CN214714491U

CN214714491U - Double-aqueous-phase bletilla striata glucomannan extraction equipment

Info

Publication number: CN214714491U
Application number: CN202120305196.0U
Authority: CN
Inventors: 柯训忠; 何俊辉; 柯诗媛
Original assignee: Guangdong Kangwang Cosmetics Co ltd
Current assignee: Guangdong Kangwang Cosmetics Co ltd
Priority date: 2021-02-03
Filing date: 2021-02-03
Publication date: 2021-11-16
Anticipated expiration: 2031-02-03

Abstract

The utility model discloses a tuber of hyacinth bletilla glucomannan two aqueous phase extraction equipment relates to tuber of hyacinth bletilla glucomannan technical field, and it is loaded down with trivial details for solving current tuber of hyacinth bletilla glucomannan two aqueous phase extraction method step, need continuous transporting the raw materials at the in-process that draws, the lower problem of extraction efficiency. Even pulp jar is located the top of centrifugal filtration jar, it is located the top of supersound countercurrent extraction machine to join in marriage the fluid reservoir, the below of supersound countercurrent extraction machine is provided with supersonic generator, join in marriage the outside one side of fluid reservoir and install the second motor, the third motor is installed to the upper end of supersound countercurrent extraction machine, the upper end of even pulp jar is provided with the opening, the driving groove is installed to one side of stand, first motor is installed to one side of driving groove lower extreme, the internally mounted of driving groove has first action wheel and first follow driving wheel, first action wheel passes through the hold-in range with first follow driving wheel and is connected.

Description

Double-aqueous-phase bletilla striata glucomannan extraction equipment

Technical Field

The utility model relates to a tuber of hyacinth bletilla glucomannan technical field specifically is a tuber of hyacinth bletilla glucomannan two aqueous phase extraction facilities.

Background

Bletilla striata is the stem piece of bletilla striata of the family Orchidaceae, which is bitter, sweet, astringent and slightly cold in nature. The bletilla striata is rich in glucomannan, and researches show that the bletilla striata glucomannan has biological activities of resisting inflammation, promoting blood coagulation and the like. As a natural polymer material, the bletilla striata glucomannan also has the characteristics of slow release function, local retention, self degradability, no irritation, no toxic or side effect, low price, easy obtainment and the like, and the application of the bletilla striata glucomannan in the preparation process of the medicine is more and more emphasized. Neutral glucomannan extracted from bletilla has obvious free radical scavenging capacity, and the scavenging effect is gradually enhanced with the increase of glucomannan concentration, thus showing dose-effect dependence. The activity of eliminating the bletilla striata gum is higher than that of vitamin E, so that the bletilla striata gum is added into the anti-aging nutritional cosmetic to supplement the nutrition of skin, eliminate excessive free radicals in the body and delay the aging of the skin, and bletilla striata glucomannan needs to be extracted in the production process of related bletilla striata products.

However, the existing double-aqueous-phase extraction method of bletilla striata glucomannan is complicated in steps, raw materials need to be continuously transported in the extraction process, and the extraction efficiency is low, so that the existing requirements are not met, and the double-aqueous-phase extraction equipment of the bletilla striata glucomannan is provided.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a tuber of hyacinth bletilla glucomannan two aqueous phases extraction equipment to current tuber of hyacinth bletilla glucomannan two aqueous phases that provide in solving above-mentioned background art draws method steps loaded down with trivial details, needs continuous transporting the raw materials at the in-process that draws, the lower problem of extraction efficiency.

In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a tuber of hyacinth bletilla glucomannan two aqueous phases extraction equipment, includes homogenate jar, centrifugal filtration jar, joins in marriage fluid reservoir, supersound countercurrent extraction machine, ultrafiltration mechanism and stand, homogenate jar is located the top of centrifugal filtration jar, it is located the top of supersound countercurrent extraction machine to join in marriage the fluid reservoir, the below of supersound countercurrent extraction machine is provided with supersonic generator, join in marriage the outside one side of fluid reservoir and install the second motor, the third motor is installed to the upper end of supersound countercurrent extraction machine, the upper end of homogenate jar is provided with the opening, the driving groove is installed to one side of stand, first motor is installed to one side of driving groove lower extreme, the internally mounted of driving groove has first action wheel and first from the driving wheel, first action wheel passes through the hold-in range with first follow driving wheel and is connected, and first motor passes through the coupling joint with first action wheel, first follow driving wheel, The puddler is all installed to the one end of second motor and third motor, and puddler and first all pass through the coupling joint from driving wheel, second motor and third motor, the outside of puddler is provided with helical blade, and helical blade and puddler welded connection, homogenate jar and centrifugal filtration jar all are connected through the backup pad with the stand.

Preferably, the internally mounted of centrifugation filter tank has a section of thick bamboo, it crosses the bearing with the centrifugation filter tank and is connected to strain a section of thick bamboo, the upper end of straining a section of thick bamboo is provided with the feed inlet, be provided with the conveying pipeline between homogenate jar and the centrifugation filter tank, and the conveying pipeline passes through the bearing with the feed inlet and be connected, the externally mounted of conveying pipeline has first valve, and the conveying pipeline passes through flange joint with first valve, the second is installed from the driving wheel in the outside of feed inlet, the curb plate is installed to the outside one side of centrifugation filter tank, the second action wheel is installed to the upper end of curb plate, the fourth motor is installed to the lower extreme of curb plate, and the fourth motor passes through the coupling joint with the second action wheel.

Preferably, be provided with the first pump body between centrifugal filtration jar and the supersound extractor against current, first conveyer pipe is all installed at the both ends of the first pump body, and the inside of the one end embedding centrifugal filtration jar of first conveyer pipe, and the inside of the opposite side embedding supersound extractor against current of first conveyer pipe, join in marriage and be provided with the transfer line between fluid reservoir and the supersound extractor against current, the externally mounted of transfer line has the second valve, and the second valve passes through flange joint with the transfer line, be provided with the second pump body between supersound extractor against current and the ultrafiltration mechanism, the second conveyer pipe is all installed at the both ends of the second pump body, and the inside of the one end embedding supersound extractor against current of second conveyer pipe, and the inside of the other end embedding ultrafiltration mechanism of second conveyer pipe.

Preferably, the ultrafiltration mechanism comprises a water inlet pipe, an ultrafiltration membrane, a water outlet pipe and a control cabinet, and the ultrafiltration membrane is positioned between the water inlet pipe and the water outlet pipe.

Preferably, the upper end of the liquid preparation tank is provided with a first liquid inlet pipe and a second liquid inlet pipe.

Preferably, the upper ends of the homogenate tank, the centrifugal filter tank, the liquid preparation tank and the ultrasonic countercurrent extractor are all provided with sight holes.

Compared with the prior art, the beneficial effects of the utility model are that:

1. the utility model discloses put into the inside of homogenate jar with tuber of hyacinth bletilla and deionized water, first motor drive puddler stirs, prepare the splendid achnatherum thick liquid, tuber of hyacinth bletilla thick liquid gets into the inside of centrifugal filtration jar through the conveying pipeline, fourth motor work drive strains a section of thick bamboo high-speed rotation, make the tuber of hyacinth bletilla thick liquid receive centrifugal force effect separation, separate the clear liquid, the clear liquid gets into the inside of supersound countercurrent extraction machine under the drive of first pump body, the inside ethanol-dipotassium hydrogen phosphate double aqueous phase solution of joining in marriage liquid jar gets into the inside of supersound countercurrent extraction machine through the transfer line simultaneously, mix with the clear liquid and form the extraction medium, when the ultrasonic wave acts on the extraction medium, produce strong cavitation effect, form many little cavities in the extraction medium, these little cavities are closed in the twinkling of an eye and produce the pressure of several thousand atmospheric pressures, impel plant cell tissue broken wall, the diffusion of dissolving out of effective component is accelerated, the solution after dissolution and diffusion enters an ultrafiltration mechanism under the drive of a second pump body, and is filtered by an ultrafiltration membrane to obtain the bletilla striata glucomannan solution.

2. The utility model discloses use helical blade to stir the raw materials, can improve and draw the mixed degree of consistency between the in-process raw materials to extraction quality has been improved.

Drawings

FIG. 1 is a front view of the double aqueous phase extraction apparatus for bletilla striata glucomannan of the present invention;

FIG. 2 is a schematic structural view of the centrifugal filter tank of the present invention;

fig. 3 is a top view of the drive slot of the present invention;

fig. 4 is a schematic structural view of the stirring rod of the present invention.

In the figure: 1. a homogenizing tank; 2. a centrifugal filtration tank; 3. preparing a liquid tank; 4. an ultrasonic countercurrent extractor; 5. an ultrafiltration mechanism; 6. a drive slot; 7. a first motor; 8. a first drive wheel; 9. a first driven wheel; 10. a stirring rod; 11. a second motor; 12. a third motor; 13. a helical blade; 14. a filter cartridge; 15. a feed inlet; 16. a side plate; 17. a second driven wheel; 18. a second drive wheel; 19. a fourth motor; 20. a delivery pipe; 21. a first valve; 22. a first pump body; 23. a first delivery pipe; 24. a transfusion tube; 25. a second valve; 26. a second pump body; 27. a second delivery pipe; 28. a water inlet pipe; 29. ultrafiltration membranes; 30. a water outlet pipe; 31. an ultrasonic generator; 32. a control cabinet; 33. a first liquid inlet pipe; 34. a second liquid inlet pipe; 35. a column; 36. a sight hole; 37. and a support plate.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.

Referring to fig. 1-4, the present invention provides an embodiment: a double aqueous phase extraction equipment of bletilla striata glucomannan comprises a homogenate tank 1, a centrifugal filter tank 2, a liquid preparation tank 3, an ultrasonic countercurrent extractor 4, an ultrafiltration mechanism 5 and a vertical column 35, wherein the homogenate tank 1 is positioned above the centrifugal filter tank 2, the liquid preparation tank 3 is positioned above the ultrasonic countercurrent extractor 4, an ultrasonic generator 31 is arranged below the ultrasonic countercurrent extractor 4, a second motor 11 is arranged at one side outside the liquid preparation tank 3, a third motor 12 is arranged at the upper end of the ultrasonic countercurrent extractor 4, an opening is arranged at the upper end of the homogenate tank 1, a driving groove 6 is arranged at one side of the vertical column 35, a first motor 7 is arranged at one side of the lower end of the driving groove 6, a first driving wheel 8 and a first driven wheel 9 are arranged inside the driving groove 6, the first driving wheel 8 is connected with the first driven wheel 9 through a synchronous belt, and the first motor 7 is connected with the first driving wheel 8 through a coupler, first from driving wheel 9, puddler 10 is all installed to the one end of second motor 11 and third motor 12, and puddler 10 and first from driving wheel 9, second motor 11 and third motor 12 all pass through coupling joint, the outside of puddler 10 is provided with helical blade 13, and helical blade 13 and puddler 10 welded connection, homogenate jar 1 and centrifugal filtration jar 2 all are connected through backup pad 37 with stand 35, put into homogenate jar 1's inside with tuber of hyacinth bletilla and deionized water, the first action wheel 8 of 7 work drives of first motor rotates, first action wheel 8 drives first from driving wheel 9 and rotates, first from driving wheel 9 drives puddler 10 and rotates the stirring to the material, the splendid attire thick liquid is prepared.

Further, a filter cylinder 14 is installed inside the centrifugal filter tank 2, the filter cylinder 14 is connected with the centrifugal filter tank 2 through a bearing, a feed inlet 15 is formed in the upper end of the filter cylinder 14, a feed delivery pipe 20 is arranged between the homogenizing tank 1 and the centrifugal filter tank 2, the feed delivery pipe 20 is connected with the feed inlet 15 through a bearing, a first valve 21 is installed outside the feed delivery pipe 20, the feed delivery pipe 20 is connected with the first valve 21 through a flange, a second driven wheel 17 is installed outside the feed inlet 15, a side plate 16 is installed on one side outside the centrifugal filter tank 2, a second driving wheel 18 is installed on the upper end of the side plate 16, a fourth motor 19 is installed at the lower end of the side plate 16, the fourth motor 19 is connected with the second driving wheel 18 through a coupler, the fourth motor 19 drives the second driving wheel 18, the second driving wheel 18 drives the second driven wheel 17, and the second driven wheel 17 drives the filter cylinder 14 to rotate at a high speed, the slurry of bletilla striata is separated by centrifugal force inside the filter cartridge 14, and the clear liquid is separated.

Further, a first pump body 22 is arranged between the centrifugal filtration tank 2 and the ultrasonic countercurrent extractor 4, a first delivery pipe 23 is arranged at both ends of the first pump body 22, one end of the first delivery pipe 23 is embedded into the centrifugal filtration tank 2, the other side of the first delivery pipe 23 is embedded into the ultrasonic countercurrent extractor 4, a delivery pipe 24 is arranged between the liquid preparation tank 3 and the ultrasonic countercurrent extractor 4, a second valve 25 is arranged outside the delivery pipe 24, the second valve 25 is connected with the delivery pipe 24 through a flange, a second pump body 26 is arranged between the ultrasonic countercurrent extractor 4 and the ultrafiltration mechanism 5, a second delivery pipe 27 is arranged at both ends of the second pump body 26, one end of the second delivery pipe 27 is embedded into the ultrasonic countercurrent extractor 4, the other end of the second delivery pipe 27 is embedded into the ultrafiltration mechanism 5, and double water phase solution and clear liquid are mixed to form an extraction medium, when the ultrasonic wave acts on the extracting medium, a strong cavitation effect is generated, a plurality of small cavities are formed in the extracting medium, and the small cavities are instantaneously closed to generate pressure of thousands of atmospheric pressures, so that the wall breaking of plant cell tissues is promoted, and the dissolution and diffusion of effective components are accelerated.

Further, the ultrafiltration mechanism 5 comprises a water inlet pipe 28, an ultrafiltration membrane 29, a water outlet pipe 30 and a control cabinet 32, the ultrafiltration membrane 29 is located between the water inlet pipe 28 and the water outlet pipe 30, the dissolved and diffused solution enters the ultrafiltration mechanism 5 through a second delivery pipe 27 under the drive of the second pump body 26, is shunted to the interior of each ultrafiltration membrane 29 through the water inlet pipe 28, enters the water outlet pipe 30 after being filtered by the ultrafiltration membrane 29, and is finally discharged through the water outlet pipe 30, so that the extracted bletilla striata glucomannan solution can be obtained.

Further, the upper end of the liquid preparation tank 3 is provided with a first liquid inlet pipe 33 and a second liquid inlet pipe 34 for preparing ethanol-dipotassium hydrogen phosphate double-aqueous-phase solution.

Furthermore, the upper ends of the homogenate tank 1, the centrifugal filter tank 2, the liquid preparation tank 3 and the ultrasonic countercurrent extractor 4 are all provided with sight holes 36, which is convenient for observation in the extraction process.

The working principle is as follows: when in use, bletilla striata and deionized water are placed in the homogenate tank 1, the first motor 7 drives the first driving wheel 8 to rotate, the first driving wheel 8 drives the first driven wheel 9 to rotate, the first driven wheel 9 drives the stirring rod 10 to rotate to stir materials, bletilla striata slurry is prepared, after the preparation is finished, the first valve 21 is opened, the bletilla striata slurry enters the interior of the centrifugal filter tank 2 through the material conveying pipe 20, the fourth motor 19 drives the second driving wheel 18 to operate, the second driving wheel 18 drives the second driven wheel 17, the second driven wheel 17 drives the filter cylinder 14 to rotate at high speed, the bletilla striata slurry is separated under the centrifugal force in the filter cylinder 14, clear liquid is separated, the clear liquid enters the interior of the ultrasonic countercurrent extractor 4 through the first conveying pipe 23 under the driving of the first pump body 22, the second valve 25 is opened at the same time, ethanol-dipotassium hydrogen phosphate double-water-phase solution prepared in the liquid preparation tank 3 enters the interior of the ultrasonic countercurrent extractor 4 through the liquid conveying pipe 24, the third motor 12 works to drive the stirring rod 10 to rotate, the double water phase solution and the clear liquid are mixed to form an extraction medium, when ultrasonic waves act on the extraction medium, a strong cavitation effect is generated, a plurality of small cavities are formed in the extraction medium, the small cavities are instantly closed to generate pressure of thousands of atmospheric pressure, the wall breaking of plant cell tissues is promoted, the dissolution and diffusion of effective components are accelerated, the solution after the dissolution and diffusion enters the ultrafiltration mechanism 5 through the second conveying pipe 27 under the driving of the second pump body 26, is shunted to the inside of each ultrafiltration membrane 29 through the water inlet pipe 28, enters the water outlet pipe 30 after being filtered by the ultrafiltration membrane 29, and is finally discharged through the water outlet pipe 30, so that the bletilla striata glucomannan solution after the extraction is finished can be obtained.

It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.

Claims

1. The utility model provides a two aqueous phase extraction equipment of tuber of hyacinth bletilla glucomannan, includes homogenate jar (1), centrifugal filtration jar (2), joins in marriage fluid reservoir (3), supersound countercurrent extraction machine (4), ultrafiltration mechanism (5) and stand (35), its characterized in that: the utility model discloses a centrifugal filter tank, including homogenate jar (1), liquid preparation tank (3), ultrasonic countercurrent extractor (4), ultrasonic generator (31) and driving groove (6), first motor (7) is installed to one side of liquid preparation tank (3) outside, third motor (12) is installed to the upper end of ultrasonic countercurrent extractor (4), the upper end of homogenate jar (1) is provided with the opening, driving groove (6) is installed to one side of stand (35), first motor (7) is installed to one side of driving groove (6) lower extreme, the internally mounted of driving groove (6) has first action wheel (8) and first driven wheel (9), first action wheel (8) pass through the hold-in range with first driven wheel (9) and are connected, and first motor (7) pass through the coupling joint with first action wheel (8), puddler (10) are all installed to the one end of first follow driving wheel (9), second motor (11) and third motor (12), and puddler (10) and first follow driving wheel (9), second motor (11) and third motor (12) all through the coupling joint, the outside of puddler (10) is provided with helical blade (13), and helical blade (13) and puddler (10) welded connection, homogenate jar (1) and centrifugal filtration jar (2) all are connected through backup pad (37) with stand (35).

2. The double aqueous phase extraction equipment of bletilla striata glucomannan according to claim 1, which is characterized in that: a filter cylinder (14) is arranged in the centrifugal filter tank (2), the filter cylinder (14) is connected with the centrifugal filter tank (2) through a bearing, a feed inlet (15) is arranged at the upper end of the filter cylinder (14), a feed delivery pipe (20) is arranged between the homogenate tank (1) and the centrifugal filter tank (2), the feed delivery pipe (20) is connected with the feed inlet (15) through a bearing, a first valve (21) is arranged outside the feed delivery pipe (20), and the material conveying pipe (20) is connected with the first valve (21) through a flange, a second driven wheel (17) is arranged on the outer side of the feeding hole (15), a side plate (16) is arranged on one side of the outer part of the centrifugal filter tank (2), a second driving wheel (18) is arranged at the upper end of the side plate (16), a fourth motor (19) is arranged at the lower end of the side plate (16), and the fourth motor (19) is connected with the second driving wheel (18) through a coupler.

3. The double aqueous phase extraction equipment of bletilla striata glucomannan according to claim 1, which is characterized in that: the utility model discloses a centrifugal filter jar (2) and supersound countercurrent extraction machine (4) between be provided with first pump body (22), first conveyer pipe (23) are all installed at the both ends of first pump body (22), and the inside of the one end embedding centrifugal filter jar (2) of first conveyer pipe (23), and the inside of the opposite side embedding supersound countercurrent extraction machine (4) of first conveyer pipe (23), be provided with transfer line (24) between joining in marriage fluid reservoir (3) and supersound countercurrent extraction machine (4), the externally mounted of transfer line (24) has second valve (25), and second valve (25) pass through flange joint with transfer line (24), be provided with second conveyer pipe (26) between supersound countercurrent extraction machine (4) and ultrafiltration mechanism (5), second conveyer pipe (27) are all installed at the both ends of the second pump body (26), and the inside of the one end embedding supersound countercurrent extraction machine (4) of second conveyer pipe (27), and the other end of the second delivery pipe (27) is embedded in the interior of the ultrafiltration mechanism (5).

4. The double aqueous phase extraction equipment of bletilla striata glucomannan according to claim 1, which is characterized in that: the ultrafiltration mechanism (5) comprises a water inlet pipe (28), an ultrafiltration membrane (29), a water outlet pipe (30) and a control cabinet (32), wherein the ultrafiltration membrane (29) is positioned between the water inlet pipe (28) and the water outlet pipe (30).

5. The double aqueous phase extraction equipment of bletilla striata glucomannan according to claim 1, which is characterized in that: the upper end of the liquid preparation tank (3) is provided with a first liquid inlet pipe (33) and a second liquid inlet pipe (34).

6. The double aqueous phase extraction equipment of bletilla striata glucomannan according to claim 1, which is characterized in that: the upper ends of the homogenate tank (1), the centrifugal filter tank (2), the liquid preparation tank (3) and the ultrasonic countercurrent extractor (4) are all provided with sight holes (36).