CN214971786U - Schisandrin B purification device - Google Patents
Schisandrin B purification device Download PDFInfo
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- CN214971786U CN214971786U CN202120689535.XU CN202120689535U CN214971786U CN 214971786 U CN214971786 U CN 214971786U CN 202120689535 U CN202120689535 U CN 202120689535U CN 214971786 U CN214971786 U CN 214971786U
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- reaction tank
- tank body
- flowing medium
- interlayer
- schisandrin
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Abstract
The utility model discloses a Schisandrin B purification device, which comprises a reaction tank body containing Schisandrin B acetone crude extract, a tank cover arranged at the top of the reaction tank body, a dropping funnel for adding water and a stirring mechanism, wherein the dropping funnel is arranged above the tank cover; the reaction tank body is double-layer glass provided with an interlayer, a heat-conducting flowing medium is injected into the interlayer, the upper part of the interlayer is provided with a flowing medium outlet, the lower part of the interlayer is provided with a flowing medium inlet, and the flowing medium outlet and the flowing medium inlet are connected with the high-low temperature circulating device through a flowing medium conveying pipeline; the below of the retort body is equipped with the support frame body, supports and fills up between support frame body and the retort body and be equipped with the heat insulating block, the utility model discloses the advantage is: the Schisandrin B purification device of the device is convenient for carrying out crystallization separation and fine extraction on the Schisandrin B acetone crude extract, and is simple to operate and convenient to control.
Description
Technical Field
The utility model relates to a chinese magnoliavine fruit B element purification technical field, concretely relates to chinese magnoliavine fruit B element purification device.
Background
At present, the domestic patent and literature data of a schisandrin B purification device are also fresh.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide a schisandrin B purification device aiming at the above requirements.
A Schisandrin B purification device comprises a reaction tank containing Schisandrin B acetone crude extract, a tank cover arranged at the top of the reaction tank, a dropping funnel for adding water and arranged above the tank cover, and a stirring mechanism;
the reaction tank body is double-layer glass provided with an interlayer, a heat-conducting flowing medium is injected into the interlayer, the upper part of the interlayer is provided with a flowing medium outlet, the lower part of the interlayer is provided with a flowing medium inlet, and the flowing medium outlet and the flowing medium inlet are connected with the high-low temperature circulating device through a flowing medium conveying pipeline; a support frame body is arranged below the reaction tank body, and a heat insulation block is arranged between the support frame body and the reaction tank body in a cushioning manner;
the tank cover is also provided with an exhaust valve, one side of the tank cover is provided with a liquid adding inlet communicated to the inside of the reaction tank body, the liquid adding inlet is provided with the dropping funnel for adding water, and the other side of the tank cover is provided with an acetone liquid backflow inlet communicated to the inside of the reaction tank body; the acetone liquid reflux inlet is connected with an arc-shaped reflux pipe, the end part of the arc-shaped reflux pipe is connected with the spherical liquid collecting part, the arc-shaped reflux pipe and the spherical liquid collecting part are of an integrally formed structure, the upper part of the spherical liquid collecting part is connected with a condensing pipe, and the lower part of the spherical liquid collecting part is provided with an acetone liquid discharge valve;
the stirring mechanism comprises a stirring motor, a stirring shaft connected with a stirring motor rotating shaft and extending into the reaction tank body, and a group of stirring blades arranged on the stirring shaft, wherein a vertical rod is arranged on the support frame body, a motor mounting plate is fixedly connected to the vertical rod, and the stirring motor is mounted on the motor mounting plate.
The bottom of the reaction tank body is also provided with a schisandra chinensis B essence extract liquid outlet with a valve.
The end part of the arc-shaped return pipe is connected with the middle part of the spherical liquid collecting part.
The vertical rod is further provided with a first limiting clamp and a second limiting clamp, the first limiting clamp clamps and fixes the condensation pipe, and the second limiting clamp clamps and fixes the lower part of the spherical liquid collecting part.
The group of stirring blades consists of two stirring blades which are arranged on the stirring shaft and are positioned at the lower part and the middle part of the reaction tank body.
The stirring paddle is a turbine type straight blade consisting of four blades.
The utility model has the advantages that: the Schisandrin B purification device of the device is convenient for carrying out crystallization separation and fine extraction on the Schisandrin B acetone crude extract, and is simple to operate and convenient to control.
Description of the drawings
Fig. 1 is a schematic structural diagram of the present invention.
Fig. 2 is a schematic structural view of the stirring blade.
Detailed Description
As shown in the attached drawing, the schizandrin B purification device comprises a reaction tank body 1 containing schizandrin B acetone crude extract, a tank cover 2 arranged at the top of the reaction tank body 1, a dropping funnel 3 for adding water arranged above the tank cover 2 and a stirring mechanism;
the reaction tank body 1 is double-layer glass provided with an interlayer 5, a heat-conducting flowing medium is injected into the interlayer 5, the upper part of the interlayer 5 is provided with a flowing medium outlet 7, the lower part of the interlayer 5 is provided with a flowing medium inlet 8, and the flowing medium outlet 7 and the flowing medium inlet 8 are connected with a high-low temperature circulating device 9 through a flowing medium conveying pipeline; a support frame body 10 is arranged below the reaction tank body 1, and a heat insulation block 6 is arranged between the support frame body 10 and the reaction tank body 1 in a cushioning manner;
the tank cover 2 is also provided with an exhaust valve 11, one side of the tank cover 2 is provided with a liquid adding inlet communicated to the inside of the reaction tank body 1, the liquid adding inlet is provided with the dropping funnel 3 for adding water, and the other side of the tank cover 2 is provided with an acetone liquid backflow inlet 12 communicated to the inside of the reaction tank body 1; the acetone liquid reflux inlet 12 is connected with an arc reflux pipe 13, the end part of the arc reflux pipe 13 is connected with a spherical liquid collecting part 14, the arc reflux pipe 13 and the spherical liquid collecting part 14 are of an integrally formed structure, the upper part of the spherical liquid collecting part 14 is connected with a condensing pipe 15, and the lower part of the spherical liquid collecting part 14 is provided with an acetone liquid discharge valve 16;
the stirring mechanism comprises a stirring motor 17, a stirring shaft 18 connected with a rotating shaft of the stirring motor 17 and extending into the interior of the reaction tank body 1, and a group of stirring blades 19 arranged on the stirring shaft 18, wherein a vertical rod 21 is arranged on the support frame body 10, a motor mounting plate 20 is fixedly connected to the vertical rod 21, and the stirring motor 17 is mounted on the motor mounting plate 20.
The bottom of the reaction tank body 1 is also provided with a schisandra chinensis B essence extract liquid outlet with a valve.
The end of the curved return pipe 13 is connected to the middle of the spherical liquid collecting part 14.
The vertical rod 21 is further provided with a first limiting clamp 31 and a second limiting clamp 32, the condensation pipe 15 is clamped and fixed by the first limiting clamp 31, and the lower portion of the spherical liquid collecting portion 14 is clamped and fixed by the second limiting clamp 32.
The group of stirring blades 19 consists of two stirring blades which are arranged on the stirring shaft 18 and are positioned at the lower part and the middle part of the reaction tank body 1.
The stirring paddle 19 is a turbine straight blade composed of four blades.
The working principle is as follows: firstly, the crude schisandrin B acetone extract is poured into a reaction tank body 1, then a tank cover 2 is covered, a stirring motor 17 is started, water is dripped into the reaction tank body 1 through a dropping funnel 3 for adding water, meanwhile, a high-low temperature circulating device 9 is started to heat the reaction tank body 1 through an interlayer 5 and a heat conduction flowing medium, acetone solution is heated and evaporated and flows into an arc-shaped backflow pipe 13 through an acetone solution backflow inlet 12, and then enters a spherical liquid collection part 14, the acetone solution is condensed into acetone solution again through a condensing pipe 15 and then falls into the spherical liquid collection part 14, and whether the condensed acetone solution is collected or not or whether the condensed acetone solution is collected or returned to the reaction tank body 1 for continuous purification is selected according to needs. After the acetone in the crude extract of schisandrin B acetone is evaporated, schisandrin B can be crystallized and separated out after water is added because of being insoluble in water, and impurities which are easy to dissolve in water in the crude extract can be dissolved in the water dripped in, thereby achieving the purpose of extraction.
Claims (6)
1. A Schisandrin B purification device is characterized by comprising a reaction tank body (1) containing Schisandrin B acetone crude extract, a tank cover (2) arranged at the top of the reaction tank body (1), a dropping funnel (3) arranged above the tank cover (2) and used for adding water, and a stirring mechanism;
the reaction tank body (1) is double-layer glass provided with an interlayer (5), a heat-conducting flowing medium is injected into the interlayer (5), a flowing medium outlet (7) is formed in the upper part of the interlayer (5), a flowing medium inlet (8) is formed in the lower part of the interlayer (5), and the flowing medium outlet (7) and the flowing medium inlet (8) are connected with a high-low temperature circulating device (9) through a flowing medium conveying pipeline; a support frame body (10) is arranged below the reaction tank body (1), and a heat insulation block (6) is arranged between the support frame body (10) and the reaction tank body (1) in a cushioning manner;
an exhaust valve (11) is further arranged on the tank cover (2), a liquid adding inlet communicated with the interior of the reaction tank body (1) is formed in one side of the tank cover (2), the liquid adding inlet is provided with the dropping funnel (3) for adding water, and an acetone liquid backflow inlet (12) communicated with the interior of the reaction tank body (1) is formed in the other side of the tank cover (2); the acetone liquid reflux inlet (12) is connected with an arc-shaped reflux pipe (13), the end part of the arc-shaped reflux pipe (13) is connected with a spherical liquid collecting part (14), the arc-shaped reflux pipe (13) and the spherical liquid collecting part (14) are of an integrally formed structure, the upper part of the spherical liquid collecting part (14) is connected with a condenser pipe (15), and the lower part of the spherical liquid collecting part (14) is provided with an acetone liquid discharge valve (16);
rabbling mechanism includes agitator motor (17), is connected and stretches into inside (mixing) shaft (18) of the retort body (1) and set up a set of stirring paddle leaf (19) on (mixing) shaft (18) with agitator motor (17) pivot, be equipped with a vertical pole (21) on support frame body (10), the rigid coupling has motor mounting panel (20) on vertical pole (21), agitator motor (17) are installed on motor mounting panel (20).
2. The device for purifying schizandrin B according to claim 1, wherein the bottom of the reaction tank body (1) is further provided with a refined schizandrin B extract liquid outlet with a valve.
3. The schizandrin B purification device according to claim 1, wherein the end of the curved return pipe (13) is connected to the middle of the spherical liquid collecting part (14).
4. The schizandrin B purification device according to claim 1, wherein the vertical rod (21) is further provided with a first limit clamp (31) and a second limit clamp (32), the first limit clamp (31) clamps and fixes the condensation tube (15), and the second limit clamp (32) clamps and fixes the lower portion of the spherical liquid collection portion (14).
5. The schizandrin B purification device according to claim 1, wherein one set of stirring blades (19) consists of two stirring blades arranged on the stirring shaft (18) and located at the lower part and the middle part of the reaction tank body (1).
6. The schizandrin B purification device according to claim 1, wherein the stirring blade (19) is a turbine type straight blade consisting of four blades.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120689535.XU CN214971786U (en) | 2021-04-06 | 2021-04-06 | Schisandrin B purification device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120689535.XU CN214971786U (en) | 2021-04-06 | 2021-04-06 | Schisandrin B purification device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214971786U true CN214971786U (en) | 2021-12-03 |
Family
ID=79096321
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202120689535.XU Active CN214971786U (en) | 2021-04-06 | 2021-04-06 | Schisandrin B purification device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214971786U (en) |
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2021
- 2021-04-06 CN CN202120689535.XU patent/CN214971786U/en active Active
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