CN212631807U - Chemical evaporative crystallization device - Google Patents

Chemical evaporative crystallization device Download PDF

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Publication number
CN212631807U
CN212631807U CN202020154884.7U CN202020154884U CN212631807U CN 212631807 U CN212631807 U CN 212631807U CN 202020154884 U CN202020154884 U CN 202020154884U CN 212631807 U CN212631807 U CN 212631807U
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CN
China
Prior art keywords
end cover
fixed mounting
bucket
hand member
holds
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Expired - Fee Related
Application number
CN202020154884.7U
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Chinese (zh)
Inventor
张留巧
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Jiangsu Aite Instrument Co ltd
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Individual
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Priority to CN202020154884.7U priority Critical patent/CN212631807U/en
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Abstract

The utility model provides an evaporation crystallization device for chemical industry relates to the chemical industry field. This evaporation crystallization device for chemical industry, including holding the bucket, the top right side that holds the bucket is connected and is link up there is the feed inlet, and the inside fixed mounting that holds the bucket has the heating crystallization wall, and the inboard fixed mounting in left end that holds the bucket has solid fixed ring, and solid fixed ring's inside is rotated and is connected with rotary mechanism, and the right-hand member that holds the bucket rotates and is connected with the end cover, and rotary mechanism runs through the end cover and extends to the right side of end cover, rotary mechanism includes the joint piece, and the joint piece cup joints the inboard at solid fixed ring. This evaporation crystallization device for chemical industry can stir the solution that holds in the bucket through the scraper blade rotation under the rotation axis drives and improve evaporation efficiency, and the scraper blade is hugged closely behind the rotation control axle and is heated the crystal body that the crystal wall will appear and scrape the effect of being convenient for get the crystal body, has solved among the prior art problem that the low crystal body of evaporation efficiency adheres to inconvenient taking out.

Description

Chemical evaporative crystallization device
Technical Field
The utility model relates to the technical field of chemical industry, specifically be an evaporation crystallization device for chemical industry.
Background
The evaporation refers to a process of separating the solvent from the solute in the solution by heating the solvent; crystallization is the process of solute polymerization into crystals, and evaporation crystallization is commonly used in chemical engineering work to realize solute precipitation in solution.
The existing chemical evaporation crystallization device simultaneously realizes the crystallization of solution by heating the wall of the evaporation barrel, so that the separated crystals are attached to the barrel wall of the evaporation barrel, and the separated crystals are not easy to separate and the evaporation crystallization speed is lower.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
The utility model provides a not enough to prior art, the utility model provides an evaporation crystallization device for chemical industry has solved the problem that the background art always provided.
(II) technical scheme
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes: an evaporation crystallization device for chemical engineering comprises a containing barrel, wherein a feed inlet is connected and communicated with the right side of the top end of the containing barrel, a heating crystallization wall is fixedly arranged in the containing barrel, a fixing ring is fixedly arranged on the inner side of the left end of the containing barrel, a rotating mechanism is rotatably connected in the fixing ring, the right end of the containing barrel is rotatably connected with a sealing end cover, the rotating mechanism penetrates through the sealing end cover and extends to the right side of the sealing end cover, the rotating mechanism comprises a clamping block which is sleeved on the inner side of the fixing ring, a groove is formed in the outer surface of the clamping block, a compression spring is rotatably connected in the groove, a top bead is rotatably connected at one end of the compression spring, the end of the top bead, which is far away from the compression spring, is fixedly clamped with the fixing ring, a rotating shaft is fixedly arranged at, an extension spring is fixedly arranged at the right end of the clamping block and positioned at the outer side of the rotating shaft, a control rod is fixedly arranged at the right end of the extension spring, the control rod penetrates through the sealing end cover and extends to the right side of the sealing end cover, a rack is fixedly arranged at the outer side of the control rod, a support plate is fixedly arranged at the outer surface of the clamping block and positioned at the outer side of the extension spring, a chute is formed in the lower side of the support plate, slide blocks are fixedly arranged at the left side and the right side of the heating crystallization wall in the chute, a scraper blade is fixedly arranged above the slide blocks, the two scraper blades are meshed through a gear, one end of the gear, which is positioned at the outer side of the two scraper blades, is meshed with the rack, the gear is rotatably connected with the support plate, an adjusting mechanism is fixedly arranged, the lower part of the fixed plate is rotatably connected with a control shaft, and the outer surface of the lower part of the control shaft, which is positioned on the top plate, is fixedly sleeved with a convex block.
Preferably, the heating crystallization wall is annular, a notch is formed in the bottom end of the heating crystallization wall, and the width of the notch is equal to that of the scraper.
Preferably, the number of the scraping plates is three, and the three groups of scraping plates are sequentially connected with the supporting plate in a sliding mode at equal intervals from left to right.
Preferably, the sliding block is connected with the inner walls of the top end and the bottom end of the sliding groove in a magnetic mode, and a notch matched with the central shaft of the gear is formed in the scraper above each group of the scrapers.
Preferably, the bottom end part of the control rod is in a horseshoe shape, the rack is fixedly connected to the plane of the horseshoe shape, and the top end of the control rod is cylindrical.
Advantageous effects
The utility model provides an evaporation crystallization device for chemical industry. The method has the following beneficial effects:
1. this evaporation crystallization device for chemical industry can stir the solution that holds in the bucket through the scraper blade rotation under the rotation axis drives and improve evaporation efficiency, and the scraper blade is hugged closely behind the rotation control axle and is heated the crystal body that the crystal wall will appear and scrape the effect of being convenient for get the crystal body, has solved among the prior art problem that the low crystal body of evaporation efficiency adheres to inconvenient taking out.
2. This evaporation crystallization device for chemical industry can realize convenient to detach rotary mechanism through setting up compression spring and top pearl to and rotate the effect that the connection can guarantee the rotating member resistance effect through spring and top pearl and recess inner wall, solved among the prior art problem that rotary mechanism is not convenient for dismantle.
Drawings
FIG. 1 is a semi-sectional view of the present invention;
FIG. 2 is a schematic view of a half-section of the clamping block of the present invention;
FIG. 3 is a schematic view of the connection of the clamping block of the present invention;
fig. 4 is a schematic view of the adjusting mechanism of the present invention.
The device comprises a containing barrel-1, a heating crystallization wall-2, a fixing ring-3, a rotating mechanism-4, a sealing end cover-5, an adjusting mechanism-6, a clamping block-7, a groove-8, a compression spring-9, a top bead-10, a rotating shaft-11, an extension spring-12, a control rod-13, a rack-14, a supporting plate-15, a chute-16, a sliding block-17, a scraper-18, a gear-19, a feeding port-20, a top plate-21, a fixing plate-22, a control shaft-23 and a bump-24.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
The embodiment of the utility model provides an evaporation crystallization device for chemical industry:
embodiment one, as shown in fig. 1-4, including holding bucket 1, the top right side that holds bucket 1 is connected and is link up feed inlet 20, the inside fixed mounting that holds bucket 1 has heating crystallization wall 2, the inside of heating crystallization wall 2 is provided with the heater strip, the inboard fixed mounting in left end that holds bucket 1 has solid fixed ring 3, gu fixed ring 3's internal rotation is connected with rotary mechanism 4, the right-hand member that holds bucket 1 rotates and is connected with end cover 5, rotary mechanism 4 runs through end cover 5 and extends to end cover 5's right side, end cover 5's right-hand member fixed mounting has guiding mechanism 6, guiding mechanism 6 and rotary mechanism 4 joint.
In the second embodiment, as shown in fig. 1-4, the rotating mechanism 4 includes a clamping block 7, the clamping block 7 is sleeved on the inner side of the fixing ring 3, a groove 8 is formed on the outer surface of the clamping block 7, a compression spring 9 is rotatably connected inside the groove 8, a top ball 10 is rotatably connected to one end of the compression spring 9 away from the groove 8, a support plate is fixedly connected to one end of the compression spring 9, the support plate is rotatably connected to the groove 8, a hemispherical wrapping sleeve is sleeved outside the top ball 10, the wrapping sleeve is fixedly connected to the compression spring 9, one end of the top ball 10 away from the compression spring 9 is fixedly clamped with the fixing ring 3, a rotating shaft 11 is fixedly installed at the right end of the clamping block 7, the right end of the rotating shaft 11 penetrates through the sealing end cap 5 and extends to the right end of the sealing end cap 5, the rotating shaft 11 is connected to an existing stepping motor, an extension spring, a control rod 13 is fixedly installed at the right end of the extension spring 12, the control rod 13 penetrates through the sealing end cover 5 and extends to the right side of the sealing end cover 5, a rack 14 is fixedly installed at the outer side of the control rod 13, the bottom end part of the control rod 13 is in a horseshoe shape, the rack 14 is fixedly connected to the plane of the horseshoe shape, the top end of the control rod 13 is cylindrical, the control rod 13 arranged in the horseshoe shape can be prevented from contacting with the rotating shaft 11, the top end of the control rod 13 is cylindrical, holes of the sealing end cover 5 can be reduced, a supporting plate 15 is fixedly installed on the outer surface of the clamping block 7 and positioned at the outer side of the extension spring 12, a sliding groove 16 is formed in the lower side of the supporting plate 15, sliding blocks 17 are fixedly installed at the left side and the right side of the heating crystallization wall 2 inside the sliding groove 16, a, the width of breach equals the width of scraper blade 18, can be convenient for adhere to the crystallization through such setting and be convenient for scrape off the adnexed crystallization in scraper blade 18 surface in the in-process that scraper blade 18 removed simultaneously, the top of scraper blade 18 with hold the inner wall laminating of bucket 1, through the gear 19 meshing between two scraper blades 18, the quantity of scraper blade 18 is three groups, three group's scraper blades 18 are from a left side to the right side in proper order equidistance and backup pad 15 sliding connection, can guarantee to strike off three group's heating crystallization wall 2 through such setting, gear 19 is located the one end and the rack 14 meshing in two scraper blades 18 outsides, gear 19 is connected with backup pad 15 rotation, slider 17 passes through magnetism with spout 16 top and bottom inner wall and is connected, the breach with the center pin adaptation of gear 19 is seted up to the top scraper blade 18 of every group scraper.
In the third embodiment, as shown in fig. 1 to 4, the adjusting mechanism 6 includes a top plate 21, the top plate 21 is fixedly installed at the right end of the control rod 13, a fixing plate 22 is fixedly installed at the right end of the end cover 5, a control shaft 23 is rotatably connected below the fixing plate 22, and a protrusion 24 is fixedly sleeved on the outer surface of the control shaft 23 below the top plate 21.
When using, pour into the solvent from feed inlet 20 and hold bucket 1 in and drive the rotation axis 11 through current step motor and rotate and then can drive the scraper blade 18 rotatory through the rotation of joint piece 7, whether can promote the efficiency of evaporation through the rotation of scraper blade 18, thereby the crystal is attached to the rotatory control shaft 23 in surface that heats crystallization wall 2 and can move up lug 24 rotation drive control lever 13 and realize that scraper blade 18 inwards moves through the cooperation of rack 14 with gear 19 and hug closely heating crystallization wall 2 after the evaporation finishes, close step motor and sweep out the crystal body after taking out sealed end cap 5 and rotary mechanism wholly.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. The utility model provides an evaporation crystallization device for chemical industry, is including holding bucket (1), its characterized in that: hold the top right side of bucket (1) and connect and link up feed inlet (20), the inside fixed mounting who holds bucket (1) has heating crystallization wall (2), the inboard fixed mounting in left end that holds bucket (1) has solid fixed ring (3), the internal rotation of solid fixed ring (3) is connected with rotary mechanism (4), the right-hand member that holds bucket (1) rotates and is connected with end cover (5), rotary mechanism (4) run through end cover (5) and extend to the right side of end cover (5), the right-hand member fixed mounting of end cover (5) has guiding mechanism (6), guiding mechanism (6) and rotary mechanism (4) joint.
2. The evaporative crystallization apparatus for chemical engineering as claimed in claim 1, wherein: rotary mechanism (4) including joint piece (7), joint piece (7) cup joint in the inboard of solid fixed ring (3), and the surface of joint piece (7) is seted up fluted (8), and the inside of recess (8) is rotated and is connected with compression spring (9), and the one end that recess (8) were kept away from in compression spring (9) is rotated and is connected with top pearl (10), and the one end that compression spring (9) were kept away from in top pearl (10) is fixed and solid fixed ring (3) joint.
3. The evaporative crystallization apparatus for chemical engineering as claimed in claim 2, wherein: the right-hand member fixed mounting of joint piece (7) has rotation axis (11), the right-hand member of rotation axis (11) runs through end cover (5) and extends to the right-hand member of end cover (5), the right-hand member of joint piece (7) is located the outside fixed mounting of rotation axis (11) and has extension spring (12), the right-hand member fixed mounting of extension spring (12) has control lever (13), control lever (13) runs through end cover (5) and extends to the right side of end cover (5), the outside fixed mounting of control lever (13) has rack (14).
4. The evaporative crystallization apparatus for chemical engineering as claimed in claim 2, wherein: the outside fixed mounting that the surface of joint piece (7) is located extension spring (12) has backup pad (15), and spout (16) have been seted up to the downside of backup pad (15), and the inside of spout (16) is located the left and right sides fixed mounting that heats crystallization wall (2) has slider (17).
5. The evaporative crystallization apparatus for chemical engineering as claimed in claim 4, wherein: the upper part of the sliding block (17) is fixedly provided with a scraper (18), the two scrapers (18) are meshed through a gear (19), one end of the gear (19) positioned at the outer sides of the two scrapers (18) is meshed with the rack (14), and the gear (19) is rotatably connected with the supporting plate (15).
6. The evaporative crystallization apparatus for chemical engineering as claimed in claim 1, wherein: adjustment mechanism (6) include roof (21), and roof (21) fixed mounting has fixed plate (22) at the right-hand member of control lever (13), and the right-hand member fixed mounting of end cover (5), the below of fixed plate (22) is rotated and is connected with control shaft (23), and the fixed lug (24) that has cup jointed of below surface that is located roof (21) of control shaft (23).
CN202020154884.7U 2020-02-07 2020-02-07 Chemical evaporative crystallization device Expired - Fee Related CN212631807U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202020154884.7U CN212631807U (en) 2020-02-07 2020-02-07 Chemical evaporative crystallization device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202020154884.7U CN212631807U (en) 2020-02-07 2020-02-07 Chemical evaporative crystallization device

Publications (1)

Publication Number Publication Date
CN212631807U true CN212631807U (en) 2021-03-02

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ID=74767300

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202020154884.7U Expired - Fee Related CN212631807U (en) 2020-02-07 2020-02-07 Chemical evaporative crystallization device

Country Status (1)

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CN (1) CN212631807U (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117224993A (en) * 2023-11-11 2023-12-15 河北华晨药业集团有限公司 Crystallization reactor for pharmaceutical chemical industry
CN117919766A (en) * 2024-03-22 2024-04-26 山西磊鑫化工股份有限公司 Reaction crystallization equipment for nitrate production
CN117919766B (en) * 2024-03-22 2024-06-04 山西磊鑫化工股份有限公司 Reaction crystallization equipment for nitrate production

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117224993A (en) * 2023-11-11 2023-12-15 河北华晨药业集团有限公司 Crystallization reactor for pharmaceutical chemical industry
CN117224993B (en) * 2023-11-11 2024-01-12 河北华晨药业集团有限公司 Crystallization reactor for pharmaceutical chemical industry
CN117919766A (en) * 2024-03-22 2024-04-26 山西磊鑫化工股份有限公司 Reaction crystallization equipment for nitrate production
CN117919766B (en) * 2024-03-22 2024-06-04 山西磊鑫化工股份有限公司 Reaction crystallization equipment for nitrate production

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Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20211122

Address after: 225400 No. 61, South Street, Xuanbao Town, Taixing City, Taizhou City, Jiangsu Province

Patentee after: Jiangsu Aite Instrument Co.,Ltd.

Address before: 215600 Zhangjiagang Hexing chemical machinery factory, Hexing street, Jinfeng Town, Zhangjiagang City, Suzhou City, Jiangsu Province

Patentee before: Zhang Liuqiao

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20210302

Termination date: 20220207