CN213852117U - A chromatography equipment for ginseng stem leaf production - Google Patents

A chromatography equipment for ginseng stem leaf production Download PDF

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Publication number
CN213852117U
CN213852117U CN202022731621.0U CN202022731621U CN213852117U CN 213852117 U CN213852117 U CN 213852117U CN 202022731621 U CN202022731621 U CN 202022731621U CN 213852117 U CN213852117 U CN 213852117U
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chromatography
ginseng
bottom end
stem leaf
feeding device
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CN202022731621.0U
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周凯
蔡冬青
季亚飞
杨小宏
杨建莉
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Yangling Dailyhealth Bio Engineering Technology Co ltd
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Yangling Dailyhealth Bio Engineering Technology Co ltd
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Abstract

The utility model provides a pair of chromatography equipment for ginseng stem leaf production, including frame, stand, pan feeding device, processing apparatus, drawing liquid device and chromatography post, frame bottom outer end is equipped with the stand respectively, frame left side wall is equipped with automatically controlled panel, the frame upper left side is equipped with the pan feeding device, pan feeding device bottom is equipped with processing apparatus, the processing apparatus right side is equipped with the drawing liquid device, drawing liquid device bottom is equipped with the chromatography post. The utility model discloses on locating same device with ginseng pre treatment facilities and chromatography equipment, need not pass through other processing procedure, can once only accomplish ginseng stem leaf's processing and chromatography extraction work, the ginseng raw materials is further taken off the incomplete, the chromatography is dry again after the purification treatment obtains ginseng stem leaf total saponin to the broken branch and leaf of ginseng by multilayer processing device in getting into processing apparatus after the arrangement of pan feeding device to improve ginseng stem leaf's chromatography extraction efficiency and degree of automation.

Description

A chromatography equipment for ginseng stem leaf production
Technical Field
The utility model relates to a chromatography equipment design technical field, in particular to a chromatography equipment for ginseng stem leaf production.
Background
Ginseng, a plant of the genus Panax of the family Araliaceae, is a traditional and famous Chinese medicinal material, and its name is recorded in Shen nong Ben Cao Jing (Shen nong's herbal medicine), which is called Ginseng, sweet in taste, slightly cold, mainly tonifying the five internal organs, calming the mind, calming the soul, stopping palpitation, eliminating pathogenic qi, improving eyesight, developing heart, benefiting intelligence, losing weight and prolonging life after long-term use. The ginseng contains various ginsenosides, volatile oil, amino acids, trace elements, organic acids, saccharides, cellulose and other components, wherein the ginsenosides are the main effective components of the ginseng and are the main indexes for evaluating the ginseng. The current ginseng stem leaf production chromatography equipment is mainly obtained by extracting with water or moderate ethanol and then refining through a macroporous resin column. Most of the existing pesticide residue treatment methods mainly adopt carbon dioxide supercritical treatment, solvent extraction and resin adsorption. The method causes certain environmental protection pressure due to the use of a large amount of water, macroporous resin and solvent. Therefore, a chromatography device for ginseng stem leaf production is provided.
SUMMERY OF THE UTILITY MODEL
The utility model aims to solve the problem of providing a chromatography device for ginseng stem leaf production, which solves the problems of environmental pollution and low chromatography efficiency of the chromatography of the ginseng stem leaf in the prior art; so as to achieve the purposes of improving the efficiency of chromatographic extraction of the ginseng stem leaves, reducing the environmental pollution caused by chromatography and improving the automation degree of the production of the ginseng stem leaves.
The utility model provides a technical scheme that above-mentioned technical problem adopted is: the utility model provides a chromatography equipment for ginseng stem leaf production, includes frame, stand, pan feeding device, processing apparatus, drawing liquid device and chromatography post, frame bottom outer end is equipped with the stand respectively, frame left side wall is equipped with automatically controlled panel, the frame upper left side is equipped with the pan feeding device, pan feeding device bottom is equipped with processing apparatus, the processing apparatus right side is equipped with the drawing liquid device, drawing liquid device bottom is equipped with the chromatography post.
As a preferred embodiment of the present invention, wherein: the feeding device is characterized in that a bearing seat is arranged in the center of the top end of the feeding device, a rotating shaft is arranged at the bottom end of the bearing seat, a plurality of spiral cutting knives are arranged on the rotating shaft, a rotating motor is arranged at the bottom end of the rotating shaft, and a damping seat is arranged at the bottom end of the edge of the outer end of the feeding device.
As a preferred embodiment of the present invention, wherein: the bottom end of the feeding device is provided with a material collecting hopper, a first reaction barrel is arranged below the material collecting hopper, a second reaction barrel is arranged on the right side of the first reaction barrel through a communicating pipeline, and a third reaction barrel is arranged on the right side of the second reaction barrel through a communicating pipeline.
As a preferred embodiment of the present invention, wherein: the bottom end of the liquid pumping device is provided with a membrane separator, the three top ends of the reaction cylinder are provided with communicating pipelines, the communicating pipelines are connected into the membrane separator, the left side of the liquid pumping device is provided with a pressure pump, the right side of the liquid pumping device is provided with a liquid conveying pipe, and the bottom end of the liquid conveying pipe is connected into the chromatographic column.
As a preferred embodiment of the present invention, wherein: the utility model discloses a chromatography column, including chromatography column, drain pipe, backflow pipe top, drain pipe below, drain pipe bottom, drainage funnel below, the chromatography column left side is equipped with chromatography liquid injection end, the chromatography column bottom is equipped with the fluid-discharge tube, the fluid-discharge tube bottom is equipped with the waste liquid bottle, the fluid-discharge tube top is equipped with the back flow, the back flow below is equipped with the drain pipe, the drain pipe bottom is equipped with drainage funnel, the drainage funnel below is equipped with three way valve, the access of a logical interface at three way valve top drainage funnel, three way valve is equipped with the shunt tubes in the other two-way interface, the shunt tubes below is equipped with aggregate unit two.
Further, a connecting pipe is arranged at the top end of the reaction cylinder, the connecting pipe extends into the collecting hopper, a cylinder plug I is arranged at the top end of the reaction cylinder, a switch brake I is arranged above the cylinder plug I, two communicating buckles are respectively arranged at the left end and the right end of the switch brake I, and the connecting pipes are respectively controlled by the communicating buckles.
Further, two tops of reaction cylinder are equipped with a section of thick bamboo stopper two, two tops of section of thick bamboo stopper are equipped with switch floodgate two, three tops of reaction cylinder are equipped with a section of thick bamboo stopper three, three tops of section of thick bamboo stopper are equipped with switch floodgate three, the connected mode that detains with communicating pipe with switch floodgate one is unanimous to the intercommunication that two tops of switch floodgate set up with the connected mode of communicating pipe with switch floodgate one is unanimous.
Further, the bottom end of the treatment device is provided with a drainage tube, the bottom end of the drainage tube is provided with a waste valve, and the bottom end of the waste valve is provided with a first material collecting device.
Further, the second collecting device comprises a first collecting bottle and a second collecting bottle, and the top ends of the first collecting bottle and the second collecting bottle are opposite to the bottoms of the shunt tubes.
Further, waste liquid bottle top is equipped with filter equipment, establish to filtration membrane on the filter equipment top, it is equipped with a plurality of absorption pieces to filter the membrane, the filtration membrane bottom is equipped with the osmotic membrane, the osmotic membrane bottom is equipped with the filter screen, filter equipment central authorities are equipped with the through-hole, the through-hole is just right the fluid-discharge tube bottom.
Compared with the prior art, the technical scheme of the utility model have following advantage:
1. the utility model provides a chromatographic equipment for ginseng stem leaf production, locate same device with ginseng pretreatment equipment and chromatographic equipment on, need not pass through other processing procedure, can once only extract the work with the chromatography of ginseng stem leaf and accomplish, the ginseng raw materials is further taken off the incomplete, the purification treatment back chromatography drying obtains ginseng stem leaf total saponin by multilayer processing device in getting into processing apparatus after the arrangement of pan feeding device in the broken branch and leaf of ginseng.
2. The production method of the technical scheme is green and environment-friendly, has low cost compared with the existing production method, greatly reduces the usage amount of the solvent, reduces the environmental protection pressure caused by the solvent, has low pesticide residue, and is more practical, convenient and good in effect compared with the existing method for removing the pesticide residue mainly by using solvent extraction and resin adsorption.
3. According to the technical scheme, the treatment solutions with different formulas are added into each reaction cylinder of the extraction device, so that pesticide residues on ginseng stems and leaves can be removed, saponins on the ginseng stems and leaves can be purified, and the chromatography device can conveniently and quickly extract the total saponins of ginseng to the greatest extent.
Drawings
FIG. 1 is a front sectional view of the chromatographic equipment for ginseng stem leaf production of the present invention;
FIG. 2 is a schematic structural view of a ginseng stem leaf processing device of the chromatography device for ginseng stem leaf production of the present invention;
FIG. 3 is a schematic structural view of a mixed liquid treatment device of a chromatography device for ginseng stem and leaf production of the present invention;
FIG. 4 is a schematic structural diagram of a chromatography device of the chromatography device for ginseng stem leaf production of the present invention;
fig. 5 is a schematic structural diagram of the filtering device of the chromatography equipment for ginseng stem leaf production of the present invention.
Wherein: 1 is a frame, 2 is a column, 3 is an electric control panel, 4 is a feeding device, 41 is a bearing seat, 42 is a rotating motor, 43 is a rotating shaft, 44 is a spiral cutting knife, 45 is a shock absorption seat, 5 is a processing device, 51 is a reaction cylinder I, 52 is a reaction cylinder II, 53 is a reaction cylinder III, 54 is a switch gate I, 55 is a switch gate II, 56 is a switch gate III, 57 is a drainage tube, 58 is a waste material valve, 6 is a liquid pumping device, 61 is a pressure pump, 62 is a liquid conveying tube, 63 is a membrane separator, 64 is a chromatographic liquid injection end, 7 is a chromatographic column, 71 is a return tube, 72 is a liquid discharge tube, 73 is a waste liquid bottle, 731 is a filtering membrane, 732 is an adsorption block, 733 is a permeable membrane, 734 is a through hole, 735 is a filtering screen, 74 is a liquid outlet tube, 75 is a drainage funnel, 76 is a three-way valve, 77 is a shunt tube, 8 is a first collecting device, 9 is a second collecting device, 91 is a first liquid collecting bottle, And 92 is a second liquid collecting bottle.
Detailed Description
The following detailed description of the embodiments of the present invention is provided with reference to the accompanying drawings and examples. The following examples are intended to illustrate the invention, but are not intended to limit the scope of the invention.
Referring to fig. 1-5, the utility model provides a chromatography equipment for ginseng stem leaf production, including frame 1, stand 2, pan feeding device 4, processing apparatus 5, liquid extraction device 6 and chromatography post 7, the outer end of the frame 1 bottom is equipped with stand 2 respectively, the frame 1 left side wall is equipped with electrical control panel 3, the frame 1 upper left side is equipped with pan feeding device 4, the pan feeding device 4 bottom is equipped with processing apparatus 5, the processing apparatus 5 right side is equipped with liquid extraction device 6, the liquid extraction device 6 bottom is equipped with chromatography post 7, the stand 2 bottom is equipped with the installation device, stand 2 is fixed on the ground through the installation device, the stand 2 bottom is equipped with a plurality of damping springs, can slow down the influence of chromatography device work vibrations to the installation ground, electrical control device 3 controls the work of the electric power part of the chromatography device, the work process and efficiency of the adjustable chromatography operation, ginseng stem leaf raw materials enter into processing apparatus 5 after being processed and mixed by pan feeding device 4, after the purification treatment by the treatment device 5, the ginseng saponin is pumped into the chromatographic column 7 through the liquid pumping device 6, and the concentration and drying treatment are carried out after the ginsenoside is decomposed by the chromatographic column 7.
Referring to fig. 2, the bearing seat 41 is established to pan feeding device 4 top central authorities, the bearing seat 41 bottom is equipped with pivot 43, be equipped with a plurality of heliciform cutting knife 44 on the pivot 43, pivot 43 bottom is equipped with rotation motor 42, 4 outer end border bottoms of pan feeding device are equipped with shock mount 45, pour the ginseng stem leaf that has cleaned into pan feeding device 4 rotation motor 42 and rotate, pivot 43 drives heliciform cutting knife 44 and cuts up the back with the ginseng fast, add specific solution in the pan feeding device 4, heliciform cutting knife 44 rotates fast and mixes liquid and ginseng garrulous leaf, it carries out preliminary treatment to ginseng garrulous leaf to be convenient for it flows into processing apparatus 5.
The bottom end of the feeding device 4 is provided with a collecting hopper, a first reaction barrel 51 is arranged below the collecting hopper, a second reaction barrel 52 is arranged on the right side of the first reaction barrel 51 through a communicating pipeline, a third reaction barrel 53 is arranged on the right side of the second reaction barrel 52 through a communicating pipeline, a mixed liquor of ginseng stems and leaves enters the first reaction barrel 51 through the collecting hopper, a water-containing alcohol solution is arranged in the first reaction barrel 51 and can treat pesticide residues of the ginseng stems and leaves, a low-carbon alcohol solution is arranged in the second reaction barrel 52 and can carry out residue removal treatment on the ginseng stems and leaves, and an ethanol solution with the water content of 0-40% is arranged in the third reaction barrel 53 to extract the ginseng total saponins.
Referring to fig. 3 and 4, a membrane separator 63 is arranged at the bottom end of the liquid extraction device 6, a communication pipeline is arranged at the top end of the reaction cylinder III 53 and is connected into the membrane separator 63, a pressure pump 61 is arranged at the left side of the liquid extraction device 6, a liquid conveying pipe 62 is arranged at the right side of the liquid extraction device 6, the bottom end of the liquid conveying pipe 62 is connected into the chromatographic column 7, the liquid extraction device 6 extracts the total ginsenosides in the reaction cylinder III 53 into the membrane separator 63 for stripping under the action of the pressure pump 61, and the stripped ginsenosides are conveyed into the chromatographic column 7 through the liquid conveying pipe 62 for chromatography.
The left side of the chromatographic column 7 is provided with a chromatographic liquid injection end 64, the bottom end of the chromatographic column 7 is provided with a liquid discharge pipe 72, the bottom end of the liquid discharge pipe 72 is provided with a waste liquid bottle 73, the top of the liquid discharge pipe 72 is provided with a return pipe 71, a liquid outlet pipe 74 is arranged below the return pipe 71, the bottom end of the liquid outlet pipe 74 is provided with a drainage funnel 75, a three-way valve 76 is arranged below the drainage funnel 75, a through port at the top of the three-way valve 76 is connected with the drainage funnel 75, a shunt pipe 77 is arranged in the other two-way port of the three-way valve 76, an aggregate device II 9 is arranged below the shunt pipe 77, different chromatographic liquids can be injected into the chromatographic column 7 in layers in the chromatographic liquid injection end 64, ginsenosides with different precisions can be obtained in the chromatographic column 7, and the ginsenosides with different production and use requirements can be obtained by the aggregate device II, the ginsenosides vapor after chromatography flows into the liquid outlet pipe 74, which is condensed into the liquid outlet pipe 74 and flows into the drainage funnel 75, the three-way valve 76 respectively leads into the aggregate device 9 for preservation, the ginseng stem leaf dregs which do not meet the chromatography requirement can enter a waste liquid bottle 73 through the bottom end of a liquid discharge pipe 72, and the dregs are collected and treated in a centralized way.
Referring to fig. 3, a connecting pipe is arranged at the top end of the first reaction cylinder 51, the connecting pipe extends into the material collecting hopper, a first cylinder plug is arranged at the top end of the first reaction cylinder 51, a first switch gate 54 is arranged above the first cylinder plug, two communicating buckles are respectively arranged at the left end and the right end of the first switch gate 54, the communicating buckles respectively control the connecting pipe, the first switch gate 54 is opened, namely the two connecting pipes are opened, the mixed solution of the ginseng crushed leaves enters the first reaction cylinder 51 through the connecting pipe, and the mixed solution passes through the second reaction cylinder 52 after being treated by the solution in the first reaction cylinder 51.
The second reaction cylinder 52 is provided with a second cylinder plug, the second cylinder plug is provided with a second switch gate 55 above the second cylinder plug, the third reaction cylinder 53 is provided with a third cylinder plug above the third cylinder plug, a third switch gate 56 is provided above the third cylinder plug, the connection mode of the communicating buckle arranged at the top end of the second switch gate 55 and the communicating pipe is consistent with the connection mode of the first switch gate 54, the connecting buckle arranged at the top end of the third switch gate 56 and the communicating pipe is consistent with the connection mode of the first switch gate 54, the second switch gate 55 and the third switch gate 56 are opened, the ginseng crushed leaf mixed liquid flowing into the first reaction cylinder 51 can be treated, pesticide residues in the ginseng mixed liquid are sequentially removed, residue removal treatment is further carried out, and pure ginseng total saponins are obtained by ethanol solution extraction.
The bottom end of the treatment device 5 is provided with a drainage tube 57, the bottom end of the drainage tube 57 is provided with a waste valve 58, the bottom end of the waste valve 58 is provided with a first material collecting device 8, the drainage tube 57 can discharge the treatment residual liquid in each reaction cylinder, the waste valve 58 controls the on-off collection process, waste materials in the reaction cylinders can be collected into the first material collecting device 8, unified treatment is facilitated, and environmental pollution is avoided.
The second collecting device 9 comprises a first collecting bottle 91 and a second collecting bottle 92, the top ends of the first collecting bottle 91 and the second collecting bottle 92 are opposite to the bottom of the shunt tube 77, and the drying and extracting devices can be arranged on the first collecting bottle 91 and the second collecting bottle 92, so that the ginsenoside flowing out from the bottom end of the three-way valve 76 can be collected conveniently.
Referring to fig. 5, a filtering device is arranged at the top end of the waste liquid bottle 73, a filtering membrane 731 is arranged at the top end of the filtering device, a plurality of adsorption blocks 732 are arranged on the filtering membrane 731, an osmotic membrane 733 is arranged at the bottom of the filtering membrane 731, a filtering screen 735 is arranged at the bottom end of the osmotic membrane 733, a through hole 734 is arranged in the center of the filtering device, the through hole 734 is right aligned to the bottom end of the liquid discharge pipe 72, the filtering device can isolate ginseng scraps from entering the upper end of the waste liquid bottle 73 through the filtering membrane 731 and the osmotic membrane 733, saponin steam cannot be prevented from entering the liquid discharge pipe 74, and the waste liquid can be discharged into the waste liquid bottle 73 through the through hole 734 by the liquid discharge pipe 72.
The utility model provides a chromatographic equipment for ginseng stem leaf production, locate ginseng pretreatment equipment and chromatographic equipment on unified device, need not pass through other processing procedure, can once only draw the work completion with the chromatography of ginseng stem leaf, the ginseng raw materials gets into in processing apparatus 5 after the arrangement of pan feeding device 4, add the processing solution of different formulas in each reaction cylinder of extraction element 5, can get rid of the pesticide residue of ginseng stem leaf, the saponin of purification ginseng stem leaf, the chromatographic equipment of being convenient for draws ginseng total saponin as far as furthest's fast, later obtain ginseng stem leaf total saponin via multilayer processing apparatus 5 further to the broken branch and leaf of ginseng after chromatography drying again.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, a plurality of improvements and decorations can be made without departing from the technical principle of the present invention, and these improvements and decorations should also be regarded as the protection scope of the present invention.

Claims (6)

1. A chromatography device for production of ginseng stem leaves comprises a rack (1), a stand column (2), a feeding device (4), a processing device (5), a liquid pumping device (6) and a chromatography column (7), and is characterized in that the stand column (2) is arranged at the outer end of the bottom of the rack (1) respectively, an electric control panel (3) is arranged on the left side wall of the rack (1), the feeding device (4) is arranged above the left side of the rack (1), the processing device (5) is arranged at the bottom end of the feeding device (4), the liquid pumping device (6) is arranged on the right side of the processing device (5), and the chromatography column (7) is arranged at the bottom end of the liquid pumping device (6);
a bearing seat (41) is arranged in the center of the top end of the feeding device (4), a rotating shaft (43) is arranged at the bottom end of the bearing seat (41), a plurality of spiral cutting knives (44) are arranged on the rotating shaft (43), a rotating motor (42) is arranged at the bottom end of the rotating shaft (43), and a damping seat (45) is arranged at the bottom end of the outer end edge of the feeding device (4);
the bottom end of the feeding device (4) is provided with a material collecting hopper, a first reaction cylinder (51) is arranged below the material collecting hopper, a second reaction cylinder (52) is arranged on the right side of the first reaction cylinder (51) through a communicating pipeline, and a third reaction cylinder (53) is arranged on the right side of the second reaction cylinder (52) through a communicating pipeline;
a membrane separator (63) is arranged at the bottom end of the liquid pumping device (6), a communicating pipeline is arranged at the top end of the third reaction cylinder (53), the communicating pipeline is connected into the membrane separator (63), a pressure pump (61) is arranged on the left side of the liquid pumping device (6), a liquid conveying pipe (62) is arranged on the right side of the liquid pumping device (6), and the bottom end of the liquid conveying pipe (62) is connected into the chromatographic column (7);
wherein, chromatography column (7) left side is equipped with chromatography liquid injection end (64), chromatography column (7) bottom is equipped with fluid-discharge tube (72), fluid-discharge tube (72) bottom is equipped with waste liquid bottle (73), fluid-discharge tube (72) top is equipped with back flow (71), back flow (71) below is equipped with drain pipe (74), drain pipe (74) bottom is equipped with drainage funnel (75), drainage funnel (75) below is equipped with three way valve (76), the logical interface at three way valve (76) top is inserted drainage funnel (75), be equipped with shunt tubes (77) in three way valve (76) other two logical interface, shunt tubes (77) below is equipped with aggregate unit two (9).
2. The chromatographic equipment for ginseng stem leaf production according to claim 1, wherein a connecting pipe is arranged at the top end of the first reaction cylinder (51), the connecting pipe extends into the collecting hopper, a first cylinder plug is arranged at the top end of the first reaction cylinder (51), a first switch gate (54) is arranged above the first cylinder plug, a communicating buckle is respectively arranged at the left end and the right end of the first switch gate (54), and the communicating buckles respectively control one connecting pipe.
3. The chromatography equipment for ginseng stem leaf production according to claim 2, wherein a second cylinder plug is arranged at the top end of the second reaction cylinder (52), a second switch gate (55) is arranged above the second cylinder plug, a third cylinder plug is arranged at the top end of the third reaction cylinder (53), a third switch gate (56) is arranged above the third cylinder plug, a connecting mode of a communicating buckle arranged at the top end of the second switch gate (55) and a communicating pipe is consistent with a connecting mode of the first switch gate (54), and a connecting mode of a communicating buckle arranged at the top end of the third switch gate (56) and a communicating pipe is consistent with a connecting mode of the first switch gate (54).
4. The chromatography equipment for ginseng stem leaf production according to claim 1, wherein a drainage tube (57) is arranged at the bottom end of the treatment device (5), a waste valve (58) is arranged at the bottom end of the drainage tube (57), and a first collecting device (8) is arranged at the bottom end of the waste valve (58).
5. The chromatography equipment for ginseng stem leaf production according to claim 1, wherein the second collecting device (9) comprises a first collecting bottle (91) and a second collecting bottle (92), and the top ends of the first collecting bottle (91) and the second collecting bottle (92) are opposite to the bottom of the diversion pipe (77).
6. The chromatography device for ginseng stem leaf production according to claim 1, wherein a filtering device is arranged at the top end of the waste liquid bottle (73), a filtering membrane (731) is arranged at the top end of the filtering device, a plurality of adsorption blocks (732) are arranged on the filtering membrane (731), a permeable membrane (733) is arranged at the bottom of the filtering membrane (731), a filtering screen (735) is arranged at the bottom end of the permeable membrane (733), and a through hole (734) is arranged in the center of the filtering device.
CN202022731621.0U 2020-11-23 2020-11-23 A chromatography equipment for ginseng stem leaf production Active CN213852117U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202022731621.0U CN213852117U (en) 2020-11-23 2020-11-23 A chromatography equipment for ginseng stem leaf production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202022731621.0U CN213852117U (en) 2020-11-23 2020-11-23 A chromatography equipment for ginseng stem leaf production

Publications (1)

Publication Number Publication Date
CN213852117U true CN213852117U (en) 2021-08-03

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Application Number Title Priority Date Filing Date
CN202022731621.0U Active CN213852117U (en) 2020-11-23 2020-11-23 A chromatography equipment for ginseng stem leaf production

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