CN212855717U - Reaction kettle for efficiently producing glutaraldehyde - Google Patents
Reaction kettle for efficiently producing glutaraldehyde Download PDFInfo
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- CN212855717U CN212855717U CN202020899124.9U CN202020899124U CN212855717U CN 212855717 U CN212855717 U CN 212855717U CN 202020899124 U CN202020899124 U CN 202020899124U CN 212855717 U CN212855717 U CN 212855717U
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Abstract
The utility model provides a reation kettle of high-efficient production glutaraldehyde, including reinforced disc, puddler, during the reaction, some reaction material adds gradually to reinforced disc, rotate reinforced disc simultaneously, the raw materials in reinforced disc is thrown into the reation kettle body through the discharge opening under the rotation effect, and another part raw materials then adds gradually to the puddler through the charge opening, the motor rotates and drives the puddler rotation, the raw materials in the puddler gets into the branch simultaneously and is thrown into the reation kettle body through the through-hole under the rotation of puddler, two parts raw materials are added gradually respectively in the reation kettle body and react gradually, can make the material fully react, improve reaction efficiency; the reaction kettle further comprises a circulating pipe, and the raw materials which are not fully reacted in the reaction kettle body can be pumped into the feeding box through the circulating pipe and enter the reaction kettle body again for further reaction, so that the reaction efficiency is improved.
Description
Technical Field
The utility model relates to a glutaraldehyde preparation technical field especially relates to a reation kettle of high-efficient production glutaraldehyde.
Background
Glutaraldehyde is an important chemical, and can be used as a processing aid in food industry, a bacteria disinfectant, a tanning agent, a wood preservative, a medicine, a polymer synthetic raw material and the like. At present, the raw materials are generally placed in a conventional reaction kettle to be stirred in the preparation process, the reaction efficiency of the conventional reaction kettle is not high, and therefore, the conventional reaction kettle needs to be improved.
SUMMERY OF THE UTILITY MODEL
In view of this, the utility model provides a production glutaraldehyde's reation kettle can feed in raw material by turns in order to improve reaction efficiency.
The technical scheme of the utility model is realized like this: the utility model provides a reation kettle of high-efficient production glutaraldehyde, including the reation kettle body, still include reinforced disc, puddler, motor, filling tube and branch, reinforced disc is located this internal of reation kettle, a plurality of discharge openings have been seted up to the inside cavity of reinforced disc and bottom, this is external at reation kettle is worn out to the reinforced disc of filling tube one end intercommunication, the other end, reinforced disc can be at this internal rotation of reation kettle, the puddler sets up and wears out reation kettle this external and be connected with motor shaft at reation kettle this internal and upper end, the branch interval sets up on the puddler, equal inside cavity of puddler and branch and mutual intercommunication, the puddler is located reation kettle body top lateral wall and is equipped with the filling opening, a plurality of through-holes have been seted up on the branch.
On the basis of above technical scheme, preferred, still include sleeve and charging box, the periphery at the charge door of puddler is established to the sleeve cover, the sleeve inner wall is equipped with sunkenly, form the cavity between sleeve inner wall and the puddler, the charging box passes through the pipe intercommunication the cavity, the puddler can rotate around the sleeve.
On the basis of the technical scheme, preferably, the charging pipe is provided with a first gear at the periphery above the reaction kettle body, a second gear is correspondingly arranged on the stirring rod, and the first gear is meshed with the second gear.
On the basis of the technical scheme, the automatic oil feeding device is preferred to further comprise a sleeve, the sleeve is sleeved on the periphery of the reaction kettle body, an oil inlet is formed in one end of the sleeve, and an oil outlet is formed in the other end of the sleeve.
Further preferably, the reaction kettle further comprises a circulating pipe and a circulating pump, one end of the circulating pipe penetrates through the sleeve and is communicated with the lower end of the reaction kettle body, the other end of the circulating pipe penetrates through the reaction kettle body and is communicated with the feeding box, and the circulating pump is located on the circulating pipe.
On the basis of the technical scheme, preferably, the supporting rod is arranged in a downward inclined mode, and an included angle between the supporting rod and the stirring rod is 30-45 degrees.
On the basis of the technical scheme, preferably, a one-way valve for feeding the reaction kettle body is arranged in each through hole.
On the basis of the above technical solution, preferably, the conduit is provided with a flow control valve.
The utility model discloses a reation kettle of high-efficient production glutaraldehyde has following beneficial effect for prior art:
(1) the utility model discloses a reation kettle of high-efficient production glutaraldehyde, including reinforced disc, the puddler, during the reaction, some reaction material adds gradually to reinforced disc, rotate reinforced disc simultaneously, the raw materials in reinforced disc is thrown into the reation kettle body through the discharge opening under the rotation effect, and another part raw materials then adds gradually to the puddler through the charge opening, the motor rotates and drives the puddler rotation, the raw materials in the puddler gets into the branch simultaneously and is thrown into the reation kettle body through the through-hole under the rotation of puddler, so two parts raw materials are added gradually respectively in the reation kettle body and react gradually, so, can make the material fully react, improve reaction efficiency;
(2) the reaction kettle for efficiently producing glutaraldehyde of the utility model also comprises a sleeve, wherein one end of the sleeve is provided with an oil inlet, the other end of the sleeve is provided with an oil outlet, and hot oil is introduced into the sleeve through the oil inlet, so that the raw material in the reaction kettle body can be heated to maintain the reaction temperature in the reaction kettle body;
(3) the utility model discloses a reation kettle of high-efficient production glutaraldehyde still includes the circulating pipe, can be with this internal not fully reacted's of reation kettle raw materials pumpingly to reinforced case in through the circulating pipe to further react in the reentrant reation kettle body, in order to improve reaction efficiency.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.
FIG. 1 is a schematic structural view of a reaction kettle for efficiently producing glutaraldehyde according to the present invention;
fig. 2 is a schematic structural view of the connection between the feeding disc and the feeding tube of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work all belong to the protection scope of the present invention.
As shown in figures 1-2, the utility model discloses a reation kettle of high-efficient production glutaraldehyde, including reation kettle body 1, reinforced disc 2, puddler 3, motor 4, filling tube 5, branch 6, sleeve 7, charging box 8, sleeve pipe 9.
The reaction kettle body 1 is used for providing a place for a reaction for preparing glutaraldehyde;
the feeding disc 2 is in a hollow cylinder shape, the feeding disc 2 is positioned in the reaction kettle body 1, the feeding disc 2 is hollow inside, and the bottom of the feeding disc 2 is provided with a plurality of discharge holes 21;
the lower end of the feeding pipe 5 is communicated with the feeding disc 2, a through hole is formed in the reaction kettle body 1 corresponding to the feeding pipe 5, the upper end of the feeding pipe 5 penetrates out of the through hole, the feeding disc 2 can rotate in the reaction kettle body 1, specifically, a gear can be arranged on the periphery of the feeding pipe 5 and is meshed with a motor rotating shaft, and therefore the feeding disc 2 can be driven to rotate through the rotation of the motor;
puddler 3, its vertical setting is in reation kettle body 1, puddler 3 upper end is worn out reation kettle body 1 and is connected with motor 4 pivot outward, 3 both sides of puddler are located reation kettle body 1 simultaneously and from top to bottom set up a plurality of branches 6, the equal inside cavity of puddler 3 and branch 6, puddler 3 and the inside intercommunication each other of branch 6, it is equipped with charge door 31 to be located reation kettle body 1 top lateral wall at puddler 3 simultaneously, a plurality of through-holes 61 have been seted up on branch 6.
When the reaction kettle works, a part of reaction raw materials (such as acid catalyst and water) are gradually added into the feeding disc 2 through the feeding pipe 5, the feeding disc 2 is rotated at the same time, the raw materials in the feeding disc 2 are thrown into the reaction kettle body 1 through the discharge hole 21 under the rotation action, while the other part of the raw material (such as 2-methoxy-3, 4-dihydro-2H-pyran (MDP)) is gradually added into the stirring rod 3 through the feeding hole 31, the motor 4 is started, the motor 4 rotates to drive the stirring rod 3 to rotate, meanwhile, the raw materials in the stirring rod 3 enter the supporting rod 6 and are thrown into the reaction kettle body 1 through the through hole 61 under the rotation of the stirring rod 3, thus, the two parts of raw materials are respectively and gradually added into the reaction kettle body 1 and react step by step, so that the materials can fully react, and the reaction efficiency is improved.
