CN215691736U

CN215691736U - Cyclopentadiene manganese tricarbonyl refined distillation bed charge recovery unit with prevent stifled

Info

Publication number: CN215691736U
Application number: CN202121975602.0U
Authority: CN
Inventors: 贺茂松; 孟俭
Original assignee: Shandong Jiahe Methyl Chemical Co ltd
Current assignee: Shandong Jiahe Methyl Chemical Co ltd
Priority date: 2021-08-20
Filing date: 2021-08-20
Publication date: 2022-02-01
Anticipated expiration: 2031-08-20

Abstract

The utility model discloses an anti-blocking cyclopentadiene manganese tricarbonyl refined distillation bottom material recovery device, which relates to the field of chemistry and comprises a distillation still, a discharging pipe fixedly arranged in the middle of the lower end of the distillation still, a material pushing mechanism, a discharging mechanism and a discharging mechanism, wherein the material pushing mechanism is arranged below the inner part of the distillation still, the discharging mechanism is arranged in the discharging pipe, the lower end of the discharging pipe is fixedly connected with a horizontally arranged discharging pipe, and the discharging mechanism is arranged in the discharging pipe. The utility model is convenient for discharging the residual materials in the distillation kettle, avoids the blockage phenomenon when discharging the materials and is convenient for people to use.

Description

Cyclopentadiene manganese tricarbonyl refined distillation bed charge recovery unit with prevent stifled

Technical Field

The utility model belongs to the technical field of chemistry, and particularly relates to a cyclopentadiene manganese tricarbonyl refined distillation bottom material recovery device with anti-blocking function.

Background

Manganese tricarbonyl (. eta. -cyclopentadienyl) manganese, distinguished therein as cyclopentadienyl manganese tricarbonyl. CAS number 12079-65-1, molecular formula C8H5MnO3, molecular weight 204.0615.

At present, when the methylcyclopentadienyl manganese tricarbonyl is purified, raw materials need to be placed in a distillation still for distillation, and after the distillation, residues need to be discharged from the distillation still.

SUMMERY OF THE UTILITY MODEL

Aiming at the situation and overcoming the defects of the prior art, the utility model provides the anti-blocking cyclopentadiene manganese tricarbonyl fine distillation bottom material recovery device, which effectively solves the problems that when the residue is discharged at present, the residue is generally directly discharged through a discharge hole at the lower side of a distillation still, the residue is easy to block, so that the discharge of the residue is influenced, and the use of people is influenced.

In order to achieve the purpose, the utility model provides the following technical scheme: the utility model provides a cyclopentadiene manganese tricarbonyl essence evaporates bed charge recovery unit with prevent stifled, still fixes the unloading pipe that sets up at stills lower extreme middle part including stills, still includes pushing equipment, unloading mechanism and row's material mechanism, pushing equipment sets up the inside below at stills, unloading mechanism sets up in the unloading pipe, the lower extreme fixed connection of unloading pipe has the row's of level setting to expect the pipe, it sets up in arranging the material pipe to arrange material mechanism.

Preferably, the pushing mechanism comprises a servo motor, a rotating rod, a first rotating rod, a second rotating rod and two groups of material pushing plates, a support is fixedly arranged below the inner part of the distillation kettle, the middle part of the upper end of the support is rotationally connected with the first rotating rod through a first bearing, the rotating rod is transversely arranged below the support, the lower end of the first rotating rod penetrates through the support and is fixedly connected with the rotating rod, the two groups of material pushing plates are fixedly connected with the lower side of the rotating rod, the upper end of the first rotating rod is fixedly connected with a first bevel gear, the second rotating rod is transversely arranged on the right side above the support, the left end of the second rotating rod is fixedly connected with a second bevel gear, the first bevel gear is meshed with the second bevel gear, the right end of the second rotating rod penetrates through a right side wall of the distillation kettle through a second bearing and extends to the outer part of the distillation kettle, the servo motor is fixedly connected with the right outer side wall of the distillation kettle through a motor seat, and the output end of the servo motor is fixedly connected with the right end of the second rotating rod through a coupler.

Preferably, the two groups of the material pushing plates are arranged in an arc shape, and the running tracks of the two groups of the material pushing plates are sequentially and alternately arranged.

Preferably, the blanking mechanism comprises a first spiral conveying blade, the lower end of the first rotating rod extends downwards to the lower portion of the inner portion of the blanking pipe, and the first spiral conveying blade is arranged in the blanking pipe and fixedly sleeved with the first rotating rod.

Preferably, it includes third bull stick and second screw feed leaf to arrange the material mechanism, third bull stick and second screw feed leaf all set up in the inside of arranging the material pipe, second screw feed leaf is pegged graft with the third bull stick is fixed, the right-hand member of third bull stick passes the right side wall of arranging the material pipe and extends to the outside of arranging the material pipe through the third bearing, the belt pulley has all been fixed cup jointed on the pole wall right side of second bull stick and third bull stick, two the belt pulley passes through belt mutual drive.

Preferably, the lower end of the distillation still is fixedly connected with a plurality of uniformly distributed support legs, and the support legs are fixedly connected with four corners of the lower end of the distillation still respectively.

The utility model has the technical effects and advantages that:

1. through the mutual matching of the distillation still, the material pushing mechanism, the blanking pipe, the blanking mechanism, the discharging pipe and the discharging mechanism, when the residue in the distillation still needs to be discharged, a servo motor is started to drive a second rotating rod to rotate, the second rotating rod drives a first rotating rod to rotate through a second bevel gear and a first bevel gear, the first rotating rod drives the rotating rod and two groups of material pushing plates to rotate, so that the residue below the interior of the distillation still can be pushed, the residue enters a discharging pipe, meanwhile, the first rotating rod can also drive a first spiral conveying blade to rotate, the first spiral conveying blade can drive the material in the discharging pipe to move downwards and convey the material to the discharging pipe, when the second rotating rod rotates, a third rotating rod is also driven to rotate through two belt wheels and a belt, the third rotating rod can drive a second spiral conveying blade to rotate, so that the material in the discharging pipe can be driven to move, the material is convenient to discharge, the blocking phenomenon is avoided when the material is discharged, and the material discharging device is convenient for people to use.

Drawings

The accompanying drawings, which are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate embodiments of the utility model and together with the description serve to explain the principles of the utility model and not to limit the utility model. In the drawings:

FIG. 1 is a schematic front view of the present invention;

FIG. 2 is a schematic cross-sectional front view of the present invention;

fig. 3 is a schematic bottom view of two sets of material pushing plates according to the present invention.

In the figure: 1. a distillation kettle; 2. a discharging pipe; 3. a discharge pipe; 4. a servo motor; 5. rotating the rod; 6. a first rotating lever; 7. a second rotating rod; 8. a material pushing plate; 9. a support; 10. a first bevel gear; 11. a second bevel gear; 12. a motor base; 13. a first spiral conveying leaf; 14. a third rotating rod; 15. a second spiral conveying leaf; 16. a belt pulley; 17. a belt; 18. and (3) a support leg.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments; all other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The utility model provides an anti-blocking cyclopentadiene manganese tricarbonyl refined distillation bottom material recovery device, which is shown in figures 1-3 and comprises a distillation kettle 1, a blanking pipe 2, a material pushing mechanism, a blanking mechanism and a material discharging mechanism, wherein the blanking pipe 2 is fixedly arranged in the middle of the lower end of the distillation kettle 1, the material pushing mechanism is arranged below the inner part of the distillation kettle 1, the blanking mechanism is arranged in the blanking pipe 2, the lower end of the blanking pipe 2 is fixedly connected with a horizontally arranged material discharging pipe 3, and the material discharging mechanism is arranged in the material discharging pipe 3.

