring 12's top, and roof 4 passes through the bolt and installs on connecting rod 3's top, presses roof 4 and can make roof 4 move down through torsion spring 12 atress.
Seal plate 6 and illumination lamp plate 9 are all installed on the bottom of roof 4 through the bolt, and bearing 5 passes through the bolt and installs on the middle part at roof 4 top, and puddler 8 is fixed in bearing 5, and 7 welding of crank are on the top of puddler 8, can drive puddler 8 through rotatory crank 7 and rotate around bearing 5, stir the synthesis to the liquid in the synthesis section of thick bamboo 10.
The synthetic cylinder rubber fixing piece 11 is installed on the top of the workbench 1 through bolts, the separating funnel fixing frame 17 is installed on the bottom of the workbench 1 through bolts, the rubber pad 23 is installed on the bottom of the base 20 through bolts, and the stability of the synthetic cylinder 10 can be improved through the installation of the synthetic cylinder rubber fixing piece 11.
Switch 21 passes through the bolt and installs on base 20's side, and switch 21 respectively with 19 electric connection of illumination lamp plate 9 and electric telescopic handle, can put through the power of illumination lamp plate 9 and electric telescopic handle 19 through switch 21, make illumination lamp plate 9 and 19 circular telegram work of electric telescopic handle.
The working principle is as follows: an organic synthesis extraction all-in-one machine comprises a workbench 1, when in use, a plurality of liquids to be synthesized are poured into a synthesis cylinder 10 for synthesis, both sides of the synthesis cylinder 10 are provided with synthesis cylinder rubber fixing parts 11 which can improve the stability of the synthesis cylinder 10, a top plate 4 is pressed to extrude a torsion spring 12 through a connecting rod 3, the torsion spring 12 is stressed to move downwards to drive the top plate 4 to move downwards, a sealing plate 6 is covered on the top of the synthesis cylinder 10, a rotary crank 7 can drive a stirring rod 8 to rotate around a bearing 5, the liquid in the synthesis cylinder 10 is stirred, the synthesis efficiency is improved, after synthesis is completed, the extrusion on the top plate 4 is released, the torsion spring 12 drives the top plate 4 to return, a hand valve 15 on a liquid outlet pipe 14 is opened, the liquid in the synthesis cylinder 10 enters a liquid separating funnel 16 through the liquid outlet pipe 14 for liquid separation, after liquid separation is completed, the liquid at the bottom layer of the liquid separating funnel 16 is conveyed into a measuring cylinder 18 for storage, can put through the power of illumination lamp plate 9 and electric telescopic handle 19 through switch 21, 19 work of circular telescopic handle circular telegram can drive workstation 1 and reciprocate, and the graduated flask 18 of the co-altitude of being convenient for collects liquid, can provide the illumination through 9 work of circular telegram of illumination lamp plate, makes things convenient for the experimenter to operate.
This equipment not only can carry out the synthetic experiment of organic matter, also can extract the experiment, combines synthetic and extraction together, and people need not separately operate, and easy operation is convenient, can stir simultaneously and improve synthetic efficiency, and the height degree that can the automatically regulated workstation in addition, the measuring cylinder of the co-altitude not of being convenient for collects liquid, can provide the illumination, and the experimenter of being convenient for operates simple structure, convenient to popularize and use.
The above examples only show some embodiments of the present invention, and the description thereof is more specific and detailed, but not to be construed as limiting the scope of the utility model. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention.

Claims (6)

1. The utility model provides an organic synthesis extraction all-in-one, includes workstation (1), its characterized in that: the top of the workbench (1) is provided with a conical groove (13), a synthesis barrel (10) is arranged on the conical groove (13), synthesis barrel rubber fixing parts (11) are installed on two sides of the synthesis barrel (10), spring storage barrels (2) are installed on four corners of the top of the workbench (1), torsion springs (12) are arranged inside the spring storage barrels (2), the top of each torsion spring (12) is connected with a connecting rod (3), a top plate (4) is installed at the top of each connecting rod (3), a bearing (5) is installed in the middle of the top of each top plate (4), a stirring rod (8) is installed inside each bearing (5), the top of each stirring rod (8) is connected with a crank (7), a sealing plate (6) is installed at the bottom of each top plate (4), and illumination lamp panels (9) are installed on two sides of each sealing plate (6), the bottom of synthesizing a section of thick bamboo (10) is connected with drain pipe (14), install hand valve (15) on drain pipe (14), separating funnel (16) are installed to the bottom of drain pipe (14), separating funnel (16) are installed on separating funnel mount (17), the bottom of separating funnel (16) is equipped with graduated flask (18), electric telescopic handle (19) are all installed to four corners of workstation (1) bottom, four corners at base (20) top are installed in electric telescopic handle (19), the side-mounting of base (20) has switch (21), rubber pad (23) are all installed to four corners of base (20) bottom, be connected with power cord (22) on base (20).
2. The organic synthesis and extraction all-in-one machine as claimed in claim 1, wherein: electric telescopic handle (19) pass through the bolt and install four corners at base (20) top, workstation (1) passes through the bolt and installs on electric telescopic handle (19)'s top, spring storage cylinder (2) pass through the bolt and install four corners at workstation (1) top.
3. The organic synthesis and extraction all-in-one machine as claimed in claim 1, wherein: the torsion spring (12) is fixed in the spring storage barrel (2) through a connecting block, the connecting rod (3) is fixedly connected with the top end of the torsion spring (12) through the connecting block, and the top plate (4) is installed on the top of the connecting rod (3) through a bolt.
4. The organic synthesis and extraction all-in-one machine as claimed in claim 1, wherein: the sealing plate (6) and the lighting lamp plate (9) are both installed on the bottom of the top plate (4) through bolts, the bearing (5) is installed on the middle portion of the top plate (4) through bolts, the stirring rod (8) is fixed in the bearing (5), and the crank (7) is connected with the top of the stirring rod (8) in a welding mode.
5. The organic synthesis and extraction all-in-one machine as claimed in claim 1, wherein: the rubber fixing part (11) of the synthesis cylinder is installed on the top of the workbench (1) through bolts, the separating funnel fixing frame (17) is installed on the bottom of the workbench (1) through bolts, and the rubber pad (23) is installed on the bottom of the base (20) through bolts.
6. The organic synthesis and extraction all-in-one machine as claimed in claim 1, wherein: switch (21) pass through the bolt and install on the side of base (20), switch (21) respectively with illumination lamp plate (9) and electric telescopic handle (19) electric connection.
CN202122413070.8U 2021-10-08 2021-10-08 Organic synthesis extraction all-in-one Active CN215916519U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202122413070.8U CN215916519U (en) 2021-10-08 2021-10-08 Organic synthesis extraction all-in-one

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202122413070.8U CN215916519U (en) 2021-10-08 2021-10-08 Organic synthesis extraction all-in-one

Publications (1)

Publication Number Publication Date
CN215916519U true CN215916519U (en) 2022-03-01

Family

ID=80406669

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202122413070.8U Active CN215916519U (en) 2021-10-08 2021-10-08 Organic synthesis extraction all-in-one

Country Status (1)

Country Link
CN (1) CN215916519U (en)

Similar Documents

Publication Publication Date Title
CN215916519U (en) Organic synthesis extraction all-in-one
CN206663110U (en) A kind of coupler draft gear attaching/detaching apparatus
CN113041890A (en) Mixed medicament preparation device
CN218421069U (en) Novel hydrogen fluoride and hydrogen chloride separation device
CN109738243B (en) High-altitude sampler for collecting black carbon
CN110538484B (en) Organic matter liquid-liquid extraction composite set
CN214436578U (en) Tridecyl trimellitate synthesis mechanism
CN221332795U (en) A vacuum distillation unit for producing methyl benzoate
CN209039313U (en) A kind of cloth bag filter press
CN205412325U (en) Chromatography device
CN215415255U (en) Preparative separation equipment for rod-shaped thin-layer chromatography
CN217756821U (en) Purification radioactive sample collection device
CN220752032U (en) A detection device that is arranged in soil and quality of water biphenyl and diphenyl ether content
CN110917986A (en) Novel waterproof coating mixing apparatus who facilitates use
CN219455578U (en) Ecological resource sampler convenient to detect
CN220811961U (en) Petrochemical oil-liquid separator
CN215179291U (en) Test block compression test device based on commercial concrete
CN212789866U (en) N-propanol rectification purification equipment
CN218392771U (en) Ethylene separation equipment
CN208688958U (en) Filter scanning platform
CN212548477U (en) Triphenylphosphine reaction menstruum recycle device
CN219307994U (en) Solid phase extraction frame
CN216970582U (en) Isobutyric acid collection device
CN220610064U (en) Separation device for purifying butyl acrylate
CN212301022U (en) Equipment for detecting atmospheric environmental pollution

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant