CN215462091U

CN215462091U - Intermittent vacuum distillation furnace for farnesol

Info

Publication number: CN215462091U
Application number: CN202120716082.5U
Authority: CN
Inventors: 陈鑫; 田金女
Original assignee: Nanjing Chaoyi Biotechnology Co ltd
Current assignee: Nanjing Chaoyi Biotechnology Co ltd
Priority date: 2021-04-08
Filing date: 2021-04-08
Publication date: 2022-01-11
Anticipated expiration: 2031-04-08

Abstract

The utility model discloses an intermittent vacuum distillation furnace for farnesol, which comprises a base, wherein the upper surface of the base is fixedly connected with a fixed seat, the top of the fixed seat is fixedly connected with a heating seat, the top of the heating seat is fixedly connected with a distillation retort, one side of the distillation retort is provided with a feed inlet, the feed inlet is fixedly connected with a feed pipe, one end of the feed pipe is fixedly connected with a hopper, the outer wall of one side of the distillation retort is fixedly connected with a motor, one end of an output shaft of the motor is fixedly connected with a gear, and the inner circumferential wall of the distillation retort is fixedly connected with two positioning rings. The device can fully stir the farnesol solution through the stirring rod, so that the farnesol solution is uniformly heated, the purification effect of the farnesol solution is improved, meanwhile, the farnesol attached to the distillation tank can be scraped through the scraper, the waste is avoided, the collection tank can be used for facilitating workers to perform centralized treatment on the distilled farnesol solution, and the convenience of the device is improved.

Description

Intermittent vacuum distillation furnace for farnesol

Technical Field

The utility model relates to the technical field of distillation, in particular to a discontinuous vacuum distillation furnace for farnesol.

Background

Farnesol is named as farnesol in Chinese, farnesol is one of daily perfumes limited by IFRA, and the commercial farnesol can be used as a daily perfume only by containing more than ninety-six percent of total weight of farnesol isomers, and is mainly used as a blending material with floral essences, such as lily of the valley, clove, rose, violet, orange blossom, cyclamen and the like.

Farnesol exists in essential oil such as lemongrass oil and citronella oil naturally, so the farnesol is purified by distillation frequently, the purity of the farnesol directly influences the using effect of the farnesol, but the purity after distillation is not enough and the using effect is not good due to nonuniform heating of a distillation and purification device on the market at present, so that the farnesol intermittent vacuum distillation furnace is very necessary.

SUMMERY OF THE UTILITY MODEL

The utility model aims to solve the defects in the prior art and provides a farnesol intermittent vacuum distillation furnace.

In order to achieve the purpose, the utility model adopts the following technical scheme:

an intermittent vacuum distillation furnace for farnesol comprises a base, wherein the upper surface of the base is fixedly connected with a fixed seat, the top of the fixed seat is fixedly connected with a heating seat, the top of the heating seat is fixedly connected with a distillation retort, one side of the distillation retort is provided with a feed inlet, a feed pipe is fixedly connected in the feed inlet, one end of the feed pipe is fixedly connected with a hopper, the outer wall of one side of the distillation retort is fixedly connected with a motor, one end of an output shaft of the motor is fixedly connected with a gear, two positioning rings are fixedly connected with the circumferential inner wall of the distillation retort, an annular fluted disc is clamped between the positioning rings, and the gear is meshed with the annular fluted disc, the bottom of the annular fluted disc is fixedly connected with a stirring rod, one side of the stirring rod is fixedly connected with a spiral sheet, one side fixedly connected with of puddler has a plurality of scrapers, and the scraper blade contacts with the inner wall of retort, the upper surface of base is equipped with cooling device.

As a further scheme of the utility model, the top of the distillation tank is fixedly connected with a reflux cavity, and one side of the feeding pipe is fixedly connected with a control valve.

As a further scheme of the utility model, the cooling device comprises a support frame, the support frame is fixed on the upper surface of the base through bolts, the upper surface of the base is provided with a collection tank, the top of the collection tank is fixedly connected with a connecting flange, the upper surface of the support frame is fixedly connected with a cooling tank, one side of the cooling tank is fixedly connected with a pipeline, one end of the pipeline penetrates through the cooling tank and is fixed with the backflow cavity, the other end of the pipeline penetrates through the cooling tank and is fixed with the connecting flange, one side of the cooling tank is provided with a water inlet, and a water inlet pipe is fixedly connected in the water inlet.

As a further scheme of the utility model, one side of the cooling tank is provided with a water outlet, and a water outlet pipe is fixedly connected in the water outlet.

As a further scheme of the utility model, the outer wall of one side of the pipeline is fixedly connected with a heat-insulating sleeve.

As a further scheme of the utility model, the bottom of the base is fixedly connected with ground feet which are uniformly distributed.

As a further scheme of the utility model, one side of the collecting tank is provided with a mounting opening, and a window is fixedly connected in the mounting opening.

The utility model has the beneficial effects that:

1. through the setting of installation puddler on circular fluted disc, starter motor makes the puddler that the gear drove on the annular fluted disc rotate, and the flight rotates simultaneously to carry out intensive mixing to farnesol solution, make it be heated evenly, avoid being heated the inhomogeneous purity that leads to after the distillation not enough, improved farnesol solution purification effect.

2. Through the setting of installation scraper blade on the puddler, the puddler rotates and makes the scraper blade produce and rotate to make the scraper blade strike off the adhered to farnesol on the retort inner wall, avoid the waste of farnesol solution, practiced thrift the cost.

3. Through the setting that is equipped with the collection tank on the base, the farnesol solution after the distillation passes through the pipeline and gets into in the collection tank, and the collection tank is collected the farnesol solution after the distillation, makes things convenient for the staff to carry out centralized processing, has improved the convenience of device.

Drawings

FIG. 1 is a schematic perspective view of an interrupted vacuum distillation furnace for farnesol according to the present invention;

FIG. 2 is a schematic sectional view of a distillation tank of an intermittent vacuum distillation furnace for farnesol according to the present invention;

FIG. 3 is a schematic sectional view of a cooling tank of an intermittent vacuum distillation furnace for farnesol according to the present invention.

In the figure: 1. a thermal insulation sleeve; 2. a pipeline; 3. a reflux cavity; 4. a hopper; 5. a control valve; 6. a distillation tank; 7. a heating base; 8. a fixed seat; 9. ground feet; 10. a base; 11. a collection tank; 12. a water outlet pipe; 13. a cooling tank; 14. a water inlet pipe; 15. a gear; 16. a motor; 17. an annular fluted disc; 18. a positioning ring; 19. a squeegee; 20. a spiral sheet; 21. a stirring rod; 22. a support frame; 23. a connecting flange; 24. a viewing window.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. It should be noted that unless otherwise explicitly stated or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly and their meaning in the context of this patent may be understood by those skilled in the art as appropriate.

Referring to fig. 1-3, an intermittent vacuum distillation furnace for farnesol comprises a base 10, wherein a fixed seat 8 is fixed on the upper surface of the base 10 through bolts, a heating seat 7 is fixed on the top of the fixed seat 8 through bolts, a distillation retort 6 is fixed on the top of the heating seat 7 through bolts, a feed inlet is formed in one side of the distillation retort 6, a feed pipe is fixed in the feed inlet through bolts, a hopper 4 is fixed at one end of the feed pipe through bolts, a motor 16 is fixed on the outer wall of one side of the distillation retort 6 through bolts, a gear 15 is fixed on one end of an output shaft of the motor 16 through bolts, two positioning rings 18 are fixed on the inner circumferential wall of the distillation retort 6 through bolts, an annular fluted disc 17 is clamped between the positioning rings 18, the positioning rings 18 can position the annular fluted disc 17, so that the annular fluted disc 17 can rotate at a proper position, and the gear 15 is meshed with the annular fluted disc 17, there is puddler 21 bottom annular fluted disc 17 through the bolt fastening, there is flight 20 in one side of puddler 21 through the bolt fastening, starter motor 16, make puddler 21 on gear 15 drives annular fluted disc 17 rotate, flight 20 rotates simultaneously, thereby carry out intensive mixing to farnesol solution, it is even to make it be heated, avoid being heated inhomogeneous purity that leads to after the distillation insufficient, there are a plurality of scraper blades 19 in one side of puddler 21 through the bolt fastening, and scraper blade 19 contacts with retort 6's inner wall, puddler 21 rotates and makes scraper blade 19 produce the rotation, thereby make scraper blade 19 strike off adnexed farnesol on to retort 6 inner wall, avoid the waste of farnesol solution, the upper surface of base 10 is equipped with cooling device.

In the utility model, it should be noted that a reflux cavity 3 is fixed on the top of a distillation tank 6 through a bolt, a control valve 5 is fixed on one side of a feeding pipe through a bolt, the control valve 5 is convenient for a worker to control the inlet and outlet of a solution in the feeding pipe, when the solution in the distillation tank 6 needs to be heated, the control valve 5 is closed to ensure that the distillation tank 6 can keep good sealing property, a cooling device comprises a support frame 22, the support frame 22 is fixed on the upper surface of a base 10 through a bolt, a collecting tank 11 is arranged on the upper surface of the base 10, a distilled farnesol solution enters the collecting tank 11 through a pipeline 2, the collecting tank 11 collects the distilled farnesol solution to facilitate the centralized treatment of the worker, a connecting flange 23 is fixed on the top of the collecting tank 11 through a bolt, a cooling tank 13 is fixed on the upper surface of the support frame 22 through a bolt, and a pipeline 2 is inserted into one side of the cooling tank 13, and the one end of pipeline 2 passes cooling tank 13 and is fixed mutually with backward flow cavity 3, the other end of pipeline 2 passes cooling tank 13 and flange 23 and fixes mutually, flange 23 is convenient to be dismantled, so that in time shift out the solution in the collection tank 11, the water inlet has been seted up to one side of cooling tank 13, there is inlet tube 14 through the bolt fastening in the inlet tube, the delivery port has been seted up to one side of cooling tank 13, there is outlet pipe 12 through the bolt fastening in the outlet port, insulation cover 1 has been cup jointed to one side outer wall of pipeline 2, the bottom of base 10 has lower margin 9 through the bolt fastening, and lower margin 9 evenly distributed, the installing port has been seted up to one side of collection tank 11, there is window 24 through the bolt fastening in the installing port, window 24 makes things convenient for the staff to observe the volume of the farnesol solution in the collection tank 11.

The working principle is as follows: when the farnesol solution needs to be purified, firstly, the control valve 5 is opened, the farnesol solution needing to be purified enters the distillation tank 6 through the hopper 4, cooling water is poured into the cooling tank 13 through the water inlet pipe 14, then the heating seat 7 is started to heat the distillation tank 6, the motor 16 is started, the gear 15 drives the annular fluted disc 17 to rotate, so that the stirring rod 21 rotates to stir the farnesol solution, meanwhile, the stirring rod 21 drives the spiral piece 20 to rotate, the farnesol moves downwards and is dispersed around, meanwhile, the stirring rod 21 drives the scraping plate 19 to rotate, so that the scraping plate 19 scrapes the farnesol attached to the inner wall of the distillation tank 6, the farnesol solution is fully stirred, the solution in the distillation tank 6 is uniformly heated, then the farnesol solution is heated and converted into gas, and enters the pipeline 2 on the cooling tank 13 through the backflow cavity 3, the cooling water then cools the hot gas in the pipe 2, so that the hot gas is condensed into water drops again when meeting cold, and the water drops flow into the collecting tank 11 through the pipe 2 to be collected.

The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and equivalent alternatives or modifications according to the technical solution of the present invention and the inventive concept thereof should be covered by the scope of the present invention.

Claims

1. The intermittent vacuum distillation furnace for farnesol comprises a base (10) and is characterized in that a fixed seat (8) is fixedly connected to the upper surface of the base (10), a heating seat (7) is fixedly connected to the top of the fixed seat (8), a distillation tank (6) is fixedly connected to the top of the heating seat (7), a feed inlet is formed in one side of the distillation tank (6), a feed pipe is fixedly connected to the feed inlet, a hopper (4) is fixedly connected to one end of the feed pipe, a motor (16) is fixedly connected to the outer wall of one side of the distillation tank (6), a gear (15) is fixedly connected to one end of an output shaft of the motor (16), two positioning rings (18) are fixedly connected to the inner circumferential wall of the distillation tank (6), an annular fluted disc (17) is clamped between the positioning rings (18), the gear (15) is meshed with the annular fluted disc (17), and a stirring rod (21) is fixedly connected to the bottom of the annular fluted disc (17), one side fixedly connected with flight (20) of puddler (21), a plurality of scraper blades (19) of one side fixedly connected with of puddler (21), and scraper blade (19) contact with the inner wall of retort (6), the upper surface of base (10) is equipped with cooling device.

2. The intermittent vacuum distillation furnace for farnesol according to claim 1, wherein the top of the distillation pot (6) is fixedly connected with a reflux cavity (3), and one side of the feeding pipe is fixedly connected with a control valve (5).

3. The intermittent vacuum distillation furnace for farnesol according to claim 2, wherein the cooling device comprises a support frame (22), the support frame (22) is fixed on the upper surface of the base (10) through bolts, the upper surface of the base (10) is provided with a collection tank (11), the top of the collection tank (11) is fixedly connected with a connecting flange (23), the upper surface of the support frame (22) is fixedly connected with a cooling tank (13), one side of the cooling tank (13) is fixedly connected with a pipeline (2), one end of the pipeline (2) penetrates through the cooling tank (13) to be fixed with the backflow cavity (3), the other end of the pipeline (2) penetrates through the cooling tank (13) to be fixed with the connecting flange (23), one side of the cooling tank (13) is provided with a water inlet, and a water inlet pipe (14) is fixedly connected in the water inlet.

4. The intermittent vacuum distillation furnace for farnesol according to claim 3, wherein a water outlet is formed in one side of the cooling tank (13), and a water outlet pipe (12) is fixedly connected in the water outlet.

5. The intermittent vacuum distillation furnace for farnesol according to claim 3, wherein the outer wall of one side of the pipeline (2) is fixedly connected with a heat preservation sleeve (1).

6. The intermittent vacuum distillation furnace for farnesol according to claim 1, wherein the bottom of the base (10) is fixedly connected with ground feet (9), and the ground feet (9) are uniformly distributed.

7. The intermittent vacuum distillation furnace for farnesol according to claim 3, wherein a mounting opening is formed in one side of the collecting tank (11), and a window (24) is fixedly connected in the mounting opening.