As shown in fig. 2, the material pushing mechanism comprises a servo motor 4, a rotating rod 5, a first rotating rod 6, a second rotating rod 7 and two groups of material pushing plates 8, a support 9 is fixedly arranged below the inner part of the distillation still 1, the middle part of the upper end of the support 9 is rotatably connected with the first rotating rod 6 through a first bearing, the rotating rod 5 is transversely arranged below the support 9, the lower end of the first rotating rod 6 penetrates through the support 9 and is fixedly connected with the rotating rod 5, the two groups of material pushing plates 8 are fixedly connected with the lower side of the rotating rod 5, the upper end of the first rotating rod 6 is fixedly connected with a first bevel gear 10, the second rotating rod 7 is transversely arranged at the right side above the support 9, the left end of the second rotating rod 7 is fixedly connected with a second bevel gear 11, the first bevel gear 10 is in meshed connection with the second bevel gear 11, the right end of the second rotating rod 7 penetrates through the right side wall of the distillation still 1 through a second bearing and extends to the outside of the distillation still 1, servo motor 4 passes through motor cabinet 12 and stills 1's right side lateral wall fixed connection, servo motor 4's output passes through the right-hand member fixed connection of shaft coupling and second bull stick 7, when needing to discharge the residue in stills 1, start servo motor 4 and can drive second bull stick 7 and rotate, the second bull stick drives first bull stick 6 through 7 second bevel gear 11 and first bevel gear 10 and rotates, first bull stick 6 drives dwang 5 and two sets of scraping wings 8 and rotates, thereby can promote the residue of stills 1 inside below, make the residue get into in unloading pipe 2.

As shown in fig. 3, the two sets of material pushing plates 8 are both arc-shaped, and the moving tracks of the two sets of material pushing plates 8 are sequentially and alternately arranged, so that the residual materials in the distillation still 1 can be concentrated to the middle, and then enter the discharging pipe 2.

As shown in fig. 2, the blanking mechanism includes a first spiral conveying blade 13, a lower end of the first rotating rod 6 extends downward to a lower portion inside the blanking tube 2, the first spiral conveying blade 13 is disposed in the blanking tube 2 and fixedly sleeved with the first rotating rod 6, the first rotating rod 6 can further drive the first spiral conveying blade 13 to rotate, and the first spiral conveying blade 13 rotates to drive the material in the blanking tube 2 to move downward and convey the material to the discharging tube 3.

As shown in fig. 2, the discharging mechanism includes a third rotating rod 14 and a second spiral conveying blade 15, the third rotating rod 14 and the second spiral conveying blade 15 are both disposed inside the discharging pipe 3, the second spiral conveying blade 15 is fixedly inserted into the third rotating rod 14, the right end of the third rotating rod 14 passes through the right side wall of the discharging pipe 3 through a third bearing and extends to the outside of the discharging pipe 3, belt pulleys 16 are fixedly sleeved on the right sides of the rod walls of the second rotating rod 7 and the third rotating rod 14, the two belt pulleys 16 are mutually transmitted through belts 17, when the second rotating rod 7 rotates, the third rotating rod 14 is also driven to rotate through the two belt pulleys 16 and the belt 17, the third rotating rod 14 rotates to drive the second spiral conveying blade 15 to rotate, so that the material inside the discharging pipe 3 can be driven to move, the material can be conveniently discharged, the blocking phenomenon can be avoided when the material is discharged, and the discharging mechanism can be conveniently used by people.

As shown in fig. 1 and fig. 2, a plurality of evenly distributed support legs 18 are fixedly connected to the lower end of the distillation still 1, and the plurality of support legs 18 are respectively fixedly connected to four corners of the lower end of the distillation still 1, so as to stably support the distillation still 1.

