CN108607228A - A kind of chemical industry distilling apparatus - Google Patents
A kind of chemical industry distilling apparatus Download PDFInfo
- Publication number
- CN108607228A CN108607228A CN201810484190.7A CN201810484190A CN108607228A CN 108607228 A CN108607228 A CN 108607228A CN 201810484190 A CN201810484190 A CN 201810484190A CN 108607228 A CN108607228 A CN 108607228A
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- China
- Prior art keywords
- side wall
- distillation case
- distillation
- chemical industry
- cooling cylinder
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of chemical industry distilling apparatus, including pedestal, incubator, distillation case and heating dish；The distillation box top is equipped with liquid-feeding tube, and capping is equipped at the top of the liquid-feeding tube；The distillation lower box part is equipped with the first outlet tube, and the first outlet tube outlet end passes through incubator side wall to be equipped with the first valve；The distillation case side wall is equipped with spiral insulating tube, and spiral insulating tube upper end is equipped with exhaust pipe；The base top is equipped with cooling cylinder, and coolant liquid is contained in the cooling cylinder；Condenser pipe is equipped in the cooling cylinder, the distillation case is internally provided with blender；The heat insulation effect of distillation case is strengthened, distillation efficiency is improved, the temperature for reducing steam is more conducive to condense, and reduces the use of condensate liquid, economizes on resources.Using so that heated liquid is more uniform for blender, strengthens heated liquid speed, improves efficiency.
Description
Technical field
The invention belongs to chemical technology field more particularly to a kind of chemical industry distilling apparatus.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, it is different using each component boiling point in mixing liquid or liquid-solid system,
So that low boiling component is evaporated, then condense to detach the unit process of entire component, is two kinds of unit operations of evaporation and condensation
Joint.With other separation means, such as extraction, filtering for crystallizing compare, its advantage is that without the use of system components with
Outer other solvents, to ensure that new impurity will not be introduced.
It needs to heat in distillation process, heat is easy to distribute in distillation process, causes distillation speed slower；And it commonly steams
Distillation unit vapor (steam) temperature when being condensed to steam is higher, and condensation effect is poor, and coolant liquid is caused to need to frequently replace, very not
It is convenient；Common distilling apparatus has that fuel factor is slower, and mixing liquid heating effect is poor in distillation process, causes to heat
Time lengthens, and wastes time.
Invention content
For overcome the deficiencies in the prior art, a kind of present invention offer heating time is short, the change with heat preservation and energy conservation effects
Work distilling apparatus.
Technical solution is used by the present invention solves the problems, such as it：A kind of chemical industry distilling apparatus, including pedestal, incubator,
Distill case and heating dish；The distillation box top is equipped with liquid-feeding tube, and capping is equipped at the top of the liquid-feeding tube；Under the distillation case
Portion is equipped with the first outlet tube, and the first outlet tube outlet end passes through incubator side wall to be equipped with the first valve；The distillation case side
Wall is equipped with spiral insulating tube, and spiral insulating tube upper end is equipped with exhaust pipe；The base top is equipped with cooling cylinder, the condensation
Coolant liquid is contained in case；Condenser pipe is equipped in the cooling cylinder, the distillation case is internally provided with blender；It is hot in cooling procedure
Amount distributes, and the air between incubator and distillation case heats, and to play insulation effect, is conducive to improve distillation effect
Rate, while being more conducive to condense by tentatively cooling steam；Blender can save the time with accelerating liquid by thermal velocity.
Further, the blender includes motor and the agitating shaft that is connected with motor output shaft, and agitating shaft is equipped with
Agitating paddle；Blender controls agitating shaft and drives agitating paddle operating, and aqueous agitation is heated evenly, and heating time is faster.
Further, the agitating shaft and motor output shaft are to be threadedly coupled so that can be with when output shaft is driven by motor
Stablize rotation, not will produce shaking, impact effect.
