CN213387834U - Device for purifying tantalum hydroxide by adopting steam injection method - Google Patents
Device for purifying tantalum hydroxide by adopting steam injection method Download PDFInfo
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- CN213387834U CN213387834U CN202022479258.8U CN202022479258U CN213387834U CN 213387834 U CN213387834 U CN 213387834U CN 202022479258 U CN202022479258 U CN 202022479258U CN 213387834 U CN213387834 U CN 213387834U
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- tantalum hydroxide
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Abstract
The utility model discloses an adopt device of steam injection method purification tantalum hydroxide, including the organism, be provided with the cavity in the organism, be provided with the intake pipe on the organism lateral wall, steam lets in through the intake pipe in the organism, be provided with first valve in the intake pipe, the bottom of the body is provided with the cylinder, and the output shaft of cylinder runs through the lateral wall of organism extends to in the cavity, be located and be provided with on the output shaft of the interior cylinder of cavity and connect the platform, connect the bench and be provided with the motor, the output shaft of motor is provided with the revolving stage, and the revolving stage is used for placing the tantalum hydroxide filter cake of treating the purification, still is provided with the blast pipe on the organism, is provided with the second valve on. The utility model discloses a relief valve settlement operating pressure, the automatic fluorine-containing gas who will evaporate of relief valve when reaching the pressure level discharges, reaches the purpose of purification product from this, and easy operation has improved the production efficiency of enterprise greatly.
Description
Technical Field
The utility model relates to a purification technical equipment field specifically is an adopt device of steam jet method purification tantalum hydroxide.
Background
In the prior art, after ammonia gas is introduced into tantalum (niobium) fluoride acid solution to neutralize and precipitate in the process, ammonia fluoride solution with a certain concentration is contained in tantalum (niobium) hydroxide precipitate during production, fluorine ions have certain influence on product quality and need to be removed, the traditional process is that tantalum (niobium) hydroxide neutralized slurry is filtered firstly, then a large amount of low-concentration ammonia water is added into a filter cake to circularly wash the filter cake until the fluorine ions are washed to a certain concentration, the process is complicated by adopting the method, a large amount of manpower and material cost is consumed, the production cost of enterprises is greatly improved, and the production efficiency of the enterprises is reduced.
SUMMERY OF THE UTILITY MODEL
In order to solve the technical problem, the utility model provides a following technical scheme:
the utility model provides a device for purifying tantalum hydroxide by adopting a steam jet method,
the novel gas cylinder purification machine comprises a machine body, be provided with the cavity in the organism, be provided with the intake pipe on the organism lateral wall, steam passes through the intake pipe lets in the organism, be provided with first valve in the intake pipe, the bottom of the body is provided with the cylinder, the output shaft of cylinder runs through the lateral wall of organism extends to in the cavity, be located be provided with on the output shaft of cylinder in the cavity and connect the platform, connect the bench and be provided with the motor, the output shaft of motor is provided with the revolving stage, the revolving stage is used for placing the tantalum hydroxide filter cake of treating the purification, still be provided with the blast pipe on the organism, be provided with the second valve on the blast pipe, the.
Preferably, the second valve is provided as a pressure relief valve.
Preferably, the connecting platform and be provided with limit structure between the bottom in the organism, limit structure is including setting up the spacing section of thick bamboo of bottom and slidable setting are in the organism the gag lever post in the spacing section of thick bamboo, the upper end of gag lever post with the lower fixed surface of connecting the platform is connected.
Preferably, the lower end of the machine body is provided with a fixed shaft, the lower end of the fixed shaft is provided with a pulley, and the pulley is provided with a brake pad.
Preferably, in order to facilitate opening and closing of the box door, the box door is provided with a handle, and the handle is provided with anti-slip lines to prevent an operator from slipping when operating the handle.
Preferably, in order to facilitate sealing of the machine body, a fluorine rubber layer is disposed at a junction between the box door and the machine body.
Preferably, in order to facilitate the operator to monitor the purification condition of the tantalum hydroxide filter cake in the machine body in real time, a window is arranged on the box door.
The utility model has the advantages that
The utility model discloses an open first valve, take high temperature and pressurized steam to pass through in the intake pipe lets in the organism, let in and close first valve after a period, take high temperature and pressurized steam to vaporize the fluorinion on tantalum hydroxide filter cake surface, thereby reach the effect to tantalum hydroxide filter cake purification, set for operating pressure through the pressure relief valve, the automatic fluorine-containing gas who will evaporate of pressure relief valve when reaching the pressure level discharges, reach the purpose of purification product from this, and is simple in operation, the production efficiency of enterprise has been improved greatly.
Drawings
Fig. 1 is a front view structural section view of the present invention.
