CN204637640U - A kind of device extracting mogroside V from Momordica grosvenori - Google Patents
A kind of device extracting mogroside V from Momordica grosvenori Download PDFInfo
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- CN204637640U CN204637640U CN201520308305.9U CN201520308305U CN204637640U CN 204637640 U CN204637640 U CN 204637640U CN 201520308305 U CN201520308305 U CN 201520308305U CN 204637640 U CN204637640 U CN 204637640U
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- momordica grosvenori
- membrane separation
- spiral wound
- mogroside
- separation device
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Abstract
The utility model discloses a kind of device extracting mogroside V from Momordica grosvenori, it is characterized in that: comprise the extraction element, the ceramic membrane separation device that are connected successively by pipeline, the dislysate outlet of described ceramic membrane separation device connects spiral wound membrane separation device, the dislysate outlet of described spiral wound membrane separation device connects macroporous resin adsorption device, described macroporous resin adsorption device junctional membrane distillation and concentration device; Described extraction element is provided with microwave generating apparatus.The device extracting mogroside V from Momordica grosvenori described in the utility model, by Microwave Extraction, ceramic membrane Separation of Solid and Liquid and removal of impurities, spiral wound separation and purification, the further separation and purification of macroporous resin adsorption, membrane distillation concentration, can effectively remove the impurity in extract and obtain higher cycles of concentration, having that technique is simple, good product purity, cycles of concentration advantages of higher.
Description
Technical field
The utility model relates to Momordica grosvenori and extracts field, particularly a kind of device extracting mogroside V from Momordica grosvenori.
Background technology
Momordica grosvenori as the endemic plant of China, because of advantage geographically, for the research of Momordica grosvenori each side is provided convenience, to its research except Momordica grosvenori composite except, mainly concentrate on the extraction and purification process aspect of Momordica grosvenori mogroside V.Momordica grosvenori belongs to the fruit of Curcurbitaceae herbaceous perennial vine plant, is south China endemic plant, mainly originates in backlands district, osmanthus, best with the Momordica grosvenori quality of Guilin.Arhat fruity is sweet, cool in nature, nontoxic, there is removing heat from the lung to relieve cough, relax bowel, clearing heat and detoxicating, eliminate the phlegm and enrich blood, the effects such as beneficial liver, invigorating the spleen, promotion functions of intestines and stomach.Containing Simon glucoside I (sianenoside I) in Momordica grosvenori, Momordica-Glycosides II E (eogroside II E), Momordica-Glycosides III (mogroside III), Momordica-Glycosides III E (mogroside III E), Momordica-Glycosides IV (ogroside IV), mogroside Ⅴ (mogroside V), Momordica-Glycosides A, the cucurbitane element triterpene glucoside materials such as Momordica grosvenori Neogroside, except Momordica-Glycosides IV and Momordica grosvenori Neogroside, be sweet substance, wherein the sugariness of mogroside Ⅴ is the highest, be equivalent to 300 times of sucrose, and sweet taste is pure, free from extraneous odour, aftertaste sense is strong, Heat stability is good, can be used as food, the sweetener of dish, the ideal sugar Dai Pin of diabetes patient.
CN101863946A discloses a kind of method extracting high-load Momordica grosvenori mogroside V in dried fructus momordicae, the method be by alcohol extracting after the fragmentation of Momordica grosvenori dry fruit, concentrated, macroporous resin adsorption is separated, ion-exchange resin decolorization, product is obtained through concentrate drying, the method process is simple, adapt to plant produced, but product purity is low, resin utilization rate is low.CN101690573A discloses a kind of mogroside V content and is greater than 60% production method of fructus, the method is separated and alumina column chromatography enzymolysis after Momordica grosvenori fragmentation, water extraction, concentrated, ion-exchange resin decolorization, macroporous resin adsorption, product is obtained finally by concentrate drying, the method can realize product beet aglucone V purity and be greater than 60%, because of through more chromatographic enrichment, make the yield of final products lower.CN10140266A discloses the preparation method of mogroside V, the method is for raw material with Momordica grosvenori crude extract, product is obtained through silica gel column chromatography, C18 post reversed phase chromatography, concentrate drying, product purity can reach more than 70%, the major defect of the method is use a large amount of organic solvents in process, product yield is low, and cost is high, is unsuitable for industrial production.CN101177444A discloses a kind of method extracting Momordica-Glycosides from Momordica grosvenori, the method be the fragmentation of Momordica grosvenori fresh fruit, enzymolysis, multi-stage countercurrent are extracted, centrifugal, ultrafiltration, concentrated, macroporous resin adsorption separation, ion-exchange resin decolorization, C18 reversed-phase silica gel chromatography, through concentrate drying, obtained product, the defect of the method is that product yield is low, product purity is low, complex process, is unfavorable for industrial production.CN104086615A discloses a kind of method preparing mogroside V from Momordica grosvenori, the method be by HIGH PRESSURE TREATMENT after Momordica grosvenori fragmentation, supercritical fluid extraction, through HP-20ss resin chromatography, concentrated, dry product, beet aglucone V purity more than 70% in product, the method technique is simple, purity is high, but due to supercritical fluid extraction equipment single treatment quantitative limitation, be unfavorable for continuous print large-scale production.Given this, be necessary to improve prior art.
Summary of the invention
For the problems referred to above, the purpose of this utility model is to provide that a kind of technique is simple, the device extracting mogroside V from Momordica grosvenori of good product purity.
For achieving the above object, the technical scheme that the utility model proposes is: a kind of device extracting mogroside V from Momordica grosvenori, it is characterized in that: comprise the extraction element, the ceramic membrane separation device that are connected successively by pipeline, the dislysate outlet of described ceramic membrane separation device connects spiral wound membrane separation device, the dislysate outlet of described spiral wound membrane separation device connects macroporous resin adsorption device, described macroporous resin adsorption device junctional membrane distillation and concentration device; Described extraction element is provided with microwave generating apparatus, and the ceramic membrane aperture in described ceramic membrane separation device is 50-200nm, and in described spiral wound separator, rolling ultrafiltration membrane molecular weight cut off is 3000-5000 dalton.
Preferably, in described spiral wound separator, rolling ultrafiltration membrane molecular weight cut off is 3500 dalton.
Preferably, described membrane distillation concentration device is doughnut membrane distillation concentration device.
Adopt technique scheme, the device extracting mogroside V from Momordica grosvenori described in the utility model, by Microwave Extraction, ceramic membrane Separation of Solid and Liquid and removal of impurities, spiral wound separation and purification, the further separation and purification of macroporous resin adsorption, membrane distillation concentration, can effectively remove the impurity in extract and obtain higher cycles of concentration, having that technique is simple, good product purity, cycles of concentration advantages of higher.
Accompanying drawing explanation
Fig. 1 is the apparatus structure schematic diagram extracting mogroside V from Momordica grosvenori described in the utility model.
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, the utility model is described further.
As shown in Figure 1, the device extracting mogroside V from Momordica grosvenori described in the utility model, comprise the extraction element 10, the ceramic membrane separation device 11 that are connected successively by pipeline, the dislysate outlet of described ceramic membrane separation device 11 connects spiral wound membrane separation device 12, the dislysate outlet of described spiral wound membrane separation device 12 connects macroporous resin adsorption device 13, described macroporous resin adsorption device 13 junctional membrane distillation and concentration device 14; Described extraction element 10 is provided with microwave generating apparatus 101, ceramic membrane aperture in described ceramic membrane separation device 11 is 50-200nm, in described spiral wound separator 13, rolling ultrafiltration membrane molecular weight cut off is 3000-5000 dalton, is preferably 3500 dalton.
During concrete use, Momordica grosvenori, after being ground into powder, adds flooding in extraction element, in the process of lixiviate, carry out Microwave Extraction by microwave generating apparatus, obtains leaching liquor and filter residue, filtrate and filter residue directly enter in ceramic membrane separation device and carry out Separation of Solid and Liquid, effectively eliminate the particles such as the filter residue in leaching liquor, then ceramic membrane dislysate enters in spiral wound membrane separation device, rolling ultrafiltration membrane molecular weight cut off is 3000-5000 dalton, in spiral wound membrane separation device, large molecular impurity is retained by milipore filter, and the small organic molecules such as mogroside V enter in dislysate through milipore filter, obtain mogroside V solution, mogroside V solution enters in membrane distillation concentration device after entering the further separation and purification of macroporous resin adsorption device again and concentrates further, obtain macroporous resin adsorption device concentrate.
Although specifically show in conjunction with preferred embodiment and describe the utility model; but those skilled in the art should be understood that; not departing from the spirit and scope of the present utility model that appended claims limits; in the form and details the utility model is made a variety of changes, be protection domain of the present utility model.
Claims (3)
1. one kind is extracted the device of mogroside V from Momordica grosvenori, it is characterized in that: comprise the extraction element, the ceramic membrane separation device that are connected successively by pipeline, the dislysate outlet of described ceramic membrane separation device connects spiral wound membrane separation device, the dislysate outlet of described spiral wound membrane separation device connects macroporous resin adsorption device, described macroporous resin adsorption device junctional membrane distillation and concentration device; Described extraction element is provided with microwave generating apparatus, and the ceramic membrane aperture in described ceramic membrane separation device is 50-200nm, and in described spiral wound separator, rolling ultrafiltration membrane molecular weight cut off is 3000-5000 dalton.
2. a kind of device extracting mogroside V from Momordica grosvenori according to claim 1, is characterized in that: in described spiral wound separator, rolling ultrafiltration membrane molecular weight cut off is 3500 dalton.
3. a kind of device extracting mogroside V from Momordica grosvenori according to claim 1, is characterized in that: described membrane distillation concentration device is doughnut membrane distillation concentration device.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201520308305.9U CN204637640U (en) | 2015-05-14 | 2015-05-14 | A kind of device extracting mogroside V from Momordica grosvenori |
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| CN201520308305.9U CN204637640U (en) | 2015-05-14 | 2015-05-14 | A kind of device extracting mogroside V from Momordica grosvenori |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115581266A (en) * | 2022-09-02 | 2023-01-10 | 湖南华诚生物资源股份有限公司 | Clean production method of momordica grosvenori dry powder and momordica grosvenori condensed juice |
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2015
- 2015-05-14 CN CN201520308305.9U patent/CN204637640U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115581266A (en) * | 2022-09-02 | 2023-01-10 | 湖南华诚生物资源股份有限公司 | Clean production method of momordica grosvenori dry powder and momordica grosvenori condensed juice |
| CN115581266B (en) * | 2022-09-02 | 2024-03-12 | 湖南华诚生物资源股份有限公司 | Clean production method of momordica grosvenori dry powder and momordica grosvenori concentrated juice |
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| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150916 Termination date: 20170514 |
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| CF01 | Termination of patent right due to non-payment of annual fee |