CN215352416U

CN215352416U - Preparation barium sulfonate uses high-efficient refining plant

Info

Publication number: CN215352416U
Application number: CN202120768249.2U
Authority: CN
Inventors: 马荣辉; 张智慧
Original assignee: Xinji Jinshi Shengrong Chemical Co ltd
Current assignee: Xinji Jinshi Shengrong Chemical Co ltd
Priority date: 2021-04-15
Filing date: 2021-04-15
Publication date: 2021-12-31
Anticipated expiration: 2031-04-15

Abstract

The utility model discloses a high-efficiency refining device for preparing barium sulfonate, and relates to a barium sulfonate refining device which comprises a filter tank and an evaporation tank, wherein the filter tank and the evaporation tank are both of hollow cylindrical structures, a glass tube is fixedly arranged in the middle of the evaporation tank along the central axis direction, two ends of the glass tube are fixedly arranged on the inner top surface and the inner bottom surface of the evaporation tank, a heating element is also fixedly arranged in the middle of the glass tube, a helical blade is fixedly arranged in the evaporation tank, and the helical blade forms a rotary channel for barium sulfonate liquid to flow from top to bottom. The backflow channel formed by the spiral blades can prolong the flowing path of the barium sulfonate liquid, further prolong the heating time, and improve the heating efficiency to the maximum extent in a limited space, so that the purpose of fully separating out water in the barium sulfonate liquid is achieved, and the effect of efficient refining is achieved.

Description

Preparation barium sulfonate uses high-efficient refining plant

Technical Field

The utility model relates to a barium sulfonate refining device, in particular to a high-efficiency refining device for preparing barium sulfonate.

Background

The antirust agent is prepared by sulfonating petroleum oil fraction, alcohol-water extracting to obtain product, saponifying with barium salt, and refining, and has strong antirust performance, corrosion inhibiting effect on metal and high antirust performance.

Then, after the barium sulfonate liquid is stored for a long time, some precipitates can be separated out from the barium sulfonate liquid, or some impurity particles can be doped in the original barium sulfonate liquid, especially after the barium sulfonate liquid is stored for a long time in a humid environment, if the tank body containing the barium sulfonate liquid has poor sealing performance, moisture can easily enter, and the barium sulfonate liquid contains moisture, so that the purity of subsequent use is influenced.

SUMMERY OF THE UTILITY MODEL

The present invention has been made to solve the above problems of the prior art, and an object of the present invention is to provide an efficient refining apparatus for producing barium sulfonate.

In order to achieve the purpose, the utility model provides the following technical scheme:

the utility model provides a preparation barium sulfonate uses high-efficient refining plant, includes filter tank and evaporating pot, filter tank and evaporating pot are hollow structure's tubular structure, the interior middle part of evaporating pot is provided with the glass pipe along the axis direction is fixed, the both ends fixed mounting of glass pipe is in the interior top surface and the interior bottom surface of evaporating pot, glass pipe middle part still fixed mounting has the heating member, fixed mounting has helical blade on the inside of evaporating pot, helical blade forms the passageway that circles round that is used for barium sulfonate liquid top-down to trickle, the fixed one end that communicates the filling tube in the interior top of evaporating pot, and the sealed and fastening intercommunication of one end of filling tube is at the output of drawing liquid pump, drawing liquid pump fixed mounting is on the lateral surface of evaporating pot, and the input of drawing liquid pump passes through the sealed and fastening intercommunication lower part in the filter tank of liquid delivery pipe, the lateral surface fixed mounting of filter tank has other drawing liquid pump, the output end of the liquid pump penetrates into the inner top cavity of the filter tank from the tank cover at the top of the filter tank through a liquid through pipe, and the input end of the liquid pump is fixedly communicated with a liquid conveying pipe used for introducing barium sulfonate stock solution.

As a further scheme of the utility model: the helical blade is made of tungsten steel materials through integral forming.

As a further scheme of the utility model: the heating member is an electric heating pipe, and the electric heating pipe is positioned in the middle of the glass pipe and is not contacted with the inner peripheral wall of the glass pipe.

As a further scheme of the utility model: the evaporating pot top is provided with a plurality of gas pockets that supply the gas to volatilize.

As a further scheme of the utility model: the top and the bottom of the filter tank and the evaporating tank are respectively provided with a feed inlet and a discharge port.

As a further scheme of the utility model: the filter unit comprises a plurality of net cylinders which can move vertically in the filter tank, adjacent net cylinders are fixedly connected through a connecting rod, and a plurality of uniformly distributed overflow holes are formed in the bottom surface of each net cylinder.

As a further scheme of the utility model: every be provided with the stirring rod in the net section of thick bamboo, the stirring rod suit is on the (mixing) shaft, and the (mixing) shaft top runs through out the filter tank and is connected with actuating mechanism, the tip of stirring rod still fixedly connected with be used for with the scraper blade that corresponds net section of thick bamboo internal perisporium sliding contact.

As a further scheme of the utility model: the driving mechanism comprises a speed reducing motor fixedly installed in a motor box, an output shaft of the speed reducing motor penetrates out of the motor box downwards and is connected with the top of the stirring shaft through a coupler, the top surface of the motor box is fixedly connected with an output end of an electric push rod, and the electric push rod is fixed on the ground through a support frame.

Compared with the prior art, the utility model has the beneficial effects that:

according to the utility model, the barium sulfonate stock solution is introduced into the filter tank through the liquid conveying pipe for filtering, impurity particles in the barium sulfonate stock solution are filtered, then the filtered barium sulfonate liquid is pumped into the evaporation tank for heating, a backflow channel formed by the spiral blade can prolong the flowing path of the barium sulfonate liquid, and further prolong the heating time, so that the heating efficiency can be improved to the maximum extent in a limited space, the purpose of fully separating out moisture in the barium sulfonate liquid is achieved, the effect of efficient refining is realized, the liquid can be scattered through the stirring rod, the filtering effect is improved, and the scraper can clean adhered substances on the inner peripheral wall of the screen cylinder.

Drawings

FIG. 1 is a schematic structural view of the present invention;

FIG. 2 is a schematic view of the inside structure of an evaporation tank according to the present invention;

FIG. 3 is a schematic view of the inside of the filtration tank of the present invention;

fig. 4 is an enlarged view of a structure in fig. 3.

In the figure: 1. a filter tank; 2. an evaporator tank; 3. a transfusion tube; 4. a liquid pump; 5. a liquid pipe is communicated; 6. a motor case; 7. a support frame; 8. an electric push rod; 9. a liquid delivery pipe; 10. a glass tube; 11. a helical blade; 12. an electric heating tube; 13. a liquid feeding pipe; 14. a stirring shaft; 15. a squeegee; 16. an overflow aperture; 17. a net drum; 18. a stirring rod.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

In the first embodiment, please refer to fig. 1 and fig. 2, a high-efficiency refining apparatus for preparing barium sulfonate comprises a filter tank 1 and an evaporator tank 2, wherein the filter tank 1 and the evaporator tank 2 are both of a hollow cylindrical structure, a glass tube 10 is fixedly disposed in the middle of the evaporator tank 2 along the central axis, two ends of the glass tube 10 are fixedly mounted on the inner top surface and the inner bottom surface of the evaporator tank 2, a heating member is further fixedly mounted in the middle of the glass tube 10, a helical blade 11 is fixedly mounted in the evaporator tank 2, the helical blade 11 forms a circular channel for flowing barium sulfonate liquid from top to bottom, the inner top of the evaporator tank 2 is fixedly communicated with one end of a liquid feeding tube 13, one end of the liquid feeding tube 13 is hermetically and fixedly communicated with the output end of a liquid pumping pump 4, the liquid pumping pump 4 is fixedly mounted on the outer side surface of the evaporator tank 2, and the input end of the liquid pumping pump 4 is hermetically and fixedly communicated with the inner lower portion of the filter tank 1 through a liquid feeding tube 9, the utility model discloses a barium sulfonate liquid heating device, including filtration jar 1, the lateral surface fixed mounting of filtration jar 1 has other drawing liquid pump 4, the output of this drawing liquid pump 4 passes through the interior top chamber that filters jar 1 from filtration jar 1 top cover through liquid through-flow pipe 5, the fixed intercommunication of input of this drawing liquid pump 4 has the transfer line 3 that is used for letting in the barium sulfonate stoste, let in the barium sulfonate stoste through transfer line 3 and filter filtration jar 1, filter impurity particle in the barium sulfonate stoste, then with the barium sulfonate liquid suction after filtering and heat in evaporating pot 2, the backward flow passageway that helical blade 11 formed can prolong the trickle route of barium sulfonate liquid, and then extension heat time, can furthest improve heating efficiency in limited space like this, thereby reach the mesh of fully separating out moisture in the barium sulfonate liquid, realize this effect of high-efficient refining.