The sleeve 7 is sleeved on the periphery of the feeding hole 31 of the stirring rod 3, a recess is formed in the inner wall of the sleeve 7, a cavity is formed between the inner wall of the sleeve 7 and the periphery of the stirring rod 3, a feeding box 8 is further arranged, the feeding box 8 is communicated with the cavity through a guide pipe 81, a feeding port is formed in the feeding box 8, the stirring rod 3 can rotate around the sleeve 7, another part of raw materials (such as 2-methoxy-3, 4-dihydro-2H-pyran (MDP)) is added into the feeding box 8 through the feeding port, and the raw materials enter the cavity through the guide pipe 81, enter the stirring rod 3 through the feeding hole 31 and finally enter the reaction kettle body 1 through the through hole 61.
Specifically, in order to facilitate the rotation of the feeding disk 2, the first gear 51 is further arranged on the periphery of the feeding pipe 5 above the reaction kettle body 1, the second gear 32 is arranged at a corresponding position on the stirring rod 3, the first gear 51 is meshed with the second gear 32, the motor 4 rotates to drive the stirring rod 3 to rotate, the second gear 32 rotates through the first gear 51, and therefore the feeding disk 2 rotates. The stirring rod 3 and the feeding disc 2 are driven to rotate simultaneously by a motor 4.
The reaction kettle further comprises a circulating pipe 11 and a circulating pump 12, specifically, one end of the circulating pipe 11 penetrates through the sleeve 9 and is communicated with the lower end of the reaction kettle body 1, the other end of the circulating pipe 11 penetrates through the reaction kettle body 1 and is communicated with the feeding box 8, the circulating pump 2 is located on the circulating pipe 11, and raw materials which are not fully reacted in the reaction kettle body 1 can be pumped into the feeding box 8 through the circulating pipe 11 and enter the reaction kettle body 1 again for further reaction. The actual circulation pipe 11 is provided with a valve.
The supporting rod 6 is arranged in a downward inclined mode, and an included angle between the supporting rod 6 and the stirring rod 3 is 30-45 degrees.
And a one-way valve for feeding the reaction kettle body 1 is arranged in each through hole 61, and the one-way valve only allows the support rod 6 to flow into the reaction kettle body 1.
In practice, a flow control valve 82 is also provided on conduit 81, and the rate at which the feed material in the feed tank 8 enters the paddle 3 can be controlled by the provision of the flow control valve 82.
The above description is only a preferred embodiment of the present invention, and should not be taken as limiting the invention, and any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (8)
1. The utility model provides a reation kettle of high-efficient production glutaraldehyde, includes reation kettle body (1), its characterized in that: the reaction kettle further comprises a feeding disc (2), a stirring rod (3), a motor (4), a feeding pipe (5) and a supporting rod (6), wherein the feeding disc (2) is positioned in the reaction kettle body (1), the feeding disc (2) is hollow inside and is provided with a plurality of discharge holes (21) at the bottom, one end of the feeding pipe (5) is communicated with the feeding disc (2), the other end of the feeding pipe penetrates out of the reaction kettle body (1), the feeding disc (2) can rotate in the reaction kettle body (1), the stirring rod (3) is arranged in the reaction kettle body (1), the upper end of the stirring rod penetrates out of the reaction kettle body (1) and is connected with a rotating shaft of the motor (4), the supporting rod (6) is arranged on the stirring rod (3) at intervals, the stirring rod (3) and the supporting rod (6) are both hollow inside and are communicated with each other, the side wall of the stirring rod (3) positioned above the reaction kettle body (1) is provided, the supporting rod (6) is provided with a plurality of through holes (61).
2. The reaction kettle for efficiently producing glutaraldehyde according to claim 1, wherein: still include sleeve (7) and charging box (8), sleeve (7) cover is established in the periphery of charge door (31) of puddler (3), sleeve (7) inner wall is equipped with sunkenly, form the cavity between sleeve (7) inner wall and puddler (3), charging box (8) are through pipe (81) intercommunication the cavity, puddler (3) can rotate around sleeve (7).
3. The reaction kettle for efficiently producing glutaraldehyde according to claim 1, wherein: the feed pipe (5) are located reation kettle body (1) top periphery and are equipped with first gear (51), correspond on puddler (3) and be equipped with second gear (32), mesh mutually between first gear (51) and second gear (32).
4. The reaction kettle for efficiently producing glutaraldehyde according to claim 1, wherein: still include sleeve pipe (9), sleeve pipe (9) cover is established in reation kettle body (1) periphery, oil inlet (91) have been seted up to one end on sleeve pipe (9), the other end is equipped with oil-out (92).
5. The reaction kettle for efficiently producing glutaraldehyde according to claim 4, wherein: still include circulating pipe (11) and circulating pump (12), circulating pipe (11) one end is passed sleeve pipe (9) and is linked together reation kettle body (1) lower extreme, the other end passes reation kettle body (1) and links together charging box (8), circulating pump (12) are located circulating pipe (11).
6. The reaction kettle for efficiently producing glutaraldehyde according to claim 1, wherein: branch (6) downward sloping setting, the contained angle is 30 ~ 45 between branch (6) and puddler (3).
7. The reaction kettle for efficiently producing glutaraldehyde according to claim 1, wherein: a one-way valve for feeding the reaction kettle body (1) is arranged in each through hole (61).
8. The reaction kettle for efficiently producing glutaraldehyde according to claim 2, wherein: the guide pipe (81) is provided with a flow control valve (82).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020899124.9U CN212855717U (en) | 2020-05-25 | 2020-05-25 | Reaction kettle for efficiently producing glutaraldehyde |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020899124.9U CN212855717U (en) | 2020-05-25 | 2020-05-25 | Reaction kettle for efficiently producing glutaraldehyde |
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| CN212855717U true CN212855717U (en) | 2021-04-02 |
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| CN202020899124.9U Active CN212855717U (en) | 2020-05-25 | 2020-05-25 | Reaction kettle for efficiently producing glutaraldehyde |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113291090A (en) * | 2021-06-17 | 2021-08-24 | 周口师范学院 | Pigment automatic measurement mixing of colors device for fine arts drawing |
| CN113975991A (en) * | 2021-10-15 | 2022-01-28 | 深圳市真味生物科技有限公司 | Processing equipment and processing method for processing and producing nicotine salt |
| CN114311304A (en) * | 2021-12-21 | 2022-04-12 | 湖南尔旭新材料有限公司 | Thermal insulation mortar production processing line |
| CN114471433A (en) * | 2022-02-17 | 2022-05-13 | 臻和慧联(浙江)环境科技有限公司 | Activated carbon regeneration system and regeneration method thereof |
-
2020
- 2020-05-25 CN CN202020899124.9U patent/CN212855717U/en active Active
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113291090A (en) * | 2021-06-17 | 2021-08-24 | 周口师范学院 | Pigment automatic measurement mixing of colors device for fine arts drawing |
| CN113291090B (en) * | 2021-06-17 | 2022-04-12 | 周口师范学院 | Pigment automatic measurement mixing of colors device for fine arts drawing |
| CN113975991A (en) * | 2021-10-15 | 2022-01-28 | 深圳市真味生物科技有限公司 | Processing equipment and processing method for processing and producing nicotine salt |
| CN114311304A (en) * | 2021-12-21 | 2022-04-12 | 湖南尔旭新材料有限公司 | Thermal insulation mortar production processing line |
| CN114471433A (en) * | 2022-02-17 | 2022-05-13 | 臻和慧联(浙江)环境科技有限公司 | Activated carbon regeneration system and regeneration method thereof |
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