Fig. 2 is a front view of the structure of the present invention.
Description of reference numerals: 1. a body; 2. a cavity; 3. an air inlet pipe; 4. a first valve; 5. a cylinder; 6. a connecting table; 7. a motor; 8. a turntable; 9. an exhaust pipe; 10. a second valve; 11. a limiting cylinder; 12. a limiting rod; 13. a fixed shaft; 14. a pulley; 15. a box door; 16. a window; 17. a handle.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Example 1
As shown in fig. 1-2, the utility model provides a device for purifying tantalum hydroxide by adopting a steam injection method,
the device comprises a machine body 1, a cavity 2 is arranged in the machine body 1, an air inlet pipe 3 is arranged on the side wall of the machine body 1, steam is introduced into the machine body 1 through the air inlet pipe 3, a first valve 4 is arranged on the air inlet pipe 3, an air cylinder 5 is arranged at the bottom of the machine body 1, an output shaft of the air cylinder 5 penetrates through the side wall of the machine body 1 and extends into the cavity 2, a connecting table 6 is arranged on the output shaft of the air cylinder 5 in the cavity 2, a motor 7 is arranged on the connecting table 6, a rotary table 8 is arranged on the output shaft of the motor 7 and used for placing a tantalum hydroxide filter cake to be purified, the rotary table 8 can be used for placing the tantalum hydroxide filter cake and also can be used for purifying the niobium hydroxide filter cake, in the embodiment, the rotary table 8 is used for placing the tantalum hydroxide filter cake, and, a second valve 10 is arranged on the exhaust pipe 9, the second valve 10 is a pressure relief valve, a box door 15 is hinged on the front surface of the machine body 1,
opening a box door 15, putting the tantalum hydroxide filter cake to be purified on a rotary table 8, closing the box door 15, opening a first valve 4, introducing steam with high temperature and pressurization into the machine body 1 through an air inlet pipe 3, closing the first valve 4 after introducing for a period of time, and vaporizing fluorine ions on the surface of the tantalum hydroxide filter cake by the steam with high temperature and pressurization so as to achieve the effect of purifying the tantalum hydroxide filter cake;
the switch of the air cylinder 5 and the motor 7 is opened, the output shaft of the air cylinder 5 drives the connecting platform 6 to ascend and descend vertically so as to drive the rotary table 8 to ascend and descend synchronously, the tantalum hydroxide filter cake in the rotary table 8 can shake vertically to increase the purification area, the purification efficiency is improved, the output shaft of the motor 7 drives the connecting platform 6 to rotate in the horizontal direction, the surface of the tantalum hydroxide filter cake is uniformly dried, and the effect of no purification dead angle is achieved;
working pressure is set through a pressure relief valve, and the pressure relief valve automatically discharges the evaporated fluorine-containing gas when reaching a pressure level, so that the aim of purifying the product is fulfilled;
a limiting structure is arranged between the connecting table 6 and the inner bottom of the machine body 1, the limiting structure comprises a limiting cylinder 11 arranged at the inner bottom of the machine body 1 and a limiting rod 12 slidably arranged in the limiting cylinder 11, the upper end of the limiting rod 12 is fixedly connected with the lower surface of the connecting table 6, and the limiting rod 12 moves along the limiting cylinder 11 in the lifting process of the connecting table 6, so that the position of the rotary table 8 is prevented from deviating;
in order to facilitate the opening and closing of the box door 15, a handle 17 is arranged on the box door 15, and in order to prevent an operator from slipping hands when operating the handle 17, anti-slip lines are arranged on the handle 17;
in order to facilitate sealing of the machine body 1, a fluororubber layer is arranged at the joint of the box door 15 and the machine body 1, on one hand, the fluororubber layer can seal the machine body 1 to prevent external impurities from entering the machine body 1 to pollute a sodium hydroxide filter cake, on the other hand, the fluororubber layer can prevent heat loss in the machine body 1 and play a role in energy saving, and the fluororubber layer also has an anti-corrosion effect;
in order to facilitate the operator to monitor the purification condition of the tantalum hydroxide filter cake in the machine body 1 in real time, the box door 15 is provided with a window 16.
Example 2
As shown in fig. 1-2, the present embodiment is further optimized based on embodiment 1, specifically, a fixed shaft 13 is disposed at a lower end of the machine body 1, a pulley 14 is disposed at a lower end of the fixed shaft 13, and a brake pad is disposed on the pulley 14.
This embodiment is through setting up fixed axle 13 and pulley 14 at organism 1's lower extreme, is convenient for the utility model discloses a removal and maintenance improve the utility model discloses a flexibility reduces operating personnel's working strength, through set up the brake block on pulley 14, plays fixed organism 1's effect, prevents that its operation process from causing the slip, leads to colliding with other equipment or operating personnel, causes the loss.
