CN208553176U - A kind of chemical industry distilling apparatus - Google Patents
A kind of chemical industry distilling apparatus Download PDFInfo
- Publication number
- CN208553176U CN208553176U CN201820606537.6U CN201820606537U CN208553176U CN 208553176 U CN208553176 U CN 208553176U CN 201820606537 U CN201820606537 U CN 201820606537U CN 208553176 U CN208553176 U CN 208553176U
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- China
- Prior art keywords
- destilling tower
- agitating shaft
- condenser
- chemical industry
- downside
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a kind of chemical industry distilling apparatus, including destilling tower, distillery is equipped in destilling tower, agitating shaft is equipped in distillery, destilling tower upper end is equipped with sealing cover, sealing cover is equipped with feed opening, scum pipe is equipped on the downside of destilling tower, destilling tower upper left side is equipped with distillation cascade, distillation cascade is equipped with solenoid valve, condenser is connected on rear side of distillation cascade, heat exchanger tube is equipped in condenser, heat exchanger tube front end is connected to distillation cascade, drainage conduit is connected on rear side of heat exchanger tube, the beneficial effects of the utility model are: passing through setting air extractor and pressure sensor, it can be in distillery in stable negative pressure state, thereby reduce the boiling point of solution, reduce the energy consumption in distillation process, additionally it is equipped with temperature sensor and attemperator, the loss of heat can be effectively reduced, it is additionally provided with agitating device simultaneously, it can make anti- It answers more uniform rapid.
Description
Technical field
The utility model relates to a kind of distilling apparatus, specially a kind of chemical industry distilling apparatus belongs to distilling apparatus technology neck
Domain.
Background technique
Distillation is a kind of thermodynamic (al) separating technology, it is different using each component boiling point in mixing liquid or liquid-solid system,
Low boiling component is evaporated, then is condensed to separate the unit process of entire component, is two kinds of unit operations of evaporation and condensation
Joint.With other separation means, such as extraction, filtering for crystallizing compare, its advantage is that without the use of system components with
Outer other solvents in Chemical Manufacture, generally require to be removed raw material miscellaneous to guarantee that new impurity will not be introduced
Then matter just can be carried out chemical reaction, while can also be purified by distillation to production product, and these production processes are both needed to
It to use and arrive distilling apparatus.
The distilling apparatus used now often carries out heating distillation in normal pressure state and condenses again, but for high boiling
Substance generally requires to be heated to very high temperature, needs a large amount of energy, causes processing cost high, and distillation equipment is more now
Without Insulation, causes during distillation a large amount of heat to be dispersed into air and cause energy waste.
Utility model content
The purpose of this utility model is that solve the above-mentioned problems and provides a kind of chemical industry distilling apparatus.
The utility model is achieved through the following technical solutions above-mentioned purpose, a kind of chemical industry distilling apparatus, including destilling tower,
It is equipped with distillery in destilling tower, agitating shaft is equipped in distillery, destilling tower upper end is equipped with sealing cover, and sealing cover is equipped with charging
Mouth, destilling tower downside are equipped with scum pipe, and destilling tower upper left side is equipped with distillation cascade, and distillation cascade is equipped with solenoid valve, distillation cascade rear side
It is connected with condenser, is equipped with heat exchanger tube in condenser, heat exchanger tube front end is connected to distillation cascade, is connected with discharge on rear side of heat exchanger tube
Pipe；It is equipped with insulating layer on the outside of the destilling tower, supporting leg is equipped on the downside of destilling tower, is equipped with electric heater unit in destilling tower；It is described
Agitating shaft is equipped with multiple groups poking bar, and agitating shaft lower end is connected with stirring motor；The agitating shaft upper end is supported by agitating shaft
It is connect with distillation inner wall of tower, agitating shaft support downside is equipped with temperature sensor, and agitating shaft support downside is equipped with baroceptor；Institute
Destilling tower upper left side is stated equipped with exhaust tube, exhaust tube is equipped with air pump；Water inlet pipe, condenser upside are equipped on the downside of the condenser
Equipped with outlet pipe.
Further, the agitating shaft is hollow structure, and the side wall of agitating shaft is equipped with through-hole, and the side of through-hole is equipped with side
Plate, in rotation, side plate pours into liquid in through-hole.
Further, the side plate is formed by a quarter part of hemispherical shell.
Further, emargination face is equipped with groove on the inside of the cancave cambered surface of the side plate, and the groove is arranged in a vertical direction.
Further, the through-hole is along the axially staggered arrangement of agitating shaft.
The beneficial effects of the utility model are: can be place in distillery by setting air extractor and pressure sensor
In stable negative pressure state, the boiling point of solution is thereby reduced, reduces the energy consumption in distillation process, is additionally equipped with temperature
Sensor and attemperator are spent, the loss of heat can be effectively reduced, while being additionally provided with agitating device, reaction can be made more
Add uniformly rapidly.
Detailed description of the invention
Fig. 1 is the destilling tower cross-sectional view of the utility model.
Fig. 2 is the condenser cross-sectional view of the utility model.
In figure: 1, destilling tower, 2, distillery, 3, agitating shaft, 4, poking bar, 5, stirring motor, 6, agitating shaft support, 7, temperature
Spend sensor, 8, baroceptor, 9, sealing cover, 10, feed opening, 11, scum pipe, 12, supporting leg, 13, exhaust tube, 14, gas
Pump, 15, distillation cascade, 16, solenoid valve, 17, condenser, 18, heat exchanger tube, 19, drainage conduit, 20, water inlet pipe, 21, outlet pipe.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
It please refers to shown in Fig. 1-2, a kind of chemical industry distilling apparatus, including destilling tower 1, distillery 2 is equipped in destilling tower 1, steam
It evaporates and is equipped with agitating shaft 3 in room 2,1 upper end of destilling tower is equipped with sealing cover 9, and sealing cover 9 is equipped with feed opening 10, sets on the downside of destilling tower 1
There is scum pipe 11,1 upper left side of destilling tower is equipped with distillation cascade 15, and distillation cascade 15 is equipped with solenoid valve 16, connects on rear side of distillation cascade 15
There is condenser 17, is equipped with heat exchanger tube 18 in condenser 17,18 front end of heat exchanger tube is connected to distillation cascade 15, connects on rear side of heat exchanger tube 18
There is drainage conduit 19；It is equipped with insulating layer on the outside of the destilling tower 1, supporting leg 12 is equipped on the downside of destilling tower 1, is equipped with electricity in destilling tower 1
Heating device；The agitating shaft 3 is equipped with multiple groups poking bar 4, and 3 lower end of agitating shaft is connected with stirring motor 5；The agitating shaft 3
Upper end is connect by agitating shaft support 6 with 1 inner wall of destilling tower, and 6 downside of agitating shaft support is equipped with temperature sensor 7, agitating shaft branch
6 downside of support is equipped with baroceptor 8；1 upper left side of destilling tower is equipped with exhaust tube 13, and exhaust tube 13 is equipped with air pump 14；Institute
It states and is equipped with water inlet pipe 20 on the downside of condenser 17, be equipped with outlet pipe 21 on the upside of condenser 17.
Further, the agitating shaft 3 is hollow structure, and the side wall of agitating shaft 3 is equipped with through-hole, and the side of through-hole is equipped with
Side plate, in rotation, side plate pours into liquid in through-hole.For axle center when may be implemented in rotation by the side plate and through-hole of setting
The stirring at place, to improve the effect of stirring.
It further, is the effect for improving stirring, the side plate is formed by a quarter part of hemispherical shell, is used
The side plate of this kind of structure has preferable scraping effect to liquid, and liquid can be guaranteed by flowing in export-oriented through-hole.
Further, emargination face is equipped with groove on the inside of the cancave cambered surface of the side plate, and the groove is arranged in a vertical direction, recessed
Convex peak is formed between slot, vortex can be generated when liquid passes through side plate cancave cambered surface, to improve the effect of mixing.
Further, the through-hole is along the axially staggered arrangement of agitating shaft 3, liquid pass through through-hole enter after agitating shaft 3 with stir
The inner wall collision for mixing axis 3, to be conducive to the mixing of liquid.
When the utility model is used, mixed solution to be distilled is added in destilling tower 1 by feed opening 10, work as distillation
When suitable mixed solution being added in room 2, sealing cover 9 is closed, then booster air pump 14, will be steamed by air pump 14 and exhaust tube 13
It evaporates and extracts negative pressure state in room 2 out, feedback regulation is then carried out by baroceptor 8, and then can be steady by air pressure in distillery 2
It is scheduled near optimum response pressure, then starts the heating device in destilling tower 1, the solution in distillery 2 is heated, together
When carry out stablizing regulation by temperature sensor, and then temperature can accurately be controlled, then start stirring motor 5,
Solution in distillery 2 is stirred by poking bar 4, under suitable pressure and temperature, required substance starts in solution
When being evaporated, the solenoid valve 16 on distillation cascade 15 is opened, then steam begins through distillation cascade 15 and enters in condenser 17,
Cold water is passed through into condenser 17 by the water inlet pipe 20 on condenser 17 again, by heat exchanger tube 18 in cold water and condenser 17
Steam carry out heat exchange, and then steam can be made to be condensed, then by drainage conduit 19 will condense into the material of liquid into
Row discharge is collected, that is, completes positive distillation process.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and
And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in
All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting
Related claim.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (5)
1. a kind of chemical industry distilling apparatus, including destilling tower (1), it is characterised in that: be equipped with distillery (2) in destilling tower (1), distillation
Agitating shaft (3) are equipped in room (2), destilling tower (1) upper end is equipped with sealing cover (9), and sealing cover (9) is equipped with feed opening (10), steams
It evaporates and is equipped with scum pipe (11) on the downside of tower (1), destilling tower (1) upper left side is equipped with distillation cascade (15), and distillation cascade (15) is equipped with electromagnetism
Valve (16), distillation cascade (15) rear side are connected with condenser (17), heat exchanger tube (18) are equipped in condenser (17), before heat exchanger tube (18)
End is connected to distillation cascade (15), is connected with drainage conduit (19) on rear side of heat exchanger tube (18)；Heat preservation is equipped on the outside of the destilling tower (1)
Layer, destilling tower (1) downside are equipped with supporting leg (12), electric heater unit are equipped in destilling tower (1)；The agitating shaft (3) is equipped with
Multiple groups poking bar (4), agitating shaft (3) lower end are connected with stirring motor (5)；Agitating shaft (3) upper end is supported by agitating shaft
(6) it is connect with destilling tower (1) inner wall, agitating shaft supports and is equipped with temperature sensor (7) on the downside of (6), sets on the downside of agitating shaft support (6)
There are baroceptor (8)；Destilling tower (1) upper left side is equipped with exhaust tube (13), and exhaust tube (13) is equipped with air pump (14)；Institute
It states and is equipped with water inlet pipe (20) on the downside of condenser (17), be equipped with outlet pipe (21) on the upside of condenser (17).
2. a kind of chemical industry distilling apparatus according to claim 1, it is characterised in that: the agitating shaft (3) is hollow structure,
The side wall of agitating shaft (3) is equipped with through-hole, and the side of through-hole is equipped with side plate, and in rotation, side plate pours into liquid in through-hole.
3. a kind of chemical industry distilling apparatus according to claim 2, it is characterised in that: the side plate is by the four of hemispherical shell
/ a part is formed.
4. a kind of chemical industry distilling apparatus according to claim 3, it is characterised in that: emargination on the inside of the cancave cambered surface of the side plate
Face is equipped with groove, and the groove is arranged in a vertical direction.
5. a kind of chemical industry distilling apparatus according to claim 4, it is characterised in that: the through-hole is axial along agitating shaft (3)
Interlaced arrangement.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820606537.6U CN208553176U (en) | 2018-04-25 | 2018-04-25 | A kind of chemical industry distilling apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820606537.6U CN208553176U (en) | 2018-04-25 | 2018-04-25 | A kind of chemical industry distilling apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208553176U true CN208553176U (en) | 2019-03-01 |
Family
ID=65480145
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820606537.6U Expired - Fee Related CN208553176U (en) | 2018-04-25 | 2018-04-25 | A kind of chemical industry distilling apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208553176U (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110833700A (en) * | 2019-11-23 | 2020-02-25 | 湖南朝露生物科技有限公司 | Vacuum low-temperature distillation equipment |
| CN112774233A (en) * | 2020-12-30 | 2021-05-11 | 徐州砥研医药科技有限公司 | Distillation device for preparing pyridine-containing medical intermediate and working method thereof |
| CN113209658A (en) * | 2021-05-14 | 2021-08-06 | 贵州福正油桐发展有限公司 | Distillation equipment is used in tung oil tree processing |
| CN115261143A (en) * | 2022-09-01 | 2022-11-01 | 浙江希格骊特科技有限公司 | Natural spice extraction device with stirring function |
| CN115449431A (en) * | 2022-09-01 | 2022-12-09 | 浙江希格骊特科技有限公司 | Natural perfume extraction device |
-
2018
- 2018-04-25 CN CN201820606537.6U patent/CN208553176U/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110833700A (en) * | 2019-11-23 | 2020-02-25 | 湖南朝露生物科技有限公司 | Vacuum low-temperature distillation equipment |
| CN112774233A (en) * | 2020-12-30 | 2021-05-11 | 徐州砥研医药科技有限公司 | Distillation device for preparing pyridine-containing medical intermediate and working method thereof |
| CN113209658A (en) * | 2021-05-14 | 2021-08-06 | 贵州福正油桐发展有限公司 | Distillation equipment is used in tung oil tree processing |
| CN113209658B (en) * | 2021-05-14 | 2022-10-25 | 贵州福正油桐发展有限公司 | Distillation equipment is used in tung oil tree processing |
| CN115261143A (en) * | 2022-09-01 | 2022-11-01 | 浙江希格骊特科技有限公司 | Natural spice extraction device with stirring function |
| CN115449431A (en) * | 2022-09-01 | 2022-12-09 | 浙江希格骊特科技有限公司 | Natural perfume extraction device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190301 Termination date: 20200425 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |