CN214344557U

CN214344557U - Ultrasonic extraction device of total alkali liquor of sophora alopecuroide

Info

Publication number: CN214344557U
Application number: CN202022971419.5U
Authority: CN
Inventors: 刘武彬; 李亚明; 杨培元
Original assignee: Inner Mongolia Qingfengyuan Biological Preparation Co ltd
Current assignee: Inner Mongolia Qingfengyuan Biological Preparation Co ltd
Priority date: 2020-12-11
Filing date: 2020-12-11
Publication date: 2021-10-08
Anticipated expiration: 2030-12-11

Abstract

The utility model discloses an supersound extraction element of total alkali lye of sophora alopecuroide, two supports including relative setting, the support lateral wall all rotates and is connected with the support ring, two the common fixedly connected with extraction bottle of support ring, be provided with quantitative conveying mechanism on the extraction bottle, the support relative lateral wall all rotates and is connected with the rotation axis, the support lateral wall is provided with the motor, the motor output runs through the support lateral wall and is connected with the rotation axis, the rotation axis is connected with powerful mixing mechanism, the lateral wall is provided with the ultrasonic wave extractor on the support. The utility model discloses a be provided with the rotatory stirring leaf that is driven by the motor in the extraction bottle and rotate, trigger the stirring to the liquid in the extraction bottle for can the intensive mixing between the extract, and utilize and be provided with ultrasonic extractor, oscillating beam and spiral oscillation piece in extraction bottle department and realize carrying out the ultrasonic wave to the liquid in the extraction bottle and draw, realize that the flash mixed has the improvement extraction rate.

Description

Ultrasonic extraction device of total alkali liquor of sophora alopecuroide

Technical Field

The utility model relates to a processing technology field is drawed to total lye, especially relates to an supersound extraction element of total lye of sophora alopecuroide.

Background

The herba Sophorae Alopecuroidis and herba Sophorae Alopecuroidis belonging to Leguminosae are used as main sources of herba Sophorae Alopecuroidis total alkali solution, and have effects of clearing heat, eliminating dampness, killing parasite, and promoting urination. Pharmacological experiments prove that the total alkaloids also have the effects of arrhythmia resistance, anticancer activity and the like. The Sophora alopecuroides and Sophora alopecuroides contain a large amount of alkaloids, wherein the highest content of the alkaloids is matrine and oxymatrine, and other similar alkaloids are also contained,

the process comprises pulverizing the seed, root, stem and leaf of herba Sophorae Alopecuroidis into coarse powder; moistening herba Sophorae Alopecuroidis coarse powder with water, sealing in a container, and standing for more than 24 hr; putting the wet sophora alopecuroide coarse powder into a reflux extractor, adding an alcohol solvent to the surface of a submerged material, closing an extraction tank, soaking for more than 12 hours, putting the extract into a concentration tank, closing a return pipe valve, adding the alcohol solvent into the extraction tank again to the surface of the submerged material, heating, starting the solvent return pipe valve after the solvent begins to reflux, continuously extracting, checking that the extract does not contain alkaloid after extracting for 8 hours, and recovering the alcohol solvent for later use; concentrating the extracting solution in the concentrated solution tank, and recovering the alcohol solvent for later use; adding acid into the concentrated solution, acidifying, centrifuging, and filtering to obtain filtrate; putting the filtrate into a reaction tank, adding 20 percent (VN) of benzene solvent, stirring and extracting, discharging an acid water layer, and recovering the benzene solvent for later use by a distillation method; adding alkali into the acid water layer for alkalization, adding into a reaction tank again, extracting with benzene, alkyl halide and ester solvent for several times, wherein the dosage of benzene, alkyl halide and ester solvent is 20% (VN) each time, and obtaining extract; transferring the benzene, alkyl halide and ester solvent into 10% sulfuric acid water solution, stirring to convert alkaloid salt into acid water, recovering benzene, halogenated alkyl and ester solvent, and collecting acid water solution.

In the production process, need divide to add benzene class, alkyl halide, ester solvent in the acid water layer many times and extract to collect, current equipment is when extracting total alkali lye, stirs through rocking the extraction flask between alkali lye and the acid water layer, and it can't fully make alkali lye and acid water mix, and current equipment divides to inwards add benzene class, alkyl halide, ester solvent operation complicacy many times, influences extraction efficiency.

SUMMERY OF THE UTILITY MODEL

The utility model aims at solving the problems that the prior equipment stirs the extraction bottle by shaking when extracting the total alkali liquor, the alkali liquor and the acid water layer, which can not fully mix the alkali liquor and the acid water, and the prior equipment adds the benzene, the alkyl halide and the ester solvent by a plurality of times, which has the defects of complex operation and influence on the extraction efficiency, in the prior production process, the ultrasonic extraction device of the total alkali liquor of sophora alopecuroides can rotate by arranging a rotary stirring blade driven by a motor in the extraction bottle, trigger and stir the liquid in the extraction bottle, so that the extraction liquor can be fully mixed, and the ultrasonic extraction device is arranged at the extraction bottle, the oscillating rod and the spiral oscillating piece are utilized to realize the ultrasonic extraction of the liquid in the extraction bottle, the extraction rate is improved by realizing rapid mixing.

In order to achieve the above purpose, the utility model adopts the following technical scheme:

the utility model provides an supersound extraction element of total alkali lye of sophora alopecuroide, includes two supports that set up relatively, the support lateral wall all rotates and is connected with the support ring, two the common fixedly connected with extraction bottle of support ring, be provided with quantitative conveying mechanism on the extraction bottle, the support relative lateral wall all rotates and is connected with the rotation axis, the support lateral wall is provided with the motor, the motor output runs through the support lateral wall and is connected with the rotation axis, the rotation axis is connected with powerful mixing mechanism, the lateral wall is provided with the ultrasonic extractor on the support.

Preferably, the quantitative conveying mechanism comprises a liquid inlet pipe arranged at the upper end of the extraction bottle, a quantitative conveying pipe fixedly connected above the liquid inlet pipe, and a liquid pouring funnel is arranged at the top of the quantitative conveying pipe.

Preferably, a plurality of quantitative cavities are uniformly arranged on the quantitative conveying pipe, and control valves are arranged on the quantitative conveying pipe below the quantitative cavities.

Preferably, powerful mixing mechanism includes the connection pad with rotating shaft tip fixed connection, two the connection pad is connected through a plurality of arc pieces that are the arc setting, the rotatory stirring leaf of arc piece inside wall fixedly connected with.

Preferably, the output end of the ultrasonic extractor is connected with an oscillating rod, a vertically arranged spiral oscillating piece is arranged in the extraction flask, and the oscillating rod penetrates into the extraction flask and is connected with the spiral oscillating piece.

Preferably, the bottom of the extraction bottle is provided with a liquid outlet pipe, and the liquid outlet pipe is provided with a liquid outlet valve.

Compared with the prior art, the beneficial effects of the utility model are that:

1. through being provided with quantitative conveyer pipe above the extraction bottle to be provided with a plurality of ration chambeies and control valve at quantitative conveyer pipe, when needs segmentation to the interior heating lye of extraction bottle, can make to be located quantitative intracavity equivalent lye and enter into the extraction bottle in proper order through opening the control valve from bottom to top in proper order, thereby make things convenient for the user of service to operate.

2. Through be provided with the rotatory stirring leaf that is driven by the motor in the extraction bottle and rotate, trigger the stirring to the liquid in the extraction bottle for can the intensive mixing between the extraction liquid, and utilize and be provided with ultrasonic extractor, oscillating rod and spiral oscillation piece in extraction bottle department and realize carrying out the ultrasonic extraction to the liquid in the extraction bottle, realize that the flash mixed has the improvement extraction rate.

Drawings

FIG. 1 is a schematic structural view of an ultrasonic extraction device for total alkali solution of Sophora alopecuroides provided by the present invention;

FIG. 2 is a schematic view of the connection relationship between the arc-shaped members in the ultrasonic extraction device of total alkali solution of Sophora alopecuroides.

In the figure: the device comprises a support 1, a support ring 2, an extraction bottle 3, a rotating shaft 4, a motor 5, an ultrasonic extractor 6, a liquid inlet pipe 7, a quantitative conveying pipe 8, a liquid pouring funnel 9, a quantitative cavity 10, a control valve 11, a connecting disc 12, an arc-shaped part 13, a rotary stirring blade 14, an oscillating rod 15 and a spiral oscillating piece 16.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.

Referring to fig. 1-2, an ultrasonic extraction device of total alkali lye of sophora alopecuroides comprises two opposite supports 1, the side walls of the supports 1 are rotatably connected with support rings 2, the two support rings 2 are fixedly connected with an extraction bottle 3, a quantitative conveying mechanism is arranged on the extraction bottle 3, further, the quantitative conveying mechanism comprises a liquid inlet pipe 7 arranged at the upper end of the extraction bottle 3, a quantitative conveying pipe 8 fixedly connected above the liquid inlet pipe 7, a liquid pouring funnel 9 is arranged at the top of the quantitative conveying pipe 8, a plurality of quantitative cavities 10 are uniformly arranged on the quantitative conveying pipe 8, a control valve 11 is arranged on the quantitative conveying pipe 8 below the quantitative cavities 10, the control valve 11 arranged at the bottom of the quantitative cavities 10 can be opened by times by arranging the quantitative cavities 10, the quality of the alkali lye entering the extraction bottle 3 at each time is consistent, and the addition of the same amount of alkali lye can be conveniently carried out by times, the operation of workers is more convenient; during the extraction process, the alkaline solution is added in sequence, and the control valve 11 is opened from bottom to top in sequence, so that the alkaline solution in the quantitative cavity 10 can enter the extraction flask 3 in the same amount every time.

All rotate to the relative lateral wall of support 1 and be connected with rotation axis 4, 1 lateral wall of support is provided with

motor

5, 5 outputs of motor run through 1 lateral wall of support and are connected with rotation axis 4, rotation axis 4 is connected with powerful mixing mechanism, furthermore, powerful mixing mechanism includes connection pad 12 with 4 tip fixed connection of rotation axis, two connection pads 12 are connected through a plurality of arc 13 that are the arc setting, 13 inside wall fixed connection of arc is rotatory stirs leaf 14, through setting up rotatory stirring leaf 14, make and to rotate under motor 5's the drive, carry out intensive mixing with the liquid of layering.

The lateral wall is provided with ultrasonic extractor 6 on support 1, and ultrasonic extractor 6 is prior art, does not describe here any more, and the advantage of adopting the ultrasonic extraction includes as follows: the best extraction rate can be obtained after the ultrasonic wave enhanced extraction is carried out for 20-40 minutes, and the extraction time is only one third or less of that of a water boiling and alcohol precipitation method. The extraction is sufficient, and the extraction amount is more than twice of that of the traditional method. After ultrasonic wave is added (under the condition of 65 ℃), the extraction time of the effective components of the plants is about 40 minutes, and the cooking time of the cooking method usually needs two to three hours which is more than 3 times of the extraction time of the ultrasonic wave; the applicability is wide, and most of various components of the traditional Chinese medicine can be extracted by ultrasonic; the ultrasonic extraction has large treatment capacity of medicinal raw materials with small relation between the properties (such as polarity) of a solvent and a target extract, is improved by times or more, has few impurities, and is easy to separate and purify effective components; the extraction process has low cost and remarkable comprehensive economic benefit;

further, the output end of the ultrasonic extractor 6 is connected with an oscillating rod 15, a vertically arranged spiral oscillating piece 16 is arranged in the extraction flask 3, and the oscillating rod 15 penetrates into the extraction flask 3 and is connected with the spiral oscillating piece 16.

Further, a liquid outlet pipe is arranged at the bottom of the extraction bottle 3, and a liquid outlet valve is arranged on the liquid outlet pipe.

In the process of extracting the total alkali liquor, the acid water is poured into the extraction bottle 3, then the alkali water consisting of benzene, alkyl halide and ester solvent is poured into the liquor pouring funnel 9 above the quantitative conveying pipe 8, the control valve 11 arranged on the quantitative conveying pipe 8 is opened in sequence, the liquid in the liquor pouring funnel 9 can gradually fill the quantitative cavity 10, and the control valve 11 is closed at the moment;

in carrying out the extraction in-process, add the buck in proper order, adopt to open in proper order and open control valve 11 from upwards opening down, make the lye that is located quantitative chamber 10 the same measurement at every turn enter into extraction flask 3 in, in order to guarantee lye and acid water ability intensive mixing, open motor 5 and ultrasonic extractor 6, motor 5 is opened and is made rotation axis 4 rotate, arc 13 that sets up on rotation axis 4 can drive rotatory stirring leaf 14 and rotate, when rotatory stirring leaf 14 is rotatory, can mix the lye and the acid water of layering, thereby guarantee to fully contact between the two, and in the stirring of rotatory stirring leaf 14, utilize ultrasonic extractor 6 to pass through the spiral oscillation piece 16 that oscillating bar 15 is connected, make spiral oscillation piece 16 can contact with the water, thereby through the advantage that utilizes the supersound to draw: the best extraction rate can be obtained after the ultrasonic wave enhanced extraction is carried out for 20-40 minutes, and the extraction time is only one third or less of that of a water boiling and alcohol precipitation method. The extraction is sufficient, and the extraction amount is more than twice of that of the traditional method. After ultrasonic wave is added (under the condition of 65 ℃), the extraction time of the effective components of the plants is about 40 minutes, and the cooking time of the cooking method usually needs two to three hours which is more than 3 times of the extraction time of the ultrasonic wave; the applicability is wide, and most of various components of the traditional Chinese medicine can be extracted by ultrasonic; the ultrasonic extraction has large treatment capacity of medicinal raw materials with small relation between the properties (such as polarity) of a solvent and a target extract, is improved by times or more, has few impurities, and is easy to separate and purify effective components; the extraction process has low cost and remarkable comprehensive economic benefit.

Thereby quickly and effectively realizing the extraction of the total alkali liquor and ensuring the processing effect and the extraction rate.

The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims

1. The utility model provides an supersound extraction element of total alkali lye of sophora alopecuroide, includes two supports that set up relatively, its characterized in that, the support lateral wall all rotates and is connected with the support ring, two the common fixedly connected with extraction bottle of support ring, be provided with quantitative conveying mechanism on the extraction bottle, the support relative lateral wall all rotates and is connected with the rotation axis, the support lateral wall is provided with the motor, the motor output runs through the support lateral wall and is connected with the rotation axis, the rotation axis is connected with powerful mixing mechanism, the lateral wall is provided with the ultrasonic extractor on the support.

2. The ultrasonic extraction device of the total sophora alopecuroide lye as claimed in claim 1, wherein the quantitative conveying mechanism comprises a liquid inlet pipe disposed at the upper end of the extraction bottle, a quantitative conveying pipe fixedly connected above the liquid inlet pipe, and a liquid pouring funnel disposed at the top of the quantitative conveying pipe.

3. The ultrasonic extraction device of the total sophora alopecuroides alkali liquor as claimed in claim 2, characterized in that a plurality of quantitative cavities are uniformly arranged on the quantitative conveying pipe, and control valves are arranged on the quantitative conveying pipes below the quantitative cavities.

4. The ultrasonic extraction device of the total sophora alopecuroides alkali liquor according to claim 1, wherein the powerful mixing mechanism comprises connecting discs fixedly connected with the end parts of the rotating shafts, the two connecting discs are connected through a plurality of arc-shaped pieces arranged in an arc shape, and the inner side walls of the arc-shaped pieces are fixedly connected with rotating stirring blades.

5. The ultrasonic extraction device of the total sophora alopecuroides lye as claimed in claim 1, wherein the output end of the ultrasonic extractor is connected with a vibration rod, a spiral vibration plate is vertically arranged in the extraction bottle, and the vibration rod penetrates into the extraction bottle and is connected with the spiral vibration plate.

6. The ultrasonic extraction device of the total sophora alopecuroide lye as claimed in claim 1, wherein the bottom of the extraction bottle is provided with a liquid outlet pipe, and the liquid outlet pipe is provided with a liquid outlet valve.