Principle of operation
The utility model relates to an adopt device of vapor injection method purification tantalum hydroxide, each part distributes as shown in figure 1-figure 2, during the use, open chamber door 15, put into the tantalum hydroxide filter cake that will treat the purification on revolving stage 8 and close chamber door 15, open first valve 4, take high temperature and pressurized steam to let in organism 1 through intake pipe 3, let in after a period of time close first valve 4, take high temperature and pressurized steam to vaporize the fluorine ion on tantalum hydroxide filter cake surface, thereby reach the effect to the purification of tantalum hydroxide filter cake;
the switch of the air cylinder 5 and the motor 7 is opened, the output shaft of the air cylinder 5 drives the connecting platform 6 to ascend and descend vertically so as to drive the rotary table 8 to ascend and descend synchronously, the tantalum hydroxide filter cake in the rotary table 8 can shake vertically to increase the purification area, the purification efficiency is improved, the output shaft of the motor 7 drives the connecting platform 6 to rotate in the horizontal direction, the surface of the tantalum hydroxide filter cake is uniformly dried, and the effect of no purification dead angle is achieved;
working pressure is set through the pressure relief valve, and the pressure relief valve automatically discharges the evaporated fluorine-containing gas when reaching a pressure level, so that the aim of purifying the product is fulfilled.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications and variations can be made in the embodiments or in part of the technical features of the embodiments without departing from the spirit and the scope of the invention.
Claims (7)
1. A device for purifying tantalum hydroxide by adopting a steam jet method is characterized in that,
comprises a machine body (1), a cavity (2) is arranged in the machine body (1), an air inlet pipe (3) is arranged on the side wall of the machine body (1), steam is introduced into the machine body (1) through the air inlet pipe (3), a first valve (4) is arranged on the air inlet pipe (3), an air cylinder (5) is arranged at the bottom of the machine body (1), an output shaft of the air cylinder (5) penetrates through the side wall of the machine body (1) and extends into the cavity (2), a connecting table (6) is arranged on the output shaft of the air cylinder (5) in the cavity (2), a motor (7) is arranged on the connecting table (6), a rotary table (8) is arranged on the output shaft of the motor (7), the rotary table (8) is used for placing tantalum hydroxide filter cakes to be purified, an exhaust pipe (9) is further arranged on the machine body (1), a second valve (10) is arranged on the, the front surface of the machine body (1) is hinged with a box door (15).
2. The apparatus for purifying tantalum hydroxide by steam injection according to claim 1,
the second valve (10) is arranged as a pressure relief valve.
3. The apparatus for purifying tantalum hydroxide by steam injection according to claim 1,
connect platform (6) with be provided with limit structure between the bottom in organism (1), limit structure is including setting up spacing section of thick bamboo (11) and the slidable setting of bottom are in organism (1) gag lever post (12) in the spacing section of thick bamboo (11), the upper end of gag lever post (12) with the lower fixed surface of connecting platform (6) is connected.
4. The apparatus for purifying tantalum hydroxide by steam injection according to claim 3,
the lower extreme of organism (1) is provided with fixed axle (13), fixed axle (13) lower extreme is provided with pulley (14), be provided with the brake block on pulley (14).
5. The apparatus for purifying tantalum hydroxide by steam injection according to claim 1,
in order to facilitate the opening and closing of the box door (15), a handle (17) is arranged on the box door (15), and anti-skidding lines are arranged on the handle (17) in order to prevent the hands of an operator from skidding when the operator operates the handle (17).
6. The apparatus for purifying tantalum hydroxide by steam injection according to claim 5,
in order to facilitate sealing of the machine body (1), a fluorine rubber layer is arranged at the joint of the box door (15) and the machine body (1).
7. The apparatus for purifying tantalum hydroxide by steam injection according to claim 6,
in order to facilitate the operator to monitor the purification condition of the tantalum hydroxide filter cake in the machine body (1) in real time, a window (16) is arranged on the box door (15).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022479258.8U CN213387834U (en) | 2020-10-30 | 2020-10-30 | Device for purifying tantalum hydroxide by adopting steam injection method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022479258.8U CN213387834U (en) | 2020-10-30 | 2020-10-30 | Device for purifying tantalum hydroxide by adopting steam injection method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN213387834U true CN213387834U (en) | 2021-06-08 |
Family
ID=76192077
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022479258.8U Active CN213387834U (en) | 2020-10-30 | 2020-10-30 | Device for purifying tantalum hydroxide by adopting steam injection method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN213387834U (en) |
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2020
- 2020-10-30 CN CN202022479258.8U patent/CN213387834U/en active Active
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