The helical blade 11 is made of tungsten steel integrally formed and has excellent corrosion resistance and high temperature resistance.

The heating member is electric heating pipe 12, and electric heating pipe 12 is in glass pipe 10 and is in the middle part, not with the contact of the internal perisporium of glass pipe 10, and the heat that produces through electric heating pipe 12 is diffused to evaporating pot 2 through glass pipe 10 in, heats barium sulfonate liquid to make the water analysis of doping in the barium sulfonate liquid, promoted the purity of barium sulfonate liquid, realize high-efficient refined purpose.

The top of the evaporating pot 2 is provided with a plurality of air holes for air volatilization.

The top and the bottom of the filter tank 1 and the evaporating tank 2 are respectively provided with a feed inlet and a discharge port.

In the second embodiment, referring to fig. 3 and fig. 4, the following technical features are added on the basis of the first embodiment: still including filtering the filter unit that sets up in jar 1, filter unit includes a plurality of net section of thick bamboo 17 that can follow vertical removal in filtering jar 1, and adjacent net section of thick bamboo 17 passes through connecting rod fixed connection, the overflow hole 16 of a plurality of equipartitions is seted up to net section of thick bamboo 17 bottom surface, and overflow hole 16 supplies liquid to flow down, and the foreign particles is held back in net section of thick bamboo 17.

Every be provided with stirring rod 18 in the net section of thick bamboo 17, stirring rod 18 suit is on (mixing) shaft 14, and (mixing) shaft 14 top is run through out filter tank 1 and is connected with actuating mechanism, the tip of stirring rod 18 still fixedly connected with be used for with the scraper blade 15 that corresponds net section of thick bamboo 17 internal perisporium sliding contact, can break up liquid through stirring rod 18, improve the filter effect, scraper blade 15 can clean the adherent of net section of thick bamboo 17 internal perisporium.

Actuating mechanism includes the gear motor of fixed mounting in motor case 6, gear motor's output shaft runs through out motor case 6 and passes through 14 tops of coupling joint (mixing) shaft down, 6 top surface fixed connection electric putter 8's of motor case output, electric putter 8 is fixed subaerial through support frame 7, can carry out the filter tank 1 with a net section of thick bamboo 17 through electric putter 8, carries out periodic cleaning.

The third embodiment is different from the first and second embodiments in that a temperature sensor is installed in the evaporation tank 2 for monitoring the real-time temperature in the evaporation tank 2, so that the evaporation condition of the barium sulfonate liquid can be controlled, and evaporation loss of the effective components of the barium sulfonate liquid due to overheating can be avoided.

During the specific use, start drawing liquid pump 4, let in the barium sulfonate stoste through transfer line 3 and filter filtering tank 1, filter impurity particle in the barium sulfonate stoste, then with the barium sulfonate liquid suction after filtering heating in evaporating pot 2, the backward flow passageway that helical blade 11 formed can prolong the trickling route of barium sulfonate liquid, and then extension heating time, can furthest's improvement heating efficiency in limited space like this, thereby reach the purpose that fully appears the moisture in the barium sulfonate liquid, realize this effect of high-efficient refining.

The power supply interface of the power utilization element in the utility model is connected with a power supply system through a switch (not shown in the figure) and a lead (not shown in the figure), so as to realize the control of the power supply interface, wherein the related circuits and control are the prior art, are well known in the prior art, and are not described herein in detail.

In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "connected" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood by those of ordinary skill in the art through specific situations.

Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the utility model can be made, and equivalents and modifications of some features of the utility model can be made without departing from the spirit and scope of the utility model.

Claims

1. The high-efficiency refining device for preparing barium sulfonate comprises a filter tank (1) and an evaporating tank (2), and is characterized in that the filter tank (1) and the evaporating tank (2) are of a hollow-structure cylinder structure, a glass tube (10) is fixedly arranged in the middle of the evaporating tank (2) along the central axis direction, two ends of the glass tube (10) are fixedly arranged on the inner top surface and the inner bottom surface of the evaporating tank (2), a heating element is fixedly arranged in the middle of the glass tube (10), a helical blade (11) is fixedly arranged in the evaporating tank (2), the helical blade (11) forms a rotary channel for flowing barium sulfonate liquid from top to bottom, one end of a liquid adding tube (13) is fixedly communicated with the inner top of the evaporating tank (2), one end of the liquid adding tube (13) is sealed and fixedly communicated with the output end of a liquid pumping pump (4), and the liquid pumping pump (4) is fixedly arranged on the outer side surface of the evaporating tank (2), and the input of drawing liquid pump (4) passes through the interior lower part that liquid sending pipe (9) is sealed and the fastening intercommunication crosses filter tank (1), the lateral surface fixed mounting who crosses filter tank (1) has other drawing liquid pump (4), and the output of this drawing liquid pump (4) is through leading to liquid pipe (5) and passing through the interior apical chamber that crosses filter tank (1) from filter tank (1) top cover, and the fixed intercommunication of input of this drawing liquid pump (4) has transfer line (3) that are used for letting in the barium sulfonate stoste.

2. The efficient refining device for preparing barium sulfonate according to claim 1, wherein the helical blade (11) is made of tungsten steel by integral molding.

3. The high-efficiency refining device for preparing barium sulfonate according to claim 1, wherein the heating element is an electric heating tube (12), and the electric heating tube (12) is located at the center of the glass tube (10) and does not contact with the inner peripheral wall of the glass tube (10).

4. The high-efficiency refining device for preparing barium sulfonate according to claim 1, wherein the top of the evaporation tank (2) is provided with a plurality of air holes for gas volatilization.

5. The efficient refining device for preparing barium sulfonate according to claim 1, wherein the top and the bottom of the filter tank (1) and the evaporation tank (2) are respectively provided with a feeding port and a discharging port.

6. The efficient refining device for preparing the barium sulfonate according to any one of claims 1 to 5, further comprising a filtering unit arranged in the filtering tank (1), wherein the filtering unit comprises a plurality of net cylinders (17) capable of vertically moving in the filtering tank (1), the adjacent net cylinders (17) are fixedly connected through a connecting rod, and a plurality of uniformly distributed overflow holes (16) are formed in the bottom surface of each net cylinder (17).

7. The efficient refining device for preparing barium sulfonate according to claim 6, wherein each screen cylinder (17) is provided with a stirring rod (18), the stirring rod (18) is sleeved on the stirring shaft (14), the top of the stirring shaft (14) penetrates out of the filter tank (1) and is connected with a driving mechanism, and the end part of the stirring rod (18) is fixedly connected with a scraper (15) which is used for being in sliding contact with the inner peripheral wall of the corresponding screen cylinder (17).

8. The efficient refining device for preparing barium sulfonate according to claim 7, wherein the driving mechanism comprises a speed reducing motor fixedly installed in a motor box (6), an output shaft of the speed reducing motor penetrates downwards out of the motor box (6) and is connected with the top of the stirring shaft (14) through a coupler, the top surface of the motor box (6) is fixedly connected with the output end of an electric push rod (8), and the electric push rod (8) is fixed on the ground through a support frame (7).