Further, the motor direction of rotation and the threaded connection direction of agitating shaft and motor output shaft are on the contrary, ensure
Being stably connected between agitating shaft and output shaft, will not shake more turning when agitating shaft rotates.
Further, the agitating shaft and distillation bottom portion are to be rotatably assorted；Agitating shaft is matched with distillation bottom portion, is added
The stability of blender when strong rotation so that heating effect is more preferable.
Further, the distillation case side wall is equipped with temperature sensing device；When the liquid distilled in case is heated to centainly
When temperature does not need blender stirring, temperature sensing device can transmit a signal to blender, stop the running of blender, save money
Source.
Further, the exhaust pipe passes through distillation case side wall to be connected to distillation case inner top；Gas is heated to float upwards,
Exhaust pipe setting can be collected into the gas more evaporated at top, reinforce distilling effect.
Further, the condenser pipe inlet is connected to spiral insulating tube lower end；The condenser pipe liquid feeding end passes through cold
The solidifying case side wall upper left corner and be fixedly connected with cooling cylinder side wall, the condenser pipe outlet end pass through the cooling cylinder side wall lower right corner and with
Cooling cylinder side wall is fixedly connected, and condenser pipe and spiral insulating tube lower end are communicated with to collect the gas after distillation, condenser pipe with
Side wall is fixedly connected with the stability of reinforcement structure.
Further, the spiral insulating tube is located between incubator and distillation case；Spiral insulating tube bottom end passes through
Incubator side wall；Reinforce the heat insulation effect of spiral insulating tube.
The beneficial effects of the invention are as follows：The heat insulation effect of distillation case is strengthened, distillation efficiency is improved, reduces the temperature of steam
Degree is more conducive to condense, and reduces the use of condensate liquid, economizes on resources.Using so that heated liquid is more uniform for blender, reinforces
Heated liquid speed, improves efficiency.
Description of the drawings
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is the structural schematic diagram of spiral insulating tube in the present invention.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
As shown in Figs. 1-2, in the embodiment of the present invention, a kind of chemical industry distilling apparatus with heat preservation and energy conservation effects, including bottom
Seat 1,1 top of the pedestal, which is fixed by the bracket, is provided with incubator 2, and bottom, which is fixed by the bracket, in incubator 2 is provided with steaming
Case 3 is evaporated, 3 bottom of distillation case is fixedly installed heating dish 4；3 top right side of distillation case is connected with liquid-feeding tube 9, and liquid-feeding tube 9 pushes up
Portion is threaded with capping 10 across insulating tube 2；3 lower left corner of distillation case is connected with the first outlet tube 5, the first outlet tube 5
Outlet end is connected with the first valve 6 across 2 side wall of insulating tube；3 side wall of the distillation case fixation is wound with spiral insulating tube 7, spiral shell
Rotation insulating tube 7 is located between insulating tube 2 and distillation case 3；7 port closed of spiral insulating tube, the connection of 7 upper end of spiral insulating tube
There are exhaust pipe 8, exhaust pipe 8 that distillation 3 side wall of case is passed through to be connected to distillation 3 inner top of case；The spiral insulating tube 7 uses copper pipe,
Copper pipe thermal conductivity is good, and when being distilled to solution, the steam of generation is entered by exhaust pipe 8 in spiral insulating tube 7, in spiral insulating tube
Tentatively cooling in 7, heat distributes in cooling procedure, and the air between insulating tube 2 and distillation case 3 heats, to play
Insulation effect is conducive to improve distillation efficiency, while being more conducive to condense by tentatively cooling steam；The spiral insulating tube 7
Bottom end is connected to 2 external right side of insulating tube across 2 side wall of insulating tube.
