CN214915963U

CN214915963U - Graphene production equipment

Info

Publication number: CN214915963U
Application number: CN202121624611.5U
Authority: CN
Inventors: 李猛; 于名讯; 于一夫; 刘剑; 段丽丽; 牛娜; 张忠霞; 董帅
Original assignee: Shandong Haimai New Material Co ltd
Current assignee: Shandong Haimai New Material Co ltd
Priority date: 2021-07-16
Filing date: 2021-07-16
Publication date: 2021-11-30
Anticipated expiration: 2031-07-16

Abstract

The utility model discloses a graphite alkene production facility relates to graphite alkene production facility field that is correlated with. The utility model discloses a box, the top fixed mounting of box has a jar body, the top fixed mounting of the jar body has driving motor, the inner chamber roof fixed mounting of the jar body has the mounting box, driving motor's bottom output stretches into in the driving gear and fixed mounting has the driving gear, the inner chamber roof of the jar body rotates and is connected with two pivots, the pivot is located all side fixed mounting of mounting box and has driven gear, driven gear meshes with the driving gear mutually, two pivots are located the inside all side fixed mounting of box and have a plurality of stirring leaves, and the stirring leaf of two pivots is the crisscross distribution. The utility model discloses a driving gear and driven gear can drive two pivots and rotate simultaneously, and the stirring effect of the mixing material in the multiplicable box of stirring leaf staggered distribution makes the reaction more abundant, is provided with a dispersion section of thick bamboo, but mixing material evenly distributed can obtain comparatively level and smooth graphite alkene material on the filter screen.

Description

Graphene production equipment

Technical Field

The utility model belongs to the technical field of the relevant production facility of graphite alkene, especially, relate to graphite alkene production facility.

Background

The graphene has excellent optical, electrical and mechanical properties, has important application prospects in the aspects of materials science, micro-nano processing, energy, biomedicine, drug delivery and the like, and is considered to be a revolutionary material in the future.

In the production of graphene materials, the Hummers method is commonly used for preparation of graphene materials due to relatively good timeliness and safety, but some existing production devices are poor in stirring effect of mixed materials, so that insufficient reaction is caused, the reaction efficiency is influenced, the yield is influenced, and the use requirements are not met.

In order to solve the problem, the utility model provides a graphite alkene production facility.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a graphite alkene production facility solves some current apparatus for producing not good to the stirring effect of mixing material, causes the reaction insufficient, influences the efficiency of reaction and influences the problem of productivity simultaneously.

In order to solve the technical problem, the utility model discloses a realize through following technical scheme:

the utility model relates to a graphene production device, which comprises a box body, wherein a tank body is fixedly arranged at the top of the box body, a driving motor is fixedly arranged at the top of the tank body, a mounting box is fixedly arranged on the top wall of an inner cavity of the tank body, the bottom output end of the driving motor extends into a driving gear and is fixedly provided with the driving gear, the top wall of the inner cavity of the tank body is rotatably connected with two rotating shafts, a driven gear is fixedly arranged on the peripheral side of the rotating shaft in the mounting box and is meshed with the driving gear, a plurality of stirring blades are fixedly arranged on the peripheral side of the rotating shaft in the box body, the stirring blades of the two rotating shafts are distributed in a staggered manner, the driving motor can drive the two rotating shafts to rotate simultaneously through the driving gear and the driven gear when rotating, the stirring effect of mixed materials in the box body can be increased due to the staggered distribution of the stirring blades, an ultrasonic vibrator is fixedly arranged on the inner bottom wall of the tank body, the inside of box from top to bottom installs dispersion section of thick bamboo, filter screen and dump bin in proper order.

Preferably, an interlayer is arranged in the side wall of the tank body, heating oil is filled in the interlayer, a heating pipe is fixedly embedded in the bottom wall of the inner cavity of the tank body and located at the bottom of the heating oil, and the heating pipe can perform oil bath heating on the mixed material.

Preferably, the inner chamber bottom of the jar body is the toper structure that contracts gradually from top to bottom, top one side of the jar body is provided with the feed inlet, be provided with electric control valve between the jar body and the box, after the mixing material reaction finishes, open electric control valve, the mixing material can fall into in the box, a dispersion section of thick bamboo and the interior back of the body wall fixed connection of box, a plurality of round holes have been seted up to the lower surface of a dispersion section of thick bamboo, and the mixture falls to a dispersion section of thick bamboo along electric control valve in, but through round hole evenly distributed on the filter screen.

Preferably, the preceding activity of box articulates there is the chamber door, the equal fixed mounting in two inside walls of box has the support bar, the equal fixed mounting in both sides of filter screen has the slider, the filter screen passes through slider sliding connection at the top of support bar, and the support bar provides support and location for the filter screen, treats that mixed material evenly distributed when on the filter screen, can take out the filter screen from the box in after opening the chamber door, the activity of waste bin is pegged graft in the inner chamber bottom of box, and the waste bin is used for the collection to waste water waste material, can take out the waste bin, conveniently washs the maintenance.

The utility model discloses following beneficial effect has:

the utility model discloses be provided with the driving gear, pivot and driven gear, add the jar body with graphite oxide through the feed inlet, the ultrasonic wave oscillator can make solution homodisperse, after ammonia and reductant solution were injected into to the feed inlet, driving motor rotates accessible driving gear and driven gear and can drive two pivots and rotate simultaneously, but stirring leaf staggered distribution multiplicable box internal mixing material's stirring effect, it is more abundant to make the reaction, and be provided with a dispersion section of thick bamboo, but mixing material along automatically controlled valve whereabouts evenly distributed on the filter screen, thereby obtain comparatively level and smooth graphite alkene material.

Of course, it is not necessary for any particular product to achieve all of the above-described advantages at the same time.

Drawings

In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art that other drawings can be obtained according to these drawings without creative efforts.

Fig. 1 is a schematic view of the overall structure of the present invention;

fig. 2 is a top view of the overall structure of the present invention;

fig. 3 is a schematic cross-sectional view of a-a in fig. 2 according to the present invention;

fig. 4 is an enlarged view of a point a in fig. 3 according to the present invention;

fig. 5 is an enlarged view of the position B in fig. 3 according to the present invention.

In the drawings, the components represented by the respective reference numerals are listed below: 1. a box body; 11. a box door; 2. a tank body; 21. a feed inlet; 22. an electrically controlled valve; 23. an ultrasonic vibrator; 24. heating a tube; 25. heating the oil; 26. mounting a box; 3. a drive motor; 31. a driving gear; 4. a rotating shaft; 41. a driven gear; 42. stirring blades; 5. a dispersing cylinder; 501. a circular hole; 6. filtering with a screen; 61. a slider; 62. a supporting strip; 7. a waste bin.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts belong to the protection scope of the present invention.

In the description of the present invention, it is to be understood that the terms "upper", "middle", "outer", "inner", and the like, indicate positional or positional relationships, are merely for convenience in describing the present invention and simplifying the description, and do not indicate or imply that the referenced components or elements must have a particular orientation, be constructed and operated in a particular orientation, and therefore should not be construed as limiting the present invention.

Referring to fig. 1-5, the utility model relates to a graphene production apparatus, which comprises a box body 1, a tank body 2 is fixedly installed on the top of the box body 1, a driving motor 3 is fixedly installed on the top of the tank body 2, a mounting box 26 is fixedly installed on the top wall of the inner cavity of the tank body 2, the bottom output end of the driving motor 3 extends into the driving gear 31 and is fixedly installed with the driving gear 31, the top wall of the inner cavity of the tank body 2 is rotatably connected with two rotating shafts 4, the peripheral side of the rotating shaft 4 in the mounting box 26 is fixedly installed with a driven gear 41, the driven gear 41 is engaged with the driving gear 31, the peripheral side of the two rotating shafts 4 in the box body 1 is fixedly installed with a plurality of stirring blades 42, the stirring blades 42 of the two rotating shafts 4 are distributed in a staggered manner, the driving motor 3 can drive the two rotating shafts 4 to rotate simultaneously through the driving gear 31 and the driven gear 41, the stirring blades 42 are distributed in a staggered manner to increase the stirring effect of the mixed materials in the box body 1, the inner bottom wall of the tank body 2 is fixedly provided with an ultrasonic vibrator 23, and the inside of the tank body 1 is sequentially provided with a dispersion cylinder 5, a filter screen 6 and a waste tank 7 from top to bottom.

An interlayer is arranged in the side wall of the tank body 2, heating oil 25 is filled in the interlayer, a heating pipe 24 is fixedly embedded in the bottom wall of the inner cavity of the tank body 2, the heating pipe 24 is positioned at the bottom of the heating oil 25, and the heating pipe 24 can heat the mixed material in an oil bath.

The inner chamber bottom of the jar body 2 is the toper structure that contracts gradually from top to bottom, top one side of the jar body 2 is provided with feed inlet 21, be provided with electric control valve 22 between the jar body 2 and the box 1, after the mixing material reaction finishes, open electric control valve 22, the mixing material can fall into in the box 1, dispersion section of thick bamboo 5 and box 1's interior back wall fixed connection, a plurality of round holes 501 have been seted up to the lower surface of dispersion section of thick bamboo 5, the mixture falls to dispersion section of thick bamboo 5 in along electric control valve 22, but through round hole 501 evenly distributed on filter screen 6.

The preceding activity of box 1 articulates there is chamber door 11, the equal fixed mounting in two inside walls of box 1 has support bar 62, the equal fixed mounting in both sides of filter screen 6 has slider 61, filter screen 6 passes through slider 61 sliding connection at the top of support bar 62, support bar 62 provides support and location for filter screen 6, treat when the misce bene material evenly distributed is on filter screen 6, can take out filter screen 6 from box 1 after

opening chamber door

11, 7 activities of waste bin are pegged graft in the inner chamber bottom of box 1, waste bin 7 is used for the collection to waste water waste, can take out waste bin 7, the convenient washing is maintained.

The embodiment is a use method of graphene production equipment, which comprises the following steps:

as shown in fig. 1-5, an external power supply is connected, graphite oxide is added into the tank body 2 through the feed port 21, the solution is uniformly dispersed through the ultrasonic vibrator 23, ammonia water and reducing agent solution are injected into the feed port 21, the stirring motor driving motor 3 drives the rotating shaft 4 to rotate and rotate the mixed material, the driving motor 3 is JS-50 in model, the heating pipe 24 can carry out oil bath heating on the mixed material, after the mixed material is reacted, the electric control valve 22 is opened, the mixture falls down along the electric control valve 22 and is uniformly distributed on the filter screen 6 through the dispersing cylinder 5, the filter screen 6 can be taken out, washed and dried, and thus the graphene material is obtained.

In the description herein, references to the description of "one embodiment," "an example," "a specific example," etc., mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

The preferred embodiments of the present invention disclosed above are intended only to help illustrate the present invention. The preferred embodiments are not intended to be exhaustive or to limit the invention to the precise embodiments disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and its practical applications, to thereby enable others skilled in the art to best understand the invention for and utilize the invention. The present invention is limited only by the claims and their full scope and equivalents.

Claims

1. Graphene production equipment comprises a box body (1) and is characterized in that the top fixed mounting of the box body (1) is provided with a tank body (2), the top fixed mounting of the tank body (2) is provided with a driving motor (3), the inner cavity top wall fixed mounting of the tank body (2) is provided with a mounting box (26), the bottom output end of the driving motor (3) extends into a driving gear (31) and is provided with a driving gear (31), the inner cavity top wall of the tank body (2) is rotatably connected with two rotating shafts (4), the circumferential side fixed mounting of the rotating shafts (4) in the mounting box (26) is provided with a driven gear (41), the driven gear (41) is meshed with the driving gear (31), the two circumferential side fixed mounting of the rotating shafts (4) in the box body (1) is provided with a plurality of stirring blades (42), and the stirring blades (42) of the rotating shafts (4) are in staggered distribution, the inner bottom wall fixed mounting of the tank body (2) is provided with an ultrasonic vibrator (23), and a dispersion cylinder (5), a filter screen (6) and a waste box (7) are sequentially arranged in the tank body (1).

2. The graphene production equipment according to claim 1, wherein the bottom of the inner cavity of the tank body (2) is of a tapered structure which gradually shrinks inwards from top to bottom, a feed inlet (21) is formed in one side of the top of the tank body (2), and an electric control valve (22) is arranged between the tank body (2) and the box body (1).

3. The graphene production equipment according to claim 1, wherein an interlayer is arranged in the side wall of the tank body (2), heating oil (25) is filled in the interlayer, a heating pipe (24) is fixedly embedded in the bottom wall of the inner cavity of the tank body (2), and the heating pipe (24) is located at the bottom of the heating oil (25).

4. The graphene production equipment according to claim 1, wherein the dispersing cylinder (5) is fixedly connected with the inner back wall of the box body (1), and a plurality of uniformly distributed round holes (501) are formed in the lower surface of the dispersing cylinder (5).

5. The graphene production equipment according to claim 1, wherein a support bar (62) is fixedly mounted on each of two inner side walls of the box body (1), sliders (61) are fixedly mounted on two sides of the filter screen (6), and the filter screen (6) is slidably connected to the tops of the support bars (62) through the sliders (61).

6. Graphene production apparatus according to claim 1, wherein the front face of the box (1) is movably hinged with a box door (11).

7. The graphene production apparatus according to claim 1, wherein the waste bin (7) is movably inserted into the bottom of the inner cavity of the box body (1).