The working principle of the utility model is as follows: when the residues in the distillation still 1 need to be discharged, the servo motor 4 is started to drive the second rotating rod 7 to rotate, the second rotating rod drives the first rotating rod 6 to rotate through the second bevel gear 11 and the first bevel gear 10 7, the first rotating rod 6 drives the rotating rod 5 and the two groups of material pushing plates 8 to rotate, so that the residues below the interior of the distillation still 1 can be pushed, the residues enter the discharging pipe 2, the first rotating rod 6 can also drive the first spiral conveying blade 13 to rotate, the first spiral conveying blade 13 can drive the materials in the discharging pipe 2 to move downwards and convey the materials to the discharging pipe 3, when the second rotating rod 7 rotates, the third rotating rod 14 is also driven to rotate through the two belt pulleys 16 and the belt 17, the third rotating rod 14 can drive the second spiral conveying blade 15 to rotate, so that the materials in the discharging pipe 3 can be driven to move, and the materials can be discharged conveniently, the blockage phenomenon is avoided when the materials are discharged, and the use by people is convenient.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a cyclopentadiene manganese tricarbonyl essence evaporates bed charge recovery unit with prevent stifled, still fixes blanking pipe (2) of setting at stills (1) lower extreme middle part including stills (1), its characterized in that: still include pushing equipment, unloading mechanism and arrange material mechanism, pushing equipment sets up the inside below at stills (1), unloading mechanism sets up in unloading pipe (2), the lower extreme fixed connection of unloading pipe (2) has row material pipe (3) that the level set up, it sets up in row material pipe (3) to arrange material mechanism.

2. The device for recovering the cyclopentadiene tricarbonyl manganese refined distillation bed charge with the blockage prevention function as claimed in claim 1, wherein the device comprises: the pushing mechanism comprises a servo motor (4), a rotating rod (5), a first rotating rod (6), a second rotating rod (7) and two groups of material pushing plates (8), a support (9) is fixedly arranged below the interior of the distillation kettle (1), the middle part of the upper end of the support (9) is rotatably connected with the first rotating rod (6) through a first bearing, the rotating rod (5) is transversely arranged below the support (9), the lower end of the first rotating rod (6) penetrates through the support (9) and is fixedly connected with the rotating rod (5), the two groups of material pushing plates (8) are fixedly connected with the lower side of the rotating rod (5), a first bevel gear (10) is fixedly connected with the upper end of the first rotating rod (6), the second rotating rod (7) is transversely arranged on the right side above the support (9), a second bevel gear (11) is fixedly connected with the left end of the second rotating rod (7), the first bevel gear (10) is meshed with the second bevel gear (11) and connected, the right end of the second rotating rod (7) penetrates through the right side wall of the distillation kettle (1) through a second bearing and extends to the outside of the distillation kettle (1), the servo motor (4) is fixedly connected with the right outer side wall of the distillation kettle (1) through a motor base (12), and the output end of the servo motor (4) is fixedly connected with the right end of the second rotating rod (7) through a coupler.

3. The device for recovering the cyclopentadiene tricarbonyl manganese refined distillation bed charge with the blockage prevention function as claimed in claim 2, wherein the device comprises: the two groups of the material pushing plates (8) are both arranged in an arc shape, and the running tracks of the two groups of the material pushing plates (8) are sequentially and alternately arranged.

4. The device for recovering the cyclopentadiene tricarbonyl manganese refined distillation bed charge with the blockage prevention function as claimed in claim 3, wherein the device comprises: the blanking mechanism comprises a first spiral conveying blade (13), the lower end of the first rotating rod (6) extends downwards to the lower portion of the interior of the blanking pipe (2), and the first spiral conveying blade (13) is arranged in the blanking pipe (2) and fixedly sleeved with the first rotating rod (6).

5. The device for recovering the cyclopentadiene manganese tricarbonyl refined distillation bed charge with the blockage prevention function as claimed in claim 4, wherein the device comprises: it includes third bull stick (14) and second spiral delivery leaf (15) to arrange material mechanism, third bull stick (14) and second spiral delivery leaf (15) all set up in the inside of arranging material pipe (3), second spiral delivery leaf (15) are pegged graft with third bull stick (14) are fixed, the right-hand member of third bull stick (14) passes through the third bearing and arranges the right side wall of material pipe (3) and extend to the outside of arranging material pipe (3), belt pulley (16), two have all been cup jointed fixedly on the pole wall right side of second bull stick (7) and third bull stick (14) belt pulley (16) through belt (17) intermeshing.

6. The device for recovering the cyclopentadiene tricarbonyl manganese refined distillation bed charge with the blockage prevention function as claimed in claim 5, wherein the device comprises: the lower end of the distillation still (1) is fixedly connected with a plurality of uniformly distributed support legs (18), and the support legs (18) are fixedly connected with the four corners of the lower end of the distillation still (1) respectively.