CN110833700A

CN110833700A - Vacuum low-temperature distillation equipment

Info

Publication number: CN110833700A
Application number: CN201911160819.3A
Authority: CN
Inventors: 蒋文波; 高宁宁; 仁向飞; 王勋华
Original assignee: Hunan Chaolu Biotechnology Co Ltd
Current assignee: Hunan Chaolu Biotechnology Co Ltd
Priority date: 2019-11-23
Filing date: 2019-11-23
Publication date: 2020-02-25

Abstract

The invention discloses vacuum low-temperature distillation equipment which comprises a bottom plate, wherein a distillation kettle and a cooling box are fixed at the top of the bottom plate, a heating mechanism is arranged on the inner wall of the bottom of the distillation kettle, a feeding mechanism is fixed on the outer wall of the top of the distillation kettle, a motor is fixed at the central position of the outer wall of the top of the distillation kettle, an output shaft of the motor penetrates through the inner wall of the top of the distillation kettle and is fixed with a rotating shaft, a plurality of stirring rods are fixed on the outer wall of the rotating shaft, the stirring rods are S-shaped, a communicating pipe is fixedly inserted between the top end of the outer wall of one side of the distillation kettle and the cooling box, one end of the communicating pipe is connected with a pipe in turn, the pipe is positioned in the cooling box, a flow guide mechanism is fixed at the bottom of the pipe, the flow guide. The invention can stir the raw materials in the distillation kettle to generate turbulent flow, improve the heating uniformity, promote the evaporation of the raw materials and further improve the distillation efficiency.

Description

Vacuum low-temperature distillation equipment

Technical Field

The invention relates to the technical field of distillation equipment, in particular to vacuum low-temperature distillation equipment.

Background

Distillation is a thermodynamic separation process that utilizes the difference in boiling points of components in a mixed liquid or liquid-solid system to vaporize lower boiling components and recondense to separate the entire component, a unit operation that combines the two unit operations of evaporation and condensation. Compared with other separation means, such as extraction, filtration crystallization and the like, the method has the advantage that other solvents except system components are not required, so that new impurities are not introduced.

Through retrieval, the patent with the Chinese patent authorization number of CN207891321U discloses equipment for producing floral hydrolat by low-temperature distillation, which comprises a distillation kettle, a condenser pipe, a liquid storage tank, a vacuum pump, a condenser and a heat exchanger, wherein the equipment is connected by pipelines, and the pipelines are provided with valves; wherein, the distillation kettle passes through the condenser pipe and connects the liquid storage pot, and the liquid storage pot is connected the vacuum pump and then is connected the condenser, and the coolant in the heat exchanger communicates to condenser and condenser pipe rethread return line flow back to in the heat exchanger in proper order through the input tube. The distillation still in the above patent has the following disadvantages: the distillation efficiency is low.

Disclosure of Invention

The invention aims to solve the defects in the prior art and provides vacuum low-temperature distillation equipment.

In order to achieve the purpose, the invention adopts the following technical scheme:

the utility model provides a vacuum cryogenic distillation equipment, includes the bottom plate, the bottom plate top is fixed with stills and cooler bin, stills bottom inner wall is equipped with heating mechanism, and stills top outer wall is fixed with feed mechanism, and stills top outer wall central point puts and is fixed with the motor, and the output shaft of motor passes stills top inner wall and is fixed with the pivot, and the pivot outer wall is fixed with a plurality of puddlers, and the puddler is the S type, it has communicating pipe to fix between stills one side outer wall top and the cooler bin to peg graft, and communicating pipe one end is connected with the pipe that returns, and the pipe that returns is located the cooler bin, it is fixed with water conservancy diversion mechanism to return the pipe bottom, and water conservancy diversion mechanism intercommunication has the collecting box, and collecting box top outer wall one side is fixed with the vacuum pump, the inlet end.

Furthermore, the flow guide mechanism comprises a connecting pipe, a hose is fixedly arranged at the bottom end of the connecting pipe after penetrating through five hundred parts of the bottom of the cooling box, and the hose is fixedly communicated with the collecting box.

Furthermore, feed mechanism includes the inlet pipe, and the inlet pipe top is fixed with the apron, and still bottom outer wall one side is fixed to peg graft and is had the unloading pipe.

Furthermore, four corners of the outer wall of the bottom of the distillation kettle are all fixed with loop bars, the bottom ends of the loop bars are sleeved with sleeves, springs are arranged in the sleeves, and the bottom ends of the sleeves are fixedly connected with the bottom plate.

Furthermore, a water inlet pipe and a water outlet pipe are fixedly inserted in the cooling box respectively, and supporting legs are fixed at four corners of the outer wall of the bottom of the cooling box.

Furthermore, a discharge pipe is fixedly inserted into the outer wall of one side of the collecting box.

Further, the outer wall of one side of the rotating shaft is further fixed with a fixing rod, one end, far away from the rotating shaft, of the fixing rod is fixed with a scraping strip, and the scraping strip is attached to the inner wall of the distillation kettle.

The invention has the beneficial effects that:

1. can heat the raw materials through stills's setting, gaseous condensation work can be enough realized to the inside cooling water of cooperation return venturi tube and cooler bin, the condensation liquid is from the leading-in collecting box of hose, accomplish distillation work, wherein need utilize the vacuum pump to take still return venturi tube and the inside air of collecting box out before distillation work, make the inside vacuum state that forms of stills, improve the evaporation rate of heating during operation, at this moment, the puddler stirs the turbulent flow to the interior raw materials of stills under the drive of motor and pivot, improve the heating degree of consistency, and promote the raw materials evaporation, further improve distillation efficiency.

2. Setting up through sleeve pipe, loop bar and spring can play the supporting role to stills, and the spring can play buffering shock attenuation effect to stills, further improves the stability of distillation work.

3. Can rotate with the puddler synchronization under the drive effect of motor and pivot through the setting of scraping strip and dead lever, scrape the strip and can strike off the raw materials that the stills inner wall adhered, play the effect of scraping when carrying out the blowdown cleaning work inside the stills, increased the convenience of device cleaning work.

Drawings

FIG. 1 is a schematic sectional view of a vacuum cryogenic distillation apparatus according to example 1 of the present invention;

FIG. 2 is a schematic perspective view of a vacuum cryogenic distillation apparatus according to example 1 of the present invention;

FIG. 3 is a schematic sectional view of a distillation still of embodiment 2 of a vacuum cryogenic distillation apparatus according to the present invention.

In the figure: the device comprises a distillation still 1, a rotating shaft 2, a stirring rod 3, a motor 4, a cover plate 5, a feeding pipe 6, a communicating pipe 7, a return pipe 8, a cooling box 9, a collecting box 10, an air guide pipe 11, a vacuum pump 12, a discharge pipe 13, a sleeve pipe 14, a sleeve rod 15, a spring 16, a connecting pipe 17, a hose 18, a discharge pipe 19, a bottom plate 20, a fixing rod 21 and a scraping strip 22.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.

Examples of which are illustrated in the accompanying drawings, wherein like reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are exemplary only for the purpose of explaining the present patent and are not to be construed as limiting the present patent.

Example 1

Referring to fig. 1 and 2, the vacuum low temperature distillation equipment comprises a bottom plate 20, a distillation still 1 and a cooling tank 9 are fixed on the top of the bottom plate 20, a heating mechanism is arranged on the inner wall of the bottom of the distillation still 1, and 1 top outer wall of stills is fixed with feed mechanism, 1 top outer wall central point of stills puts and is fixed with motor 4, the output shaft of motor 4 passes 1 top inner wall of stills and is fixed with

pivot

2, 2 outer wall of pivot are fixed with a plurality of puddler 3, puddler 3 is the S type, it has communicating pipe 7 to be fixed to peg graft between 1 one side outer wall top of stills and the

cooler bin

9, 7 one end of communicating pipe is connected with back venturi tube 8, it is located the cooler bin 9 to return

venturi tube

8, 8 bottom mounting of back venturi tube has water conservancy diversion mechanism, water conservancy diversion mechanism intercommunication has collecting

box

10, 10 top outer wall one side of collecting box is fixed with vacuum pump 12, vacuum pump 12' S inlet end is fixed with air duct 11, air duct 11.

Flow guide mechanism includes connecting pipe 17, connecting pipe 17 bottom is passed and is fixed with hose 18 bottom 9 bottom five hundred, hose 18 and the fixed intercommunication of collecting box 10, feed mechanism includes inlet pipe 6, 6 tops of inlet pipe are fixed with apron 5, 1 bottom outer wall one side of stills is fixed with unloading pipe 19 of pegging graft, four corners of 1 bottom outer wall of stills all are fixed with loop bar 15, sleeve 14 has been cup jointed to loop bar 15 bottom, be equipped with spring 16 in the

sleeve

14, 14 bottom of sleeve and 20 fixed connection of bottom plate, it has inlet tube and outlet pipe to peg graft respectively on the cooling box 9, and four corners of cooling box 9 bottom outer wall all are fixed with the supporting leg, the fixed unloading pipe 13 of pegging graft of collecting box 10 one side outer wall.

The working principle of the embodiment is as follows: the raw materials are put into the distillation still 1 from the feeding pipe 6, the cover plate 6 is covered, wherein before the distillation operation, the vacuum pump 12 is needed to pump out the air in the return pipe 8 and the collecting box 10 of the distillation still 1, so that the interior of the distillation still 1 is in a vacuum state, the evaporation rate during the heating operation is improved, at the moment, the stirring rod 3 is driven by the motor 4 and the rotating shaft 2 to stir the raw materials in the distillation still 1, the heating uniformity is improved, the evaporation of the raw materials is promoted, the distillation efficiency is further improved, the distillation still 1 can heat the raw materials, the condensation operation of gas can be realized by matching with the cooling water in the return pipe 8 and the cooling box 9, the condensed liquid is guided into the collecting box 10 from the hose 18 to complete the distillation operation, the sleeve 14, the sleeve 15 and the spring 16 can play a supporting role in the distillation still 1, and the spring 16 can play a buffering and damping, further improving the stability of the distillation operation.

Example 2

Referring to fig. 3, a vacuum cryogenic distillation apparatus, which is different from embodiment 1 in that a fixing rod 21 is further fixed on an outer wall of one side of a rotating shaft 2, a scraping strip 22 is fixed on one end of the fixing rod 21 away from the rotating shaft 2, and the scraping strip 22 is attached to an inner wall of a distillation still 1.

The working principle of the embodiment is as follows: scrape strip 22 and dead lever 21 and can rotate with puddler 3 synchronous under the drive effect of motor 4 and pivot 2, scrape strip 22 and can strike off the raw materials that stills 1 inner wall was adhered, play the effect of scraping when carrying out the blowdown cleaning work in stills 1 inside, increased the convenience of device cleaning work.

In the description of this patent, it is to be understood that the terms "coaxial," "bottom," "one end," "top," "middle," "other end," "upper," "one side," "top," "inner," "front," "center," "two ends," and the like are used in the orientations and positional relationships indicated in the drawings for convenience in describing the patent and for simplicity in description, and are not intended to indicate or imply that the referenced device or element must have a particular orientation, be constructed and operated in a particular orientation, and are not to be considered limiting of the patent.

In this patent, unless expressly stated or limited otherwise, the terms "mounted," "disposed," "connected," "secured," "screwed" and the like are to be construed broadly and can, for example, be fixedly connected, detachably connected, or integrally formed; can be mechanically or electrically connected; they may be directly connected or indirectly connected through an intermediate, or they may be connected internally or in an interactive relationship with each other, and unless otherwise specifically limited, the specific meaning of the above terms in this patent will be understood by those skilled in the art according to the specific circumstances.

The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims

1. A vacuum low-temperature distillation device comprises a bottom plate (20), wherein a distillation kettle (1) and a cooling box (9) are fixed at the top of the bottom plate (20), and is characterized in that a heating mechanism is arranged on the inner wall of the bottom of the distillation kettle (1), a feeding mechanism is fixed on the outer wall of the top of the distillation kettle (1), a motor (4) is fixed at the central position of the outer wall of the top of the distillation kettle (1), an output shaft of the motor (4) penetrates through the inner wall of the top of the distillation kettle (1) and is fixed with a rotating shaft (2), a plurality of stirring rods (3) are fixed on the outer wall of the rotating shaft (2), the stirring rods (3) are S-shaped, a communicating pipe (7) is fixedly inserted between the top end of the outer wall of one side of the distillation kettle (1) and the cooling box (9), one end of the communicating pipe (7) is connected with a return pipe (8), the return, the flow guide mechanism is communicated with a collecting box (10), a vacuum pump (12) is fixed on one side of the outer wall of the top of the collecting box (10), an air guide pipe (11) is fixed at the air inlet end of the vacuum pump (12), and the air guide pipe (11) is inserted into the collecting box (10).

2. A vacuum cryogenic distillation apparatus according to claim 1, characterised in that the diversion mechanism comprises a connecting pipe (17), a hose (18) is fixed at the bottom end of the connecting pipe (17) through five hundred of the bottom of the cooling tank (9), and the hose (18) is fixedly communicated with the collection tank (10).

3. The vacuum cryogenic distillation equipment as claimed in claim 2, wherein the feeding mechanism comprises a feeding pipe (6), a cover plate (5) is fixed at the top end of the feeding pipe (6), and a discharging pipe (19) is fixed and inserted at one side of the outer wall of the bottom of the distillation still (1).

4. The vacuum cryogenic distillation equipment according to claim 1, wherein sleeve rods (15) are fixed at four corners of the outer wall of the bottom of the distillation kettle (1), a sleeve (14) is sleeved at the bottom end of each sleeve rod (15), a spring (16) is arranged in each sleeve (14), and the bottom end of each sleeve (14) is fixedly connected with the bottom plate (20).

5. A vacuum cryogenic distillation apparatus according to claim 4, wherein the cooling tank (9) is fixedly inserted with a water inlet pipe and a water outlet pipe, and the cooling tank (9) is fixed with support legs at four corners of the outer wall of the bottom.

6. A vacuum cryogenic distillation apparatus according to any one of claims 1 to 5, characterised in that a discharge pipe (13) is fixedly inserted into the outer wall of one side of the collection box (10).

7. The vacuum cryogenic distillation equipment as claimed in claim 1, wherein a fixing rod (21) is further fixed on the outer wall of one side of the rotating shaft (2), a scraping bar (22) is fixed on one end of the fixing rod (21) far away from the rotating shaft (2), and the scraping bar (22) is attached to the inner wall of the distillation kettle (1).