CN211169857U

CN211169857U - A apparatus for producing graphite alkene material

Info

Publication number: CN211169857U
Application number: CN201922270380.1U
Authority: CN
Inventors: 孙四清; 赵爱民; 周爱国; 高庆凯; 张卫国; 刘德苓; 刘栋; 宋允华; 高岭; 王广哲
Original assignee: Lianyungang Linhai New Material Co ltd
Current assignee: Lianyungang Linhai New Material Co ltd
Priority date: 2019-12-17
Filing date: 2019-12-17
Publication date: 2020-08-04
Anticipated expiration: 2029-12-17

Abstract

The utility model discloses a production device for producing graphene materials, the on-line screen storage device comprises a base, the top left side of base is connected with the casing, the top right side of base is connected with the grudging post, the inner chamber bottom of casing is connected with the heating pipe, the inner chamber top of casing is connected with the inner tank, inner tank right side wall bottom intercommunication has the discharging pipe, the ultrasonic vibrator is installed to the inner chamber bottom of inner tank, the top of casing has the apron through bolted connection, the top left side of apron is connected with agitator motor, agitator motor's bottom power take off end is connected with the (mixing) shaft, the one end that the (mixing) shaft stretches into the inner tank is connected with the stirring leaf, the top of casing runs through has first dog-house, the top right side of; the utility model has the advantages of reasonable design, easy operation collects dispersion, mixes, stirring, heating, filtration, washing, stoving in an organic whole, is favorable to the production and processing of graphite alkene material, has saved spatial layout, has improved production efficiency.

Description

A apparatus for producing graphite alkene material

Technical Field

The utility model relates to a relevant production facility technical field of graphite alkene especially relates to a apparatus for producing graphite alkene material.

Background

Graphene is a polymer made of carbon atoms in sp²The hybrid tracks form a hexagonal honeycomb lattice two-dimensional carbon nanomaterial. The graphene has excellent optical, electrical and mechanical properties, has important application prospects in the aspects of materials science, micro-nano processing, energy, biomedicine, drug delivery and the like, and is considered to be a revolutionary material in the future. With the gradual breakthrough of mass production and large-size problems, the industrial application of graphene is accelerating, and the commercial application in the fields of mobile devices, aerospace and new energy batteries is gradually increased based on the existing research resultsMuch more.

In the production of graphene materials, the Hummers method is commonly used due to relatively good timeliness and safety, but the existing production device is complex in process, each step is separated from each other, the operation is complex, the consumed time is long, and the production efficiency is low.

SUMMERY OF THE UTILITY MODEL

The utility model provides a apparatus for producing graphite alkene material, easy operation has improved production efficiency. In order to realize the technical purpose, the technical effect is achieved, and the utility model discloses a realize through following technical scheme.

A production device for producing graphene materials comprises a base, wherein the left side of the top of the base is connected with a shell, the right side of the top of the base is connected with a vertical frame, supporting legs are connected with four corners of the bottom of the base, the bottom of an inner cavity of the shell is connected with a heating pipe, the top of the inner cavity of the shell is connected with an inner tank, the bottom of the right side wall of the inner tank is communicated with a discharging pipe, one end, extending out of the shell, of the discharging pipe is provided with a first electric control valve, the bottom of the inner cavity of the inner tank is provided with an ultrasonic vibrator, the top of the shell is connected with a cover plate through a bolt, the left side of the top of the cover plate is connected with a stirring motor, the bottom power output end of the stirring motor is connected with a stirring shaft, one end, extending into the inner tank, the top right side of casing is connected with the water tank, the bottom right side of apron is connected with the shower head.

Preferably, in a apparatus for producing graphite alkene material, the left side wall bottom of grudging post is connected with the dump bin, the right side wall top of grudging post is connected with the drying-machine, the front end middle part of grudging post rotates and is connected with the damping pivot, damping pivot lateral wall is connected with the filter screen, the filter screen is located the discharging pipe below.

Preferably, in a production device for producing graphite alkene material, seted up left water storage chamber and right water storage chamber in the water tank, the intercommunication has the second to throw material pipe between left water storage chamber and the inner tank, the intercommunication has the honeycomb duct between right water storage chamber and the shower head, all install the second automatically controlled valve on second throw material pipe and the honeycomb duct.

Preferably, in a production device for producing graphene materials, the upper portion and the lower portion of the shell are respectively connected with an oil inlet pipe and an oil outlet pipe, and the oil outlet pipe is provided with a control valve.

Preferably, in a production device for producing graphene materials, the outer side wall of the shell is connected with a thermal insulation coating.

Preferably, in the production device for producing graphene materials, the waste bin is located right below the spray header.

The utility model has the advantages that:

1. the utility model has reasonable structural design and simple operation, integrates dispersion, mixing, stirring, heating, filtering, washing and drying, is beneficial to the production and processing of graphene materials, saves the spatial layout and improves the production efficiency;

2. the device is convenient to feed, can stir the mixed material through the stirring blades, enables the mixed material to be uniformly heated through oil bath heating, is safe and stable, and is beneficial to reaction and output of graphene materials;

3. the cover plate in the device can be detachably connected through the bolt, the device assembly is convenient to clean and replace, the service life of the device is prolonged, the safety protection performance is improved through the heat insulation coating, and the device is more practical.

Drawings

In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art that other drawings can be obtained according to these drawings without creative efforts.

Fig. 1 is a schematic view of the overall structure of the present invention;

fig. 2 is a schematic structural view of the middle standing frame of the present invention;

fig. 3 is a schematic structural diagram of the middle water tank of the present invention.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts belong to the protection scope of the present invention.

Referring to fig. 1-3, the present embodiment is a production apparatus for producing graphene materials, including a base 1, a housing 2 is connected to the left side of the top of the base 1, a vertical frame 3 is connected to the right side of the top of the base 1, support legs 4 are connected to four corners of the bottom of the base 1, a heating pipe 5 is connected to the bottom of an inner cavity of the housing 2, an inner tank 6 is connected to the top of the inner cavity of the housing 2, a discharging pipe 7 is communicated to the bottom of the right side wall of the inner tank 6, a first electric control valve 8 is installed at one end of the discharging pipe 7 extending out of the housing 2, an ultrasonic vibrator 9 is installed at the bottom of the inner cavity of the inner tank 6, a cover plate 10 is connected to the top of the housing 2 through a bolt, a stirring motor 11 is connected to the left side of the top of the cover plate 10, a stirring shaft 12 is connected to the, the lower end of the first feeding pipe 14 extends into the inner tank 6, the right side of the top of the shell 2 is connected with a water tank 15, and the right side of the bottom of the cover plate 10 is connected with a spray header 16.

The left side wall bottom of grudging post 3 is connected with dump bin 301, and the right side wall top of grudging post 3 is connected with drying-machine 302, and the front end middle part of grudging post 3 rotates and is connected with damping pivot 303, and damping pivot 303 lateral wall is connected with filter screen 304, and filter screen 304 is located discharging pipe 7 below.

A left water storage cavity 151 and a right water storage cavity 152 are formed in the water tank 15, a second feeding pipe 153 is communicated between the left water storage cavity 151 and the inner tank 6, a guide pipe 154 is communicated between the right water storage cavity 152 and the spray header 16, and a second electric control valve 155 is mounted on each of the second feeding pipe 153 and the guide pipe 154, so that water flow output is controlled conveniently.

The upper part and the lower part of the shell 2 are respectively connected with an oil inlet pipe 201 and an oil outlet pipe 202, and the oil outlet pipe 202 is provided with a control valve for facilitating the oil to enter and exit.

The outer side wall of the shell 2 is connected with a heat insulation coating, the protection effect is good, and accidental contact scalding of operators is avoided.

The waste tank 301 is located under the spray header 16, which facilitates waste liquid collection.

The utility model discloses a concrete implementation way does:

when the device is used, an external power supply is connected, the base 1 is fixed through the supporting legs 4, graphite oxide is added into the inner tank 6 through the first feeding pipe 14, water is added into the inner tank 6 through the second feeding pipe 153 in the left water storage cavity 151, the solution is uniformly dispersed through the ultrasonic vibrator 9, ammonia water and reducing agent solution are injected into the first feeding pipe 14, the stirring shaft 12 is driven to rotate through the stirring motor 11, the stirring blade 13 rotates the mixed material, the stirring effect is good, oil is injected into the shell 2 through the oil inlet pipe 201, the oil is heated through the heating pipe 5, the mixed material is subjected to oil bath heating, after the reaction of the mixed material is finished, the first electric control valve 8 is opened, the mixture falls along the discharging pipe 7 and enters the filter screen 304, the material is filtered through the filter screen 304, waste liquid falls into the waste material tank 301 for collection, the water is fed into the spray header 16 through the guide pipe 154, the spray header 16 washes the material, the filter screen 304 is rotated to the right side of the vertical frame 3 through the damping rotating shaft 303, and the washed material is dried through the dryer 302, so that the graphene material is obtained.

In the description herein, references to the description of "one embodiment," "an example," "a specific example," etc., mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

The preferred embodiments of the present invention disclosed above are intended only to help illustrate the present invention. The preferred embodiments are not intended to be exhaustive or to limit the invention to the precise embodiments disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and its practical applications, to thereby enable others skilled in the art to best understand the invention for and utilize the invention. The present invention is limited only by the claims and their full scope and equivalents.

Claims

1. A apparatus for producing graphene materials, includes base (1), its characterized in that: the improved stirring device is characterized in that a shell (2) is connected to the left side of the top of the base (1), a vertical frame (3) is connected to the right side of the top of the base (1), supporting legs (4) are connected to the four corners of the bottom of the base (1), a heating pipe (5) is connected to the bottom of the inner cavity of the shell (2), an inner tank (6) is connected to the top of the inner tank (2), a discharging pipe (7) is communicated with the bottom of the right side wall of the inner tank (6), a first electric control valve (8) is installed at one end, extending out of the shell (2), of the discharging pipe (7), an ultrasonic vibrator (9) is installed at the bottom of the inner cavity of the inner tank (6), a cover plate (10) is connected to the top of the shell (2) through bolts, a stirring motor (11) is connected to the left side of the top of the cover plate (10), a stirring shaft (12) is connected, a first feeding pipe (14) penetrates through the top of the shell (2), the lower end of the first feeding pipe (14) extends into the inner tank (6), the right side of the top of the shell (2) is connected with a water tank (15), and the right side of the bottom of the cover plate (10) is connected with a spray header (16).

2. The production apparatus for producing a graphene material according to claim 1, wherein: the left side wall bottom of grudging post (3) is connected with dump bin (301), the right side wall top of grudging post (3) is connected with drying-machine (302), the front end middle part of grudging post (3) is rotated and is connected with damping pivot (303), damping pivot (303) lateral wall is connected with filter screen (304), filter screen (304) are located discharging pipe (7) below.

3. The production apparatus for producing a graphene material according to claim 1, wherein: a left water storage cavity (151) and a right water storage cavity (152) are formed in the water tank (15), a second feeding pipe (153) is communicated between the left water storage cavity (151) and the inner tank (6), a guide pipe (154) is communicated between the right water storage cavity (152) and the spray header (16), and a second electric control valve (155) is installed on the second feeding pipe (153) and the guide pipe (154).

4. The production apparatus for producing a graphene material according to claim 1, wherein: the upper part and the lower part of the shell (2) are respectively connected with an oil inlet pipe (201) and an oil outlet pipe (202), and the oil outlet pipe (202) is provided with a control valve.

5. The production apparatus for producing a graphene material according to claim 1, wherein: the outer side wall of the shell (2) is connected with a heat insulation coating.

6. The production apparatus for producing a graphene material according to claim 2, wherein: the waste box (301) is positioned right below the spray header (16).