CN214041002U - Observable micro-nano mechanical testing device - Google Patents

Observable micro-nano mechanical testing device Download PDF

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CN214041002U
CN214041002U CN202023234288.9U CN202023234288U CN214041002U CN 214041002 U CN214041002 U CN 214041002U CN 202023234288 U CN202023234288 U CN 202023234288U CN 214041002 U CN214041002 U CN 214041002U
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马增胜
孙坤
周益春
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Xiangtan University
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Xiangtan University
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Abstract

The utility model discloses a observable micro-nano mechanics testing device, relating to the technical field of precise scientific instruments; the device comprises a supporting component, a driving component, a carrying component and an imaging component; the driving assembly and the imaging assembly are respectively vertically arranged on the supporting assembly, the carrying assembly is horizontally arranged on the supporting assembly, and the carrying assembly is positioned below the driving assembly and the imaging assembly; the carrying assembly is used for carrying a sample and realizing the movement of the sample; the driving assembly is used for driving the pressure head to apply load on the sample and enable the sample to generate indentation; the imaging assembly is used to observe and analyze indentations on a test specimen. The utility model discloses a micro-nano mechanics testing arrangement of observable type can effectively measure the mechanical properties parameter of material, simple structure, and the measuring result precision is high.

Description

Observable micro-nano mechanical testing device
Technical Field
The utility model relates to an accurate scientific instrument technical field especially relates to a micro-nano mechanics testing arrangement of observable type.
Background
With the development of science and technology, the pressing-in experiment of materials at the microscopic scale has gradually become a standard experiment for researching the mechanical properties of the materials, and is widely applied to the fields of material surface engineering, microelectronic devices, metal ceramic testing, semiconductor research and development, biological engineering, medical materials and the like. Compared with the traditional mechanical property test means, the micro-indentation test has the remarkable characteristics of simple operation, simple sample preparation, rich test contents, micro-damage and the like, and is widely used for testing the characteristics of hardness, modulus, stress-strain curve, fracture toughness, creep relaxation and the like of materials. Therefore, it is a direction to be urgently needed to provide an effective method and an effective instrument for testing mechanical property parameters of materials by researching observable micro-nano mechanical testing equipment.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing a micro-nano mechanics testing arrangement of observable type to solve the problem that above-mentioned prior art exists, can effectively measure the mechanical properties parameter of material.
In order to achieve the above object, the utility model provides a following scheme:
the utility model provides a observable micro-nano mechanical testing device, which comprises a supporting component, a driving component, a carrying component and an imaging component; the driving assembly and the imaging assembly are respectively vertically arranged on the supporting assembly, the carrying assembly is horizontally arranged on the supporting assembly, and the carrying assembly is positioned below the driving assembly and the imaging assembly; the carrying assembly is used for carrying a sample and realizing the movement of the sample; the driving assembly is used for driving the pressure head to apply load on the sample and enable the sample to generate indentation; the imaging assembly is used to observe and analyze indentations on a test specimen.
Optionally, the support assembly includes a support bottom plate and a support back plate, the support bottom plate is horizontally disposed, and the support back plate is vertically and fixedly disposed on one side of the top of the support bottom plate; the driving assembly and the imaging assembly are arranged on the supporting back plate, and the carrying assembly is arranged on the supporting bottom plate.
Optionally, the object carrying assembly comprises an X-axis precision sliding table, a sliding block is horizontally arranged on the X-axis precision sliding table in a sliding manner, an adapter plate is fixedly mounted at the top of the sliding block, a clamping table is fixedly connected to the top of the adapter plate, and the clamping table is used for clamping a sample; the bottom of the X-axis precision sliding table is fixedly arranged on the supporting bottom plate.
Optionally, the driving assembly includes a supporting module, a precise pressing device, a load detecting module and a displacement detecting module; the support module comprises a cantilever beam and a grating fixing frame, the grating fixing frame is fixedly arranged at the lower part of the horizontally arranged cantilever beam, the precise pressing device is fixedly connected to the cantilever beam, an output shaft of the precise pressing device is vertically arranged downwards, the load detection module is fixedly connected to the lower end of the output shaft of the precise pressing device in a threaded manner, the displacement detection module is fixedly connected to the grating fixing frame, the lower end of the load detection module is fixedly connected with a pressure head fixing device, and the pressure head fixing device is used for fixedly installing a pressure head; one end of the cantilever beam is fixedly connected with the support back plate.
Optionally, the imaging assembly comprises a microscope, a microscope support and a Z-axis sliding table; the microscope is fixed to the top of the microscope support through jackscrews, one side of the bottom of the microscope support is fixed to the Z-axis sliding table through bolts, and the Z-axis sliding table is fixed to the supporting back plate through bolts.
Optionally, the precise pressing device is a linear stepping motor, and the precise pressing device is fixedly connected to the cantilever beam through a bolt; the load detection module is a force sensor, the top of the force sensor is connected with the precise pressing device through an adapter, and the bottom of the force sensor is connected with the pressure head fixer; the displacement detection module comprises a grating ruler and a grating reading head, a long circular hole is formed in the grating fixing frame, the grating reading head is fixedly connected to the long circular hole of the grating fixing frame through a bolt, the grating ruler is adhered to the pressing head fixing device, the grating ruler and the grating reading head are oppositely arranged, and the grating ruler is parallel to the grating reading head.
Optionally, the microscope comprises an objective lens, a point light source, a lens barrel and a camera; the objective lens is of a turret structure, the upper part of the lens barrel is connected with the camera through threads, the lower part of the lens barrel is connected with the objective lens through threads, the lower part of the lens barrel is connected with the point light source through a jackscrew, and the middle part of the lens barrel is fixed on a microscope bracket through the jackscrew; the camera can directly transmit the image formed by the objective lens to the control system for real-time observation.
The utility model also provides an adopt above-mentioned micro-nano mechanics testing arrangement's of observable type micro-nano mechanics testing method, including following step:
(1) connecting the precise pressing device with a computer, electrically connecting the load detection module and the displacement detection module with an analog-to-digital converter acquisition card, electrically connecting the analog-to-digital converter acquisition card with the computer, and electrically connecting the X-axis precise sliding table, the Z-axis precise sliding table and the microscope with the computer respectively;
(2) a pressure head is arranged on the pressure head fixer, a sample is fixed on the carrying assembly, and the computer drives the X-axis precision sliding table to enable the sample to be positioned under the pressure head;
(3) setting parameters of a test sample and a pressure head through a computer, selecting a test loading mode, inputting loading time, load retention time and unloading time, and starting an indentation test;
(4) in the pressing process of the pressure head, when the load detection module detects the minimum response force value, the pressure head is judged to be in contact with the test sample at the moment, and the indentation test is completed according to the set control parameters and the loading, load retention and unloading time;
(5) the analog-digital converter acquisition card acquires load and displacement signals in the test process, converts the load and displacement signals into load and displacement values, and displays the load and displacement values on a computer software interface to obtain a load-displacement curve in the test process, wherein the load-displacement curve comprises a load-displacement curve in the loading process and a load-displacement curve in the unloading process;
(6) the X-axis precision sliding table is controlled by the computer to move the sample to the bottom of the microscope, then the Z-axis precision sliding table is controlled by the computer to move the microscope to a focusing position, the sample is observed, and data are transmitted to the computer.
Optionally, in step (5), the loading section and the unloading section in the load-displacement curve are represented by the following two fitting formulas:
P=Ch2
P=B(h-hp)m
wherein P is the press-in load, and C, B and m are both fitting values; the contact stiffness of a material is the slope of the indentation at the maximum load reached, i.e.:
Figure BDA0002867925370000031
contact depth h of materialcCan be used to calculate the contact area of the indenter, which is expressed as:
Figure BDA0002867925370000032
wherein ε is the indenter form factor; the hardness is a parameter of the material resisting the pressing-in of the hard object, and the formula is as follows:
Figure BDA0002867925370000041
in the formula, AcThe actual contact area of the pressure head is expressed by the following formula:
Figure BDA0002867925370000042
Ciis a fitting parameter; in order to calculate the elastic modulus of the material, the contact projected area and the contact stiffness of the pressure head need to be introduced:
Figure BDA0002867925370000043
wherein beta is the indenter profile parameter, ErIn terms of reduced modulus, the value is determined from the modulus of elasticity of the material and indentor and PoissonAnd (3) determining:
Figure BDA0002867925370000044
in the formula, E is the elastic modulus of the material to be measured, v is the Poisson's ratio, EiIs the modulus of elasticity, v, of the indenteriIs the poisson's ratio of the indenter; according to the formula, the elastic modulus of the tested material is as follows:
Figure BDA0002867925370000045
at this time, the hardness and elastic modulus of the material can be determined.
Optionally, in step (6), the crack length c of the film material is recorded, and then the residual stress and fracture toughness of the material can be calculated:
Figure BDA0002867925370000046
Figure BDA0002867925370000047
the toughness of the surface fracture (CRI),
Figure BDA0002867925370000048
σr-residual stress, GPa; p-indentation load, mN; c-half crack length, μm; h ist-film thickness, μm; χ -a constant related to indenter and coating properties;
the above formula variant yields:
Figure BDA0002867925370000051
handle
Figure BDA0002867925370000052
Is regarded as c-1/2As a function of (a) or (b),obtaining the slope and intercept of a straight line fitting equation by a linear fitting method, wherein
Figure BDA0002867925370000053
Delta is a parameter related to the geometry of the indenter, E and H are the young's modulus and hardness of the coating respectively,
Figure BDA0002867925370000054
is the intercept of a linear fit equation,
Figure BDA0002867925370000055
the method is characterized in that the method is a slope of a linear fitting equation, when the thickness of a coating is known, the residual stress of a material can be obtained through the slope, and the residual stress is substituted into an intercept to obtain the surface fracture toughness of the coating;
Figure BDA0002867925370000056
in the formula (I), the compound is shown in the specification,
Figure BDA0002867925370000057
the fracture toughness of the interface, is,
Figure BDA0002867925370000058
σr-residual stress, GPa; p-indentation load, mN; c-half crack length, μm; χ -a constant related to indenter and coating properties;
by conversion to obtain
Figure BDA0002867925370000059
Handle
Figure BDA00028679253700000510
Is regarded as c1/2The slope and intercept of a straight line fitting equation are obtained through a linear fitting method; wherein
Figure BDA0002867925370000061
δ is a parameter related to the indenter geometry, E and H are the young's modulus and hardness of the coating, respectively;
Figure BDA0002867925370000062
is the intercept of a linear fit equation,
Figure BDA0002867925370000063
the residual stress of the material and the fracture toughness of the material interface can be obtained by linear fitting the slope of the equation.
The utility model discloses for prior art gain following technological effect:
the utility model has simple integral structure and high precision of measuring results; the driving assembly is used for driving the pressure head to apply a load on the sample to generate an indentation; the carrying assembly is used for carrying a sample and realizing the movement of the sample; the imaging component is used for observing the indentation on the sample and analyzing to obtain various mechanical parameters; the whole cooperation can realize the movement, indentation generation by loading, observation, analysis and the like of the sample without transferring the sample, and the working efficiency is high; the long round hole is formed in the grating fixing frame, the bolt penetrates through the long round hole to be in threaded connection with the grating reading head, the distance between the grating reading head and the grating ruler is convenient to adjust, and the observable range is large; the objective lens is of a turret structure, observation can be performed under different multiplying powers, high multiplying power and a large visual field are achieved, and the camera can directly transmit images formed by the objective lens to a computer for real-time observation.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.
FIG. 1 is a front view of an observable micro-nano mechanical testing device;
FIG. 2 is an isometric view of an observable micro-nano mechanical testing device;
FIG. 3 is a basic structure diagram of an observable micro-nano mechanical testing device;
FIG. 4 is a structural diagram of a supporting part of the observable micro-nano mechanical testing device;
FIG. 5 is a structural diagram of an object carrying assembly of the observable micro-nano mechanical testing device;
FIG. 6 is a structural diagram of a drive assembly of the observable micro-nano mechanical testing device;
FIG. 7 is a structural diagram of an imaging assembly of an observable micro-nano mechanical testing device;
FIG. 8 is a cross-sectional view of loading and unloading by the observation method of the present invention;
FIG. 9 is a load-displacement curve chart of an observation method according to the present invention;
description of reference numerals: 100. the micro-nano mechanical testing device comprises an observable micro-nano mechanical testing device, a supporting assembly, a driving assembly, a carrying assembly, a 4 imaging assembly, a 5 supporting back plate, a 6 supporting bottom plate, a 7X-axis precise sliding table, an 8 adapter plate, a 9 clamping table, a 10 cantilever beam, a 11 grating fixing frame, a 12 precise pressing device, a 13 adapter, a 14 force sensor, a 15 pressure head fixing device, a 16 grating reading head, a 17 pressure head, a 18Z-axis sliding table, a 19 microscope support, a 20 microscope, a 21 objective lens, a 22 point light source, a 23 lens cone, a 24 camera, a 25 grating ruler and a 26 sliding block.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
The utility model aims at providing a micro-nano mechanics testing arrangement of observable type to solve the problem that above-mentioned prior art exists, can effectively measure the mechanical properties parameter of material.
In order to make the above objects, features and advantages of the present invention more comprehensible, the present invention is described in detail with reference to the accompanying drawings and the detailed description.
The utility model provides a observable micro-nano mechanics testing device 100, as shown in figures 1-9, comprising a supporting component 1, a driving component 2, a carrying component 3 and an imaging component 4; the driving assembly 2 and the imaging assembly 4 are respectively vertically arranged on the supporting assembly 1, the carrying assembly 3 is horizontally arranged on the supporting assembly 1, and the carrying assembly 3 is positioned below the driving assembly 2 and the imaging assembly 4; the object carrying assembly 3 is used for carrying a sample and realizing the movement of the sample; the driving assembly 2 is used for driving the pressure head to apply load on the sample and make the sample generate indentation; the imaging assembly 4 is used to observe and analyze the indentations on the test sample.
Preferably, the supporting assembly 1 comprises a supporting bottom plate 6 and a supporting back plate 5, the supporting bottom plate 6 is horizontally arranged, the supporting back plate 5 is fixedly and vertically arranged on one side of the top of the supporting bottom plate 6, and the supporting bottom plate and the supporting back plate are connected through threads and are mainly used for supporting the indentation, the object stage and the imaging assembly 4; the driving assembly 2 and the imaging assembly 4 are arranged on the supporting backboard 5, and the carrying assembly 3 is arranged on the supporting bottom board 6. The supporting bottom plate 6 is preferably made of granite, and granite is lighter than steel and heavier than aluminum, so that the supporting bottom plate is a material which is commonly applied at present. Granite has the main advantages of small deformation, good stability, no rusting, easy plane processing and easy realization of higher planeness than cast iron. The internal damping coefficient is 15 times larger than that of steel, and the shock absorption effect is good. Non-conducting, diamagnetic, can not produce adhesion or magnetization with metal. The supporting back plate 5 is preferably made of steel, is easy to process, has excellent bearing capacity, can effectively increase the weight, and improves the stability of the instrument. The object carrying assembly 3 comprises an X-axis precision sliding table 7, a sliding block 26 is horizontally arranged on the X-axis precision sliding table 7 in a sliding mode, an adapter plate 8 is fixedly arranged at the top of the sliding block 26, a clamping table 9 is fixedly connected to the top of the adapter plate 8, and the clamping table 9 is used for clamping a sample; the bottom of the X-axis precision sliding table 7 is fixedly arranged on the supporting bottom plate 6. The driving assembly 2 comprises a supporting module, a precise pressing device 12, a load detection module and a displacement detection module; the supporting module comprises a cantilever beam 10 and a grating fixing frame 11, the grating fixing frame 11 is fixedly installed at the lower part of the cantilever beam 10 which is horizontally arranged, a precise pressing device 12 is fixedly connected onto the cantilever beam 10, an output shaft of the precise pressing device 12 is vertically arranged downwards, a load detection module is fixedly connected to the lower end of the output shaft of the precise pressing device 12 in a threaded mode, a displacement detection module is fixedly connected onto the grating fixing frame 11, a pressure head fixing device 15 is fixedly connected to the lower end of the load detection module, and the pressure head fixing device 15 is used for fixedly installing a pressure head 17; one end of the cantilever beam 10 is fixedly connected with the support back plate 5. The cantilever 10 is preferably made of steel, and has strong bearing capacity and is not easy to deform. The top of the grating fixing frame is connected with a stepping motor by screw threads, and the bottom of the grating fixing frame is connected with a grating fixing frame 11. The imaging assembly 4 comprises a microscope, a microscope stand and a Z-axis sliding table 18; the microscope is fixed at the top of the microscope support by adopting a jackscrew, one side of the bottom of the microscope support is fixed on the Z-axis sliding table 18 through a bolt, and the Z-axis sliding table 18 is fixed on the supporting back plate 5 through a bolt. The Z-axis precision sliding table can drive the video microscope to complete focusing through the microscope support.
Specifically, the precise pressing device 12 is a linear stepping motor, and the precise pressing device 12 is fixedly connected to the cantilever beam 10 through a bolt; the load detection module is a force sensor 14, the top of the force sensor 14 is connected with the precision pressing device 12 through an adapter 13, and the bottom of the force sensor 14 is connected with a pressing head fixer 15; the displacement detection module comprises a grating ruler 25 and a grating reading head 16, a long circular hole is formed in the grating fixing frame 11, the grating reading head is fixedly connected to the long circular hole of the grating fixing frame 11 through a bolt, the grating ruler 25 is adhered to the pressing head fixing device 15, the grating ruler and the grating reading head 16 are oppositely arranged, the grating ruler 25 is parallel to the grating reading head 16, and the distance between the grating reading head 16 and the grating ruler 25 can be adjusted conveniently. The microscope 20 is a video microscope and comprises an objective lens 21, a point light source 22, a lens cone 23 and a camera 24; the objective lens 21 is of a turret structure, observation can be carried out under different multiplying powers, and coexistence of high multiplying power and a large visual field is realized; the upper part of the lens cone 23 is connected with the camera 24 through threads, the lower part of the lens cone 23 is connected with the objective lens 21 through threads, the lower part of the lens cone 23 is connected with the point light source 22 through a jackscrew, and the middle part of the lens cone 23 is fixed on the microscope bracket 19 through the jackscrew; the camera 24 can directly transmit the image formed by the objective lens 21 to a control system such as a computer, and perform real-time observation.
The utility model also provides an adopt above-mentioned micro-nano mechanics testing arrangement's of observable type micro-nano mechanics testing method, including following step:
(1) the precise pressing device 12 is connected with a computer, the load detection module and the displacement detection module are electrically connected with an analog-digital converter acquisition card, the analog-digital converter acquisition card is electrically connected with the computer, and the X-axis precise sliding table 7, the Z-axis precise sliding table and the microscope are respectively and electrically connected with the computer;
(2) a pressure head 17 is arranged on the pressure head fixer 15, a sample is fixed on the carrying assembly 3, and the computer drives the X-axis precision sliding table 7 to enable the sample to be positioned under the pressure head 17;
(3) setting parameters of a test sample and a pressure head, including a Poisson ratio of a sample material, a thickness of the sample material, a thickness of a film, a type of the pressure head 17 and a material parameter of the pressure head 17, selecting a test loading mode as a load control mode or a displacement control mode, setting corresponding control parameters as a maximum loading load value or a maximum loaded displacement value, inputting loading time, load retention time and unloading time, and starting an indentation test;
(4) in the pressing process of the pressure head, when the load detection module detects the minimum response force value, the pressure head 17 is judged to be in contact with the test sample at the moment, and the indentation test is completed according to the set control parameters and the loading, load retention and unloading time;
(5) the analog-digital converter acquisition card acquires load and displacement signals in the test process, converts the load and displacement signals into load and displacement values, and displays the load and displacement values on a computer software interface to obtain a load-displacement curve in the test process, wherein the load-displacement curve comprises a load-displacement curve in the loading process and a load-displacement curve in the unloading process;
(6) the X-axis precision sliding table 7 is controlled by the computer to move the sample to the bottom of the microscope, then the Z-axis precision sliding table is controlled by the computer to move the microscope to a focusing position, the sample is observed, and data are transmitted to the computer. As shown in fig. 8, which is a comparative schematic view of the indentation surface after unloading and the indentation surface at the time of maximum load and the initial surface, fig. 9 is a load-displacement graph of the loading process and the unloading process.
Optionally, in step (5), the loading section and the unloading section in the load-displacement curve are represented by the following two fitting formulas:
P=Ch2
P=B(h-hp)m
wherein P is the press-in load, and C, B and m are both fitting values; for the data of the unloading section, the utility model takes 20% -60% of the data of the unloading section to carry out fitting, and obtains the formula of the unloading section with better correlation; the contact stiffness of a material is the slope of the indentation at the maximum load reached, i.e.:
Figure BDA0002867925370000101
contact depth h of materialcCan be used to calculate the contact area of the indenter, which is expressed as:
Figure BDA0002867925370000102
wherein ε is the indenter form factor; for Berkovich indenters, Vickers indenters, and ball indenters, the ε is 0.75; whereas for a Rockwell cone indenter, ε is 0.72, and for a flat indenter, ε is 1. According to the traditional elastic-plastic theory, the hardness is a parameter of the material resisting the pressing-in of the hard object, and the formula is as follows:
Figure BDA0002867925370000103
in the formula, AcThe value is one of important influence factors of the experimental test accuracy for the actual contact area of the pressure head, and the formula is as follows:
Figure BDA0002867925370000104
Cifor fitting parameters, obtained by testing, of Rockwell indenter, Bohr indenter and Vickers indenterDesign area function as A-24.5 h2(ii) a In order to calculate the elastic modulus of the material, the contact projected area and the contact stiffness of the pressure head need to be introduced:
Figure BDA0002867925370000105
wherein beta is an indenter morphology parameter, beta is 1.034 and 1.012 for Berkovich indenters and Vickers indenters, and beta is 1 when the indenter is a circular indenter. ErThe value of the reduced modulus is determined by the elastic modulus and Poisson's ratio of the material and the indenter:
Figure BDA0002867925370000106
in the formula, E is the elastic modulus of the material to be measured, v is the Poisson's ratio, EiIs the modulus of elasticity, v, of the indenteriIs the poisson's ratio of the indenter; the typical indenter material is diamond, which has a modulus of elasticity and a poisson ratio of 1141 GPa and 0.07, respectively. According to the formula, the elastic modulus of the tested material is as follows:
Figure BDA0002867925370000111
at this time, the hardness and elastic modulus of the material can be determined.
Optionally, in step (6), the crack length c of the film material is recorded, and then the residual stress and fracture toughness of the material can be calculated:
Figure BDA0002867925370000112
Figure BDA0002867925370000113
the toughness of the surface fracture (CRI),
Figure BDA0002867925370000114
σr-residual stress, GPa; p-indentation load, mN; c-half crack length, μm; h ist-film thickness, μm; x-a constant related to indenter and coating properties;
the above formula variant yields:
Figure BDA0002867925370000115
handle
Figure BDA0002867925370000116
Is regarded as c-1/2By a linear fitting method, obtaining the slope and intercept of a straight line fitting equation, wherein
Figure BDA0002867925370000117
δ is a parameter related to the indenter geometry, δ being 0.016 for vickers indenter. E and H are the young's modulus and hardness of the coating respectively,
Figure BDA0002867925370000121
is the intercept of a linear fit equation,
Figure BDA0002867925370000122
the method is characterized in that the method is a slope of a linear fitting equation, when the thickness of a coating is known, the residual stress of a material can be obtained through the slope, and the residual stress is substituted into an intercept to obtain the surface fracture toughness of the coating;
Figure BDA0002867925370000123
in the formula (I), the compound is shown in the specification,
Figure BDA0002867925370000124
the fracture toughness of the interface, is,
Figure BDA0002867925370000125
σr-residueStress, GPa; p-indentation load, mN; c-half crack length, μm; x-a constant related to indenter and coating properties;
by conversion to obtain
Figure BDA0002867925370000126
Handle
Figure BDA0002867925370000127
Is regarded as c1/2The slope and intercept of a straight line fitting equation are obtained through a linear fitting method; wherein
Figure BDA0002867925370000128
δ is a parameter related to the indenter geometry, δ being 0.016 for vickers indenter, E and H being the young's modulus and hardness of the coating, respectively;
Figure BDA0002867925370000129
is the intercept of a linear fit equation,
Figure BDA00028679253700001210
the residual stress of the material and the fracture toughness of the material interface can be obtained by linear fitting the slope of the equation.
The utility model discloses a concrete example is applied to explain the principle and the implementation mode of the utility model, and the explanation of the above example is only used to help understand the method and the core idea of the utility model; meanwhile, for the general technical personnel in the field, according to the idea of the present invention, there are changes in the concrete implementation and the application scope. In summary, the content of the present specification should not be construed as a limitation of the present invention.

Claims (7)

1. The utility model provides a micro-nano mechanics testing arrangement of observable type which characterized in that: the device comprises a supporting component, a driving component, a carrying component and an imaging component; the driving assembly and the imaging assembly are respectively vertically arranged on the supporting assembly, the carrying assembly is horizontally arranged on the supporting assembly, and the carrying assembly is positioned below the driving assembly and the imaging assembly; the carrying assembly is used for carrying a sample and realizing the movement of the sample; the driving assembly is used for driving the pressure head to apply load on the sample and enable the sample to generate indentation; the imaging assembly is used to observe and analyze indentations on a test specimen.
2. The observable micro-nano mechanical testing device of claim 1, wherein: the supporting assembly comprises a supporting bottom plate and a supporting back plate, the supporting bottom plate is horizontally arranged, and the supporting back plate is fixedly and vertically arranged on one side of the top of the supporting bottom plate; the driving assembly and the imaging assembly are arranged on the supporting back plate, and the carrying assembly is arranged on the supporting bottom plate.
3. The observable micro-nano mechanical testing device of claim 2, wherein: the carrying assembly comprises an X-axis precise sliding table, a sliding block is horizontally arranged on the X-axis precise sliding table in a sliding manner, a transfer plate is fixedly arranged at the top of the sliding block, and a clamping table is fixedly connected to the top of the transfer plate and used for clamping a sample; the bottom of the X-axis precision sliding table is fixedly arranged on the supporting bottom plate.
4. The observable micro-nano mechanical testing device of claim 2, wherein: the driving assembly comprises a supporting module, a precise pressing device, a load detection module and a displacement detection module; the support module comprises a cantilever beam and a grating fixing frame, the grating fixing frame is fixedly arranged at the lower part of the horizontally arranged cantilever beam, the precise pressing device is fixedly connected to the cantilever beam, an output shaft of the precise pressing device is vertically arranged downwards, the load detection module is fixedly connected to the lower end of the output shaft of the precise pressing device in a threaded manner, the displacement detection module is fixedly connected to the grating fixing frame, the lower end of the load detection module is fixedly connected with a pressure head fixing device, and the pressure head fixing device is used for fixedly installing a pressure head; one end of the cantilever beam is fixedly connected with the support back plate.
5. The observable micro-nano mechanical testing device of claim 2, wherein: the imaging assembly comprises a microscope, a microscope bracket and a Z-axis sliding table; the microscope is fixed to the top of the microscope support through jackscrews, one side of the bottom of the microscope support is fixed to the Z-axis sliding table through bolts, and the Z-axis sliding table is fixed to the supporting back plate through bolts.
6. The observable micro-nano mechanical testing device of claim 4, wherein: the precise pressing device is a linear stepping motor and is fixedly connected to the cantilever beam through a bolt; the load detection module is a force sensor, the top of the force sensor is connected with the precise pressing device through an adapter, and the bottom of the force sensor is connected with the pressure head fixer; the displacement detection module comprises a grating ruler and a grating reading head, a long circular hole is formed in the grating fixing frame, the grating reading head is fixedly connected to the long circular hole of the grating fixing frame through a bolt, the grating ruler is adhered to the pressing head fixing device, the grating ruler and the grating reading head are oppositely arranged, and the grating ruler is parallel to the grating reading head.
7. The observable micro-nano mechanical testing device of claim 5, wherein: the microscope comprises an objective lens, a point light source, a lens barrel and a camera; the objective lens is of a turret structure, the upper part of the lens barrel is connected with the camera through threads, the lower part of the lens barrel is connected with the objective lens through threads, the lower part of the lens barrel is connected with the point light source through a jackscrew, and the middle part of the lens barrel is fixed on a microscope bracket through the jackscrew; the camera can directly transmit the image formed by the objective lens to the control system for real-time observation.
CN202023234288.9U 2020-12-29 2020-12-29 Observable micro-nano mechanical testing device Active CN214041002U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112611662A (en) * 2020-12-29 2021-04-06 湘潭大学 Observable micro-nano mechanical testing device and method
CN114414374A (en) * 2022-01-21 2022-04-29 矿冶科技集团有限公司 Superfine ceramic powder crushing strength testing equipment and method
CN115931548A (en) * 2022-10-13 2023-04-07 荣梓华 Young modulus determination method and device and electronic equipment

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112611662A (en) * 2020-12-29 2021-04-06 湘潭大学 Observable micro-nano mechanical testing device and method
CN112611662B (en) * 2020-12-29 2024-10-01 湘潭大学 Observable micro-nano mechanical testing device and testing method
CN114414374A (en) * 2022-01-21 2022-04-29 矿冶科技集团有限公司 Superfine ceramic powder crushing strength testing equipment and method
CN115931548A (en) * 2022-10-13 2023-04-07 荣梓华 Young modulus determination method and device and electronic equipment

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