CN212504151U - Deuterium removing reaction device for heavy oxygen water - Google Patents
Deuterium removing reaction device for heavy oxygen water Download PDFInfo
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- CN212504151U CN212504151U CN202020984420.9U CN202020984420U CN212504151U CN 212504151 U CN212504151 U CN 212504151U CN 202020984420 U CN202020984420 U CN 202020984420U CN 212504151 U CN212504151 U CN 212504151U
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- oxygen water
- heavy oxygen
- deuterium
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Abstract
The utility model discloses a deuterium removing reaction device for heavy oxygen water, which comprises a deuterium removing reaction device body for heavy oxygen water and a hydrogen generator, wherein the deuterium removing reaction device body for heavy oxygen water is provided with a tail gas emission collection inlet, an isotope heavy oxygen water stock solution inlet, a glass conduit, a heavy oxygen water synthesis reaction device, a flowmeter, a condensing device, a heavy oxygen water reaction electrode plate, a stock solution tank, a condensate water inlet, a heavy oxygen water reaction electrode plate and a condensate water outlet, the deuterium removing reaction device body for heavy oxygen water generates hydrogen by an electrolytic method, potassium hydroxide aqueous solution is used as electrolyte, noble metal is used as an electrode, the hydrogen and oxygen are thoroughly separated by adopting the Zhonghepu latest membrane separation technology, and a transition metal catalysis technology is adopted in an electrolytic cell, so that the oxygen content in hydrogen generation is less than 3ppm, the beneficial effects of the utility model are small in volume, the sample loss is relatively small, the generated gas is relatively pure, and the eighteen oxygen gases are prevented from being lost in the electrolytic process.
Description
Technical Field
The utility model relates to a deuterium removing technology for heavy oxygen water and the technical field of oxygen and hydrogen reaction, in particular to a deuterium removing reaction device for heavy oxygen water.
Background
In the existing technical field, the deuterium normalization process of heavy oxygen water is not many, generally, deuterium in heavy oxygen water is removed by an electrolytic method, generated oxygen octadeca gas is collected to react with high-purity hydrogen to generate deuterium normalization heavy oxygen water, and in the electrolytic method deuterium removal process, a pure water hydrogen generator is used for electrolytic deuterium removal, but because an electrolytic tank is too large, more heavy oxygen water is consumed, and the deuterium normalization process is not widely applied.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a small, the sample loss is less relatively, and the gaseous ratio of production is purer, avoids oxygen eighteen gaseous heavy oxygen water deuterium removing reaction unit that runs off at the electrolysis in-process to solve the problem that proposes in the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: the heavy oxygen water deuterium removing reaction device comprises a heavy oxygen water deuterium removing reaction device body and a hydrogen generator, wherein the hydrogen generator is arranged on the heavy oxygen water deuterium removing reaction device body, a glass guide pipe is arranged above the hydrogen generator, a heavy oxygen water synthesis reaction device is arranged at one end of the glass guide pipe, a flowmeter is arranged on the glass guide pipe above the right of the heavy oxygen water synthesis reaction device, and a condensing device is arranged on the glass guide pipe in the center of the bottom of the heavy oxygen water synthesis reaction device.
Preferably, the left end of the hydrogen generator is provided with a tail gas discharge collection inlet, the right end of the hydrogen generator is provided with an isotope heavy oxygen water stock solution inlet, a stock solution tank is arranged inside the hydrogen generator, a glass guide pipe is arranged between the bottom of the outer left end of the stock solution tank and the left end, the bottom of the outer left end of the stock solution tank and the glass guide pipe in the middle of the left end are connected with a heavy oxygen water reaction electrode plate, the left end of the heavy oxygen water reaction electrode plate is connected with the tail gas discharge collection inlet, a condensate water spiral pipeline is arranged inside the stock solution tank, and the middle of the outer wall of the right side of the stock solution tank is connected with the isotope heavy oxygen water stock solution inlet.
Preferably, a condensed water outlet is arranged at the upper end of the condensed water spiral pipeline, and a condensed water inlet is arranged at the bottom end of the condensed water spiral pipeline.
Preferably, the heavy oxygen water reaction electrode plate is connected with 220V voltage.
Preferably, a glass conduit between the hydrogen generator and the heavy oxygen water synthesis reaction device inputs oxygen eighteen gases into the heavy oxygen water synthesis reaction device.
Preferably, a glass conduit between the flow meter and the heavy oxygen water synthesis reaction device inputs 99.999 percent of high-purity hydrogen into the heavy oxygen water synthesis reaction device.
Preferably, the heavy oxygen water synthesis reaction device inputs isotope heavy oxygen water vapor into the condensing device.
Compared with the prior art, the beneficial effects of the utility model are that:
(1) the utility model discloses it is small, the sample loss is less relatively, and the gas of production is purer, avoids oxygen eighteen gas to run off at the electrolysis in-process.
Drawings
FIG. 1 is a schematic view of the structure of the heavy oxygen water deuterium removing reaction apparatus of the present invention;
fig. 2 is a schematic diagram of the structure of the hydrogen generator of the present invention.
In the figure: 1. a tail gas discharge collection inlet; 2. a liquid inlet for isotope heavy oxygen water stock solution; 3. a glass conduit; 4. a heavy oxygen water synthesis reaction device; 5. a flow meter; 6. a condensing unit; 7. a heavy oxygen water reaction electrode plate; 8. a stock solution tank; 9. a condensed water inlet; 10. a condensate spiral pipe; 11. a condensed water outlet; 12. a hydrogen generator; 13. deuterium removing reaction device body for heavy oxygen water.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1, the present invention provides a technical solution: a deuterium removing reaction device for heavy oxygen water comprises a deuterium removing reaction device body 13 for heavy oxygen water, the hydrogen generator 12 is arranged on a hydrogen generator 12 body 13 of the deuterium removing reaction device for the heavy oxygen water, a glass guide pipe 3 is arranged above the hydrogen generator 12, one end of the glass guide pipe 3 is provided with a deuterium synthesizing reaction device 4, the glass guide pipe 3 between the hydrogen generator 12 and the deuterium synthesizing reaction device 4 inputs eighteen-oxygen gas into the deuterium synthesizing reaction device 4, the glass guide pipe 3 at the upper right of the deuterium synthesizing reaction device 4 is provided with a flow meter 5, the glass guide pipe 3 between the flow meter 5 and the deuterium synthesizing reaction device 4 inputs 99.999 percent high-purity hydrogen into the deuterium synthesizing reaction device 4, the glass guide pipe 3 at the center of the bottom of the deuterium synthesizing reaction device 4 is provided with a condensing device 6, and the deuterium synthesizing reaction device 4 inputs isotope heavy oxygen water vapor into the condensing device 6.
The left end of the hydrogen generator 12 is provided with a tail gas discharge collection inlet 1, the right end of the hydrogen generator 12 is provided with an isotope heavy oxygen water stock solution inlet 2, the hydrogen generator 12 is internally provided with a stock solution tank 8, the bottoms of the outer left ends of the stock solution tank 8 and the middle of the left end are both provided with glass guide pipes 3, and the bottoms of the outer left ends of the stock solution tank 8 and the middle of the left end are connected with a heavy oxygen water reaction electrode plate 7 through the glass guide pipes 3.
The left end of heavy oxygen water reaction electrode plate 7 is connected with tail gas exhaust collection inlet 1, and the inside of raw liquor tank 8 is equipped with comdenstion water helical tube 10, and the upper end of comdenstion water helical tube 10 is equipped with comdenstion water export 11, and the bottom of comdenstion water helical tube 10 is equipped with comdenstion water inlet 9, is connected with isotope heavy oxygen water raw liquor inlet 2 in the middle of the right side outer wall of raw liquor tank 8.
Firstly, a condensed water outlet 11 and a condensed water inlet 9 are connected into a condensed water system, a raw liquid tank 8 is made to be in a low-temperature environment, raw liquid is added from a isotope heavy oxygen water raw liquid inlet 2, waiting for 5 minutes, the liquid is cooled to 2 ℃, a heavy oxygen water reaction electrode plate 7 is connected with 220V voltage to start reaction, deuterium and oxygen in heavy oxygen water are separated, oxygen eighteen gas starts to be generated at the moment, the deuterium and oxygen eighteen gas enter a heavy oxygen water synthesis reaction device 4 along a pipeline, a hydrogen flowmeter 5 is adjusted, high-purity hydrogen enters the heavy oxygen water synthesis reaction device 4 along a glass conduit 3, two mixed gases, high-purity hydrogen 5 and oxygen eighteen gas prepared by electrolysis react under the action of a catalyst, and the deuterium is removed by synthesizing the oxygen eighteen water.
The utility model discloses it is small, the sample loss is less relatively, and the gas of production is purer, avoids oxygen eighteen gas to run off at the electrolysis in-process.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The utility model provides a heavy oxygen water deuterium removing reaction device, includes heavy oxygen water deuterium removing reaction device body (13), hydrogen generator (12), its characterized in that: the deuterium removing reaction device for the heavy oxygen water is characterized in that a hydrogen generator (12) is arranged on the heavy oxygen water deuterium removing reaction device body (13), a glass guide pipe (3) is arranged above the hydrogen generator (12), a heavy oxygen water synthesis reaction device (4) is arranged at one end of the glass guide pipe (3), a flowmeter (5) is arranged on the glass guide pipe (3) above the right of the heavy oxygen water synthesis reaction device (4), and a condensing device (6) is arranged on the glass guide pipe (3) in the center of the bottom of the heavy oxygen water synthesis reaction device (4).
2. The heavy oxygen water deuterium removing reaction apparatus according to claim 1, wherein: the left end of hydrogen generator (12) is equipped with tail gas emission and collects entry (1), the right-hand member of hydrogen generator (12) is equipped with isotope heavy oxygen water stock solution inlet (2), the inside of hydrogen generator (12) is equipped with crude liquid jar (8), all be equipped with glass pipe (3) in the middle of the outside left end bottom and the left end of crude liquid jar (8), the outside left end bottom of crude liquid jar (8) is connected with heavy oxygen water reaction electrode board (7) with glass pipe (3) in the middle of the left end, the left end and the tail gas emission of heavy oxygen water reaction electrode board (7) are collected entry (1) and are connected, and the inside of crude liquid jar (8) is equipped with comdenstion water helical tube (10), be connected with isotope heavy oxygen water stock solution inlet (2) in the middle of the right side outer wall of crude liquid jar (8).
3. The heavy oxygen water deuterium removing reaction apparatus according to claim 2, wherein: the upper end of the condensed water spiral pipeline (10) is provided with a condensed water outlet (11), and the bottom end of the condensed water spiral pipeline (10) is provided with a condensed water inlet (9).
4. The heavy oxygen water deuterium removing reaction apparatus according to claim 2, wherein: the heavy oxygen water reaction electrode plate (7) is connected with 220V voltage.
5. The heavy oxygen water deuterium removing reaction apparatus according to claim 1, wherein: and eighteen oxygen gases are input into the heavy oxygen water synthesis reaction device (4) through a glass conduit (3) between the hydrogen generator (12) and the heavy oxygen water synthesis reaction device (4).
6. The heavy oxygen water deuterium removing reaction apparatus according to claim 1, wherein: the glass conduit (3) between the flowmeter (5) and the heavy oxygen water synthesis reaction device (4) inputs 99.999 percent of high-purity hydrogen into the heavy oxygen water synthesis reaction device (4).
7. The heavy oxygen water deuterium removing reaction apparatus according to claim 1, wherein: the heavy oxygen water synthesis reaction device (4) inputs isotope heavy oxygen water vapor into the condensing device (6).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020984420.9U CN212504151U (en) | 2020-06-02 | 2020-06-02 | Deuterium removing reaction device for heavy oