CN111715166A - Distillation residue and sludge conversion sulfur-fixing agent reaction kettle - Google Patents
Distillation residue and sludge conversion sulfur-fixing agent reaction kettle Download PDFInfo
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- CN111715166A CN111715166A CN202010570637.XA CN202010570637A CN111715166A CN 111715166 A CN111715166 A CN 111715166A CN 202010570637 A CN202010570637 A CN 202010570637A CN 111715166 A CN111715166 A CN 111715166A
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- Prior art keywords
- pipe
- kettle body
- fixedly connected
- reaction kettle
- residue
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 88
- 238000004821 distillation Methods 0.000 title claims abstract description 44
- 239000010802 sludge Substances 0.000 title claims abstract description 26
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 21
- 238000005070 sampling Methods 0.000 claims abstract description 41
- 239000003814 drug Substances 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 12
- 229910052717 sulfur Inorganic materials 0.000 claims description 11
- 239000011593 sulfur Substances 0.000 claims description 11
- 230000005540 biological transmission Effects 0.000 claims description 8
- 244000309464 bull Species 0.000 claims description 7
- 238000007599 discharging Methods 0.000 claims description 7
- 229910000831 Steel Inorganic materials 0.000 claims description 5
- 239000010959 steel Substances 0.000 claims description 5
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 4
- 229910052748 manganese Inorganic materials 0.000 claims description 4
- 239000011572 manganese Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 238000003756 stirring Methods 0.000 description 18
- 238000007790 scraping Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 239000013043 chemical agent Substances 0.000 description 3
- 239000005864 Sulphur Substances 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C18/00—Disintegrating by knives or other cutting or tearing members which chop material into fragments
- B02C18/06—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
- B02C18/14—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within horizontal containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/0804—Cleaning containers having tubular shape, e.g. casks, barrels, drums
- B08B9/0808—Cleaning containers having tubular shape, e.g. casks, barrels, drums by methods involving the use of tools, e.g. by brushes, scrapers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Food Science & Technology (AREA)
- Mechanical Engineering (AREA)
- Environmental & Geological Engineering (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a distillation residue and sludge conversion sulfur-fixing agent reaction kettle, which belongs to the technical field of sulfur-fixing agent products and comprises a reaction kettle body, wherein the left side of the top of the reaction kettle body is communicated with a sludge pipe, the top of the reaction kettle body is communicated with a medicament pipe, the right side of the top of the reaction kettle body is communicated with a residue pipe, the front side and the back side of the inner wall of the residue pipe are fixedly connected with fixed cutters which are arranged equidistantly, the inner part of the residue pipe is rotatably connected with a rotating shaft, the right end of the rotating shaft penetrates through and extends to the right side of the residue pipe, and the front side and the back side of the rotating shaft are fixedly connected with rotating cutters which are arranged equidistantly and are positioned in the residue pipe. The invention solves the problems that distillation residues are attached to the inner wall of a reaction kettle to influence the reaction, the distillation residues are likely to agglomerate to block a feed material, a special distillation residue chopping device is required to be installed, the production cost is increased, and the product sampling is inconvenient after the reaction.
Description
Technical Field
The invention relates to the technical field of sulfur fixing agent products, in particular to a distillation residue and sludge conversion sulfur fixing agent reaction kettle.
Background
The application market prospect of distillation residues and sludge conversion sulfur-fixing agent products in the chemical industry is wide, the gap between the total amount of the chemical distillation residues and the sludge conversion sulfur-fixing agent products is large, the lowest collection and treatment cost of the current dangerous waste market is 5300 yuan per ton, but the production cost of the conversion sulfur-fixing agent products needs 2800 yuan per ton, the minimum amount of the conversion sulfur-fixing agent products can be 2500 yuan per ton, and the treatment method has great economic benefit, and the treatment method is gradually replacing the chemical sludge and chemical distillation residues incineration treatment method.
At present, distillation residue and sludge conversion sulfur fixing agent need stir and add the medicament modulation in reation kettle, consider summer temperature hot, can lead to the distillation residue to adhere to the inner wall at reation kettle, influence going on of reaction, weather is cold winter, distillation residue is probably the caking, can produce the jam when the pan feeding, need install special distillation residue device of cutting up, the manufacturing cost has been increased, and after the reaction, the product need the sampling to detect, current reation kettle samples inconveniently, for this reason, distillation residue and sludge conversion sulfur fixing agent reation kettle are provided and the above-mentioned problem is solved.