1 top of the pedestal, which is also fixed by the bracket, is provided with cooling cylinder 11, and coolant liquid is contained in cooling cylinder 11；It is described
11 top right side of cooling cylinder is provided with liquid injection port 12, and 11 lower left corner of the cooling cylinder is connected with the second outlet tube 14, and second goes out liquid
The second valve 15 is connected on pipe 14；Condenser pipe 13 is provided in the cooling cylinder 11,13 liquid feeding end of the condenser pipe passes through cold
It coagulates the 11 side wall upper left corner of case and is fixedly connected with 11 side wall of cooling cylinder, 13 inlet of the condenser pipe and 7 lower end of spiral insulating tube
Connection；13 outlet end of the condenser pipe passes through the 11 side wall lower right corner of cooling cylinder and is fixedly connected with 11 side wall of cooling cylinder, described cold
Solidifying pipe 13 is helix tube, and solution condensation channel is longer, and condensation effect is more preferable；The condenser pipe 13 uses copper pipe, copper pipe thermal conductivity
It is good, convenient for cooling；Tentatively cooling steam downward spiral flows into condenser pipe 13, is further condensed, condensed
Liquid is discharged from 13 liquid outlet of condenser pipe.
The distillation case 3 is internally provided with blender 20；After injecting liquid activated heater into distillation case 3, blender is opened
Beginning work.The operating of motor 21 drives the operating of agitating shaft 22 so that agitating paddle starts to rotate, and stirs liquid so that heated liquid
More uniformly；Blender 20 can save the time with accelerating liquid by thermal velocity.
The blender 20 includes motor 21 and the agitating shaft 22 being connected with 21 output shaft of motor, and agitating shaft 22 is equipped with
Agitating paddle 23；Blender 20 controls agitating shaft 22 and agitating paddle 23 is driven to operate, and aqueous agitation is heated evenly, and heating time is more
Soon.
The agitating shaft 22 is to be threadedly coupled with 21 output shaft of motor so that output shaft can be stablized when being driven by motor 21
Rotation, not will produce shaking, impact effect；Preferably, 21 direction of rotation of the motor and 21 output shaft of agitating shaft 22 and motor
Threaded connection direction on the contrary, ensure agitating shaft 22 rotate when agitating shaft 22 and output shaft between being stably connected with, will not more turn
More shake.The agitating shaft 22 is to be rotatably assorted with 3 bottom of distillation case；Agitating shaft 22 is matched with 3 bottom of distillation case, reinforces rotation
When blender 20 stability so that heating effect is more preferable.
3 side wall of distillation case is equipped with temperature sensing device 24；When the liquid distilled in case 3 is heated to certain temperature not
When blender 20 being needed to stir, temperature sensing device 24 can transmit a signal to blender 20, stop the running of blender 20, save
Resource.The temperature sensing device 24 is temperature sensor common on the market.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (9)
1. a kind of chemical industry distilling apparatus, including pedestal（1）, incubator（2）, distillation case（3）And heating dish（4）；The distillation
Case（3）Top is equipped with liquid-feeding tube（9）, the liquid-feeding tube（9）Top is equipped with capping（10）；The distillation case（3）Lower part is equipped with the
One outlet tube（5）, first outlet tube（5）Outlet end passes through incubator（2）Side wall is equipped with the first valve（6）；The distillation
Case（3）Side wall is equipped with spiral insulating tube（7）, the spiral insulating tube（7）Upper end is equipped with exhaust pipe（8）；It is characterized in that：It is described
Pedestal（1）Top is equipped with cooling cylinder（11）, the cooling cylinder（11）Inside it is contained with coolant liquid；The cooling cylinder（11）It is interior be equipped with it is cold
Solidifying pipe（13）, the distillation case（3）It is internally provided with blender（20）.
2. a kind of chemical industry distilling apparatus according to claim 1, it is characterised in that：The blender（20）Including motor
（21）With with motor（21）The agitating shaft that output shaft is connected（22）, agitating shaft（22）It is equipped with agitating paddle（23）.
3. a kind of chemical industry distilling apparatus according to claim 2, it is characterised in that：The agitating shaft（22）With motor（21）
Output shaft is to be threadedly coupled.
4. a kind of chemical industry distilling apparatus according to claim 2, it is characterised in that：The motor（21）Output shaft rotation side
To with agitating shaft（22）And motor（21）The threaded connection direction of output shaft is opposite.
5. a kind of chemical industry distilling apparatus according to claim 2, it is characterised in that：The agitating shaft（22）With distillation case
（3）Bottom is to be rotatably assorted.
6. a kind of chemical industry distilling apparatus according to claim 1, it is characterised in that：The distillation case（3）Side wall is equipped with
Temperature sensing device（24）.
7. a kind of chemical industry distilling apparatus according to claim 1, it is characterised in that：The exhaust pipe（8）Across distillation case
（3）Side wall is connected to distillation case（3）Inner top.
8. a kind of chemical industry distilling apparatus according to claim 1, it is characterised in that：The condenser pipe（13）Inlet and spiral shell
Revolve insulating tube（7）Lower end is connected to；The condenser pipe（13）Liquid feeding end passes through cooling cylinder（11）The side wall upper left corner and and cooling cylinder
（11）Side wall is fixedly connected, the condenser pipe（13）Outlet end passes through cooling cylinder（11）The side wall lower right corner and and cooling cylinder（11）Side
Wall is fixedly connected.
9. a kind of chemical industry distilling apparatus according to claim 1, it is characterised in that：The spiral insulating tube（7）Positioned at guarantor
Incubator（2）With distillation case（3）Between；The spiral insulating tube（7）Bottom end passes through incubator（2）Side wall.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810484190.7A CN108607228A (en) | 2018-05-19 | 2018-05-19 | A kind of chemical industry distilling apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810484190.7A CN108607228A (en) | 2018-05-19 | 2018-05-19 | A kind of chemical industry distilling apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108607228A true CN108607228A (en) | 2018-10-02 |
Family
ID=63663593
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810484190.7A Withdrawn CN108607228A (en) | 2018-05-19 | 2018-05-19 | A kind of chemical industry distilling apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108607228A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110068146A (en) * | 2019-04-28 | 2019-07-30 | 南通睿智超临界科技发展有限公司 | A kind of novel hot-water heating system for supercritical fluid extraction equipment |
| CN110791414A (en) * | 2019-11-09 | 2020-02-14 | 云南师范大学 | Biochemical sample extraction system and method |
| CN112774233A (en) * | 2020-12-30 | 2021-05-11 | 徐州砥研医药科技有限公司 | Distillation device for preparing pyridine-containing medical intermediate and working method thereof |
| CN114225458A (en) * | 2021-12-25 | 2022-03-25 | 东营威联化学有限公司 | Extractive distillation device for separating aromatic hydrocarbon |
-
2018
- 2018-05-19 CN CN201810484190.7A patent/CN108607228A/en not_active Withdrawn
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110068146A (en) * | 2019-04-28 | 2019-07-30 | 南通睿智超临界科技发展有限公司 | A kind of novel hot-water heating system for supercritical fluid extraction equipment |
| CN110791414A (en) * | 2019-11-09 | 2020-02-14 | 云南师范大学 | Biochemical sample extraction system and method |
| CN110791414B (en) * | 2019-11-09 | 2023-05-09 | 云南师范大学 | Biochemical sample extraction system and method thereof |
| CN112774233A (en) * | 2020-12-30 | 2021-05-11 | 徐州砥研医药科技有限公司 | Distillation device for preparing pyridine-containing medical intermediate and working method thereof |
| CN114225458A (en) * | 2021-12-25 | 2022-03-25 | 东营威联化学有限公司 | Extractive distillation device for separating aromatic hydrocarbon |
| CN114225458B (en) * | 2021-12-25 | 2022-12-09 | 东营威联化学有限公司 | Extractive distillation device for separating aromatic hydrocarbon |
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| Date | Code | Title | Description |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20181002 |