Disclosure of Invention
1. Technical problem to be solved
Aiming at the problems in the prior art, the invention aims to provide a reaction kettle for converting distillation residues and sludge into a sulfur fixing agent, which has the advantages of cleaning residues on the inner wall of the reaction kettle, chopping the distillation residues and conveniently sampling after reaction, and solves the problems that the distillation residues are attached to the inner wall of the reaction kettle to influence the reaction, the distillation residues are likely to agglomerate to block the feeding material, a special distillation residue chopping device is required to be installed, the production cost is increased, and the products are inconvenient to sample after reaction.
2. Technical scheme
In order to solve the above problems, the present invention adopts the following technical solutions.
Distillation residue and solid sulphur agent reation kettle of sludge transformation, including the reation kettle body, the left side intercommunication at reation kettle body top has the sludge pipe, the top intercommunication of reation kettle body has the medicament pipe, the right side intercommunication at reation kettle body top has the residue pipe, the front of residue inside pipe wall all fixedly connected with the back fixed cutter that the equidistance was arranged, the inside rotation of residue pipe is connected with the pivot, the right-hand member of pivot runs through and extends to the right side of residue pipe, the front of pivot all fixedly connected with the back equidistance is arranged and is located the inside rotary cutter of residue pipe, the bottom intercommunication of reation kettle body has the discharging pipe, the right side of reation kettle body is through fixed plate fixed mounting has the motor, the output shaft fixedly connected with bull stick of motor, the left end of bull stick runs through and extends to the inside of reation kettle body, the bull stick all cup jointed the belt pulley with the right-hand member of pivot, a transmission belt is connected between the two belt pulleys in a transmission manner, a first bevel gear is sleeved at the left end of the rotating rod, a rotating rod is rotatably connected to the inner top wall of the reaction kettle body, a second bevel gear is sleeved at the outer side of the rotating rod and is meshed with the first bevel gear, connecting sleeves are sleeved at the two ends of the rotating rod, stirring rods distributed in an annular manner are fixedly connected to the outer sides of the two connecting sleeves, a connecting plate is fixedly connected to one end of each stirring rod, which is far away from the connecting sleeves, arc-shaped scraping plates are fixedly connected to one side, which is close to the inner wall of the reaction kettle body, of the connecting plate, one side, which is far away from the connecting plate, is contacted with the inner wall of the reaction kettle body, a sampling pipe is communicated with the bottom of the right side of the reaction kettle body, a lead screw is rotatably connected to the inner, the outside threaded connection of lead screw has the carriage release lever, the left end fixedly connected with sample piece of carriage release lever, the bottom intercommunication of sample pipe has the connecting pipe, the outside threaded connection of connecting pipe has the sample jar.
Preferably, the bottom fixedly connected with helical blade of dwang, helical blade's bottom extends to the inside of discharging pipe, helical blade is made for high manganese wear-resisting steel material.
Preferably, the left side fixedly connected with locating lever of the internal wall of reation kettle, the right-hand member fixedly connected with holding ring of locating lever, the bottom of dwang is rotated with the inboard of holding ring and is connected.
Preferably, the spout has been seted up to the interior roof of sampling pipe, the right side fixed connection limit slide at carriage release lever top, limit slide extends to the inside of spout and rather than sliding connection.
Preferably, the top of the sample tank is fixedly connected with an internal thread ring, and the outer side of the connecting pipe is provided with an external thread.
Preferably, the right side of the reaction kettle body is embedded with a framework oil seal, and the outer side of the rotating rod is fixedly connected with the inner ring of the framework oil seal.
3. Advantageous effects
Compared with the prior art, the invention has the advantages that:
(1) the scheme includes that distillation residues are thrown into a residue pipe, a driving motor enables a rotating rod to rotate, the rotating rod drives a driving belt through a belt pulley at the bottom, the belt pulley at the top is driven by the driving belt to enable a rotating shaft to rotate, the rotating shaft drives a rotating cutter to be matched with a fixed cutter in a rotating mode to cut up the distillation residues caked in winter, blockage of the residue pipe is avoided, meanwhile, the rotating rod drives a first bevel gear to rotate, the rotating rod can rotate due to meshing of the first bevel gear and a second bevel gear, the rotating rod drives a stirring rod to rotate through a connecting sleeve, the stirring rod can stir and enable the reaction to be complete, the stirring rod drives a connecting plate to rotate, the connecting plate enables a plurality of arc-shaped scraping plates to slide on the inner wall of a reaction kettle body, distillation residues attached to the inner wall of the reaction kettle body can be scraped off, hot temperature in summer is avoided, the distillation, the operation can be completed only by a driving motor, the machine has multiple functions, the production cost is reduced, after the reaction is completed, the screw rod is rotated by rotating the turntable, the moving rod which is connected with the screw threads on the outer side of the screw rod moves towards the inside of the reaction kettle body along the screw rod by rotating the screw rod, the turntable is reversed again to drive the moving rod to drive the sampling block to reset, when the sampling block is reset, the product can enter the inside of the sampling block and push part of the product to enter the sampling pipe along with the resetting of the sampling block, the product can enter the sampling pipe and be discharged into the inside of the sample tank from the connecting pipe, the sampling can be completed by unscrewing the sample tank, the sampling can be completed only by rotating the turntable once in the positive and negative directions, the operation is simple and convenient, the problem that the distillation residues are attached to the inner wall of the reaction kettle to influence the reaction is solved, the distillation residues are likely to be agglomerated to block the, and the product sampling is inconvenient after the reaction.
(2) The helical blade that this scheme was made by high manganese wear-resisting steel material long service life prevents that the condition that the discharging pipe took place to block up during the ejection of compact from appearing.
(3) This scheme can fix a position the dwang by locating lever and holding ring to guarantee dwang pivoted stability, reduce the possibility that takes place to rock.
(4) This scheme drives the sample piece when internal sample to reation kettle at the carriage release lever, and the carriage release lever can drive spacing slider and slide in the inside of spout, carries on spacingly by the cooperation of spacing slider and spout to the removal of carriage release lever, prevents that carriage release lever and lead screw from breaking away from the phenomenon appearance that causes unable sample.
(5) This scheme can cooperate the external screw thread in the connecting pipe outside through the internal thread ring to make threaded connection between sample jar and the connecting pipe, conveniently connects and dismantles, is convenient for collect the product in the sample jar and detects.
(6) The scheme can seal the joint of the rotating rod and the reaction kettle body by the arrangement of the framework oil seal, so that the sealing property of the reaction is ensured, and the abrasion of the rotating rod is avoided.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is an enlarged view taken at A in FIG. 1 according to the present invention;
FIG. 3 is a schematic top cross-sectional view of an arcuate squeegee blade of the invention;
FIG. 4 is a top view of the residue pipe of the present invention.
The reference numbers in the figures illustrate:
1. a reaction kettle body; 2. a sludge pipe; 3. a drug tube; 4. a residue pipe; 5. fixing the cutter; 6. a rotating shaft; 7. rotating the cutter; 8. a discharge pipe; 9. a motor; 10. a rotating rod; 11. a belt pulley; 12. a transmission belt; 13. a first bevel gear; 14. rotating the rod; 15. a second bevel gear; 16. connecting sleeves; 17. a stirring rod; 18. a connecting plate; 19. an arc-shaped scraper plate; 20. a sampling tube; 21. a screw rod; 22. a travel bar; 23. a sampling block; 24. a connecting pipe; 25. a sample tank; 26. a helical blade; 27. positioning a rod; 28. a positioning ring; 29. a chute; 30. a limiting slide block; 31. an internally threaded ring; 32. framework oil seal; 33. a turntable.
Detailed Description
The technical solution in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention; it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments, and all other embodiments obtained by those skilled in the art without any inventive work are within the scope of the present invention.
In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "top/bottom", and the like indicate orientations or positional relationships based on those shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "sleeved/connected," "connected," and the like are to be construed broadly, e.g., "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1-4, a distillation residue and sludge conversion sulfur fixing agent reaction kettle comprises a reaction kettle body 1, the left side of the top of the reaction kettle body 1 is communicated with a sludge pipe 2, the top of the reaction kettle body 1 is communicated with a chemical agent pipe 3, sludge and a chemical agent are respectively fed into the reaction kettle body 1 through the sludge pipe 2 and the chemical agent pipe 3, the right side of the top of the reaction kettle body 1 is communicated with a residue pipe 4, the front side and the back side of the inner wall of the residue pipe 4 are fixedly connected with fixed cutters 5 arranged at equal intervals, the inner part of the residue pipe 4 is rotatably connected with a rotating shaft 6, the right end of the rotating shaft 6 penetrates through and extends to the right side of the residue pipe 4, the front side and the back side of the rotating shaft 6 are fixedly connected with rotating cutters 7 arranged at equal intervals and positioned in the residue pipe 4, the bottom of the reaction kettle body 1 is communicated with a discharge pipe 8, the right side of the reaction kettle body 1 is, the motor 9 makes the rotating rod 10 rotate, the left end of the rotating rod 10 penetrates and extends to the inside of the reaction kettle body 1, the right ends of the rotating rod 10 and the rotating shaft 6 are respectively sleeved with a belt pulley 11, a transmission belt 12 is connected between the two belt pulleys 11 in a transmission way, the rotating rod 10 drives the transmission belt 12 through the bottom belt pulley 11, the transmission belt 12 drives the belt pulley 11 at the top to rotate the rotating shaft 6, the rotating cutter 7 is driven by the rotating shaft 6 to be in rotating fit with the fixed cutter 5 to cut up the distillation residues caked in winter, so as to avoid blocking the residue pipe 4, the left end of the rotating rod 10 is sleeved with a first bevel gear 13, the rotating rod 10 drives the first bevel gear 13 to rotate, the inner top wall of the reaction kettle body 1 is rotatably connected with a rotating rod 14, the outer side of the rotating rod 14 is sleeved with a second bevel gear 15, the second bevel gear 15 is meshed with the first bevel gear 13, the rotating, the two ends of the rotating rod 14 are sleeved with the connecting sleeves 16, the outer sides of the two connecting sleeves 16 are fixedly connected with stirring rods 17 distributed in an annular shape, the rotating rod 14 drives the stirring rods 17 to rotate through the connecting sleeves 16, the stirring rods 17 can stir to enable the reaction to be sufficient, one ends of the stirring rods 17 far away from the connecting sleeves 16 are fixedly connected with connecting plates 18, one sides of the connecting plates 18 close to the inner wall of the reaction kettle body 1 are fixedly connected with arc-shaped scraping plates 19 arranged at equal intervals, one sides of the arc-shaped scraping plates 19 far away from the connecting plates 18 are in contact with the inner wall of the reaction kettle body 1, the stirring rods 17 drive the connecting plates 18 to rotate, the connecting plates 18 enable the arc-shaped scraping plates 19 to slide on the inner wall of the reaction kettle body 1, distillation residues attached to the inner wall of the reaction kettle body 1 can be scraped, the hot temperature in summer can be avoided, the distillation residues can be attached to, sampling pipe 20's inside is rotated and is connected with lead screw 21, the right-hand member of lead screw 21 runs through and extends to sampling pipe 20's right side and fixedly connected with carousel 33, the outside threaded connection of lead screw 21 has carriage release lever 22, the left end fixedly connected with sampling piece 23 of carriage release lever 22, the bottom intercommunication of sampling pipe 20 has connecting pipe 24, the outside threaded connection of connecting pipe 24 has sample jar 25, it makes lead screw 21 rotate to rotate carousel 33 to rotate, carriage release lever 22 removes to the inside of reation kettle body 1, reversal carousel 33 makes carriage release lever 22 drive sampling piece 23 reset again, along with the reseing of sampling piece 23, can make the product get into sampling pipe 20 and follow the inside that connecting pipe 24 discharged into sample jar 25, unscrew sample jar 25 and can accomplish the sampling.
Further, the bottom fixedly connected with helical blade 26 of dwang 14, helical blade 26's bottom extends to the inside of discharging pipe 8, and helical blade 26 is made for the wear-resisting steel material of high manganese, and helical blade 26 long service life who is made by the wear-resisting steel material of high manganese takes place the condition appearance that blocks up when preventing the ejection of compact discharging pipe 8.
Further, the left side fixedly connected with locating lever 27 of the 1 inner wall of the reaction kettle body, the right-hand member fixedly connected with holding ring 28 of locating lever 27, the bottom of dwang 14 is rotated with the inboard of holding ring 28 and is connected, can fix a position dwang 14 by locating lever 27 and holding ring 28 to guarantee dwang 14 pivoted stability, reduce the possibility that the emergence was rocked.
Further, spout 29 has been seted up to the interior roof of sampling pipe 20, the right side fixed connection limit slide 30 at carriage release lever 22 top, limit slide 30 extends to the inside of spout 29 and rather than sliding connection, when carriage release lever 22 drives sampling block 23 and takes a sample to the reation kettle body 1 in, carriage release lever 22 can drive limit slide 30 and slide in the inside of spout 29, it is spacing to carry out by limit slide 30 and the cooperation of spout 29 the removal of carriage release lever 22, prevent that carriage release lever 22 and lead screw 21 from breaking away from the phenomenon appearance that causes unable sampling.
Further, the top fixed connection of sample tank 25 has internal thread ring 31, and the outside of connecting pipe 24 is provided with the external screw thread, can cooperate the external screw thread in the connecting pipe 24 outside through internal thread ring 31 to make threaded connection between sample tank 25 and the connecting pipe 24, and the product of being convenient for collect in sample tank 25 is detected with dismantling to the convenient connection.
Further, the right side of the reaction kettle body 1 is embedded with a framework oil seal 32, the outer side of the rotating rod 10 is fixedly connected with the inner ring of the framework oil seal 32, the connecting part of the rotating rod 10 and the reaction kettle body 1 can be sealed by the framework oil seal 32, the reaction tightness is ensured, and the rotating rod 10 is prevented from being abraded.
The model of the motor 9 may be Y90L-4, and other electrical components used in this embodiment may be used, and the electronic components are all connected to an external power supply and a control switch, and the specific circuit connection manner and the use method thereof are commonly disclosed technologies, and thus, redundant description is not repeated here.
The working principle is as follows: when the invention is used, firstly, sludge and medicament are respectively put into a reaction kettle body 1 through a sludge pipe 2 and a medicament pipe 3, distillation residues are put into the reaction kettle body 1 through a residue pipe 4, a driving motor 9 enables a rotating rod 10 to rotate, the rotating rod 10 drives a driving belt 12 through a belt pulley 11 at the bottom, the belt pulley 11 at the top is driven by the driving belt 12 to enable a rotating shaft 6 to rotate, the rotating shaft 6 drives a rotating cutter 7 to rotate to match with a fixed cutter 5 to cut up the distillation residues caked in winter, so as to avoid the blockage of the residue pipe 4, meanwhile, the rotating rod 10 drives a first bevel gear 13 to rotate, the rotating rod 14 can rotate through the meshing of the first bevel gear 13 and a second bevel gear 15, the rotating rod 14 drives a stirring rod 17 to rotate through a connecting sleeve 16, the stirring rod 17 can stir to enable the reaction to be full, the stirring rod 17 drives a connecting plate 18 to rotate, the connecting plate 18 enables a plurality, the distillation residue attached to the inner wall of the reaction kettle body 1 can be scraped, the phenomenon that the distillation residue is attached to the inner wall of the reaction kettle body 1 to influence the reaction in summer due to hot temperature is avoided, the operation can be completed only by driving the motor 9, the device has multiple purposes, and the production cost is reduced, after the reaction is completed, the screw rod 21 is rotated by rotating the turntable 33, the movable rod 22 which is connected with the outer side in a threaded manner is moved to the inside of the reaction kettle body 1 along the screw rod 21 by the rotation of the screw rod 21, the turntable 33 is reversed again to drive the movable rod 22 to drive the sampling block 23 to reset, when the reset is completed, the product enters the inside of the sampling block 23, and the sampling block 23 can push partial product to enter the sampling pipe 20, along with the reset of the sampling block 23, the product can enter the sampling pipe 20 and be discharged into the inside of the sample tank 25 from the connecting pipe 24, the sampling can be completed by screwing down the sample tank 25, and the sampling can be, the operation is simple and convenient, the problem that the distillation residues are attached to the inner wall of the reaction kettle to influence the reaction is solved, the distillation residues are likely to agglomerate to cause the feed blockage, a special distillation residue chopping device needs to be installed, the production cost is increased, and the product sampling is inconvenient after the reaction.
The foregoing is only a preferred embodiment of the present invention; the scope of the invention is not limited thereto. Any person skilled in the art should be able to cover the technical scope of the present invention by equivalent or modified solutions and modifications within the technical scope of the present invention.
Claims (6)
1. Distillation residue and mud conversion sulfur-fixing agent reation kettle, including the reation kettle body (1), its characterized in that: the left side intercommunication at the reation kettle body (1) top has sludge pipe (2), the top intercommunication of the reation kettle body (1) has medicament pipe (3), the right side intercommunication at the reation kettle body (1) top has residue pipe (4), the front of residue pipe (4) inner wall and the equal fixedly connected with in back of the fixed cutter (5) that the equidistance was arranged, the inside rotation of residue pipe (4) is connected with pivot (6), the right-hand member of pivot (6) runs through and extends to the right side of residue pipe (4), the front of pivot (6) and the equal fixedly connected with in back of pivot are arranged and are located the inside rotating cutter (7) of residue pipe (4) equidistance, the bottom intercommunication of the reation kettle body (1) has discharging pipe (8), the right side of the reation kettle body (1) is through fixed plate fixed mounting have motor (9), the output shaft fixedly connected with bull stick (10) of motor (9), the left end of bull stick (10) runs through and extends to the inside of the reation kettle body (1), belt pulley (11), two have all been cup jointed with the right-hand member of pivot (6) in bull stick (10) the transmission is connected with drive belt (12) between belt pulley (11), first bevel gear (13) have been cup jointed to the left end of bull stick (10), the interior roof of the reation kettle body (1) rotates and is connected with dwang (14), second bevel gear (15) have been cup jointed in the outside of dwang (14), second bevel gear (15) and first bevel gear (13) meshing, adapter sleeve (16), two have been cup jointed at the both ends of dwang (14) the equal fixedly connected with annular agitator arm (17) that distributes in the outside of adapter sleeve (16), the equal fixedly connected with connecting plate (18) of one end that adapter sleeve (16) was kept away from agitator arm (17), arc one side fixedly connected with equidistance that connecting plate (18) are close to reation kettle body (1) inner wall is arranged Scraper blade (19), one side of connecting plate (18) and the inner wall contact of the reation kettle body (1) are kept away from to arc scraper blade (19), the bottom intercommunication on reation kettle body (1) right side has sampling pipe (20), the inside of sampling pipe (20) is rotated and is connected with lead screw (21), the right-hand member of lead screw (21) runs through and extends to right side and fixedly connected with carousel (33) of sampling pipe (20), the outside threaded connection of lead screw (21) has carriage release lever (22), the left end fixedly connected with sampling piece (23) of carriage release lever (22), the bottom intercommunication of sampling pipe (20) has connecting pipe (24), the outside threaded connection of connecting pipe (24) has sample jar (25).
2. The distillation residue and sludge conversion sulfur fixing agent reaction kettle according to claim 1, characterized in that: the bottom end fixedly connected with helical blade (26) of dwang (14), the bottom of helical blade (26) extends to the inside of discharging pipe (8), helical blade (26) are made for high manganese wear-resisting steel material.
3. The distillation residue and sludge conversion sulfur fixing agent reaction kettle according to claim 1, characterized in that: the left side fixedly connected with locating lever (27) of the internal wall of reation kettle (1), the right-hand member fixedly connected with holding ring (28) of locating lever (27), the bottom of dwang (14) rotates with the inboard of holding ring (28) to be connected.
4. The distillation residue and sludge conversion sulfur fixing agent reaction kettle according to claim 1, characterized in that: spout (29) have been seted up to the interior roof of sample pipe (20), the right side fixed connection limit slide (30) at carriage release lever (22) top, limit slide (30) extend to the inside of spout (29) and rather than sliding connection.
5. The distillation residue and sludge conversion sulfur fixing agent reaction kettle according to claim 1, characterized in that: the top of sample jar (25) is fixed connection has interior screw thread ring (31), the outside of connecting pipe (24) is provided with the external screw thread.
6. The distillation residue and sludge conversion sulfur fixing agent reaction kettle according to claim 1, characterized in that: the right side of the reaction kettle body (1) is embedded with a framework oil seal (32), and the outer side of the rotating rod (10) is fixedly connected with the inner ring of the framework oil seal (32).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112284091A (en) * | 2020-11-07 | 2021-01-29 | 湖南德之聚新材料有限公司 | Powder wall stagnation-free iron oxide black drying tower |
| CN114345498A (en) * | 2021-12-29 | 2022-04-15 | 图方便（苏州）环保科技有限公司 | Toilet sewage discharging device with fermentation and crushing functions and application thereof |
| CN114371109A (en) * | 2022-01-18 | 2022-04-19 | 合肥清风环保科技有限公司 | Oil smoke online detection device capable of preventing oil stain residue and detection method thereof |
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| CN112284091A (en) * | 2020-11-07 | 2021-01-29 | 湖南德之聚新材料有限公司 | Powder wall stagnation-free iron oxide black drying tower |
| CN114345498A (en) * | 2021-12-29 | 2022-04-15 | 图方便（苏州）环保科技有限公司 | Toilet sewage discharging device with fermentation and crushing functions and application thereof |
| CN114371109A (en) * | 2022-01-18 | 2022-04-19 | 合肥清风环保科技有限公司 | Oil smoke online detection device capable of preventing oil stain residue and detection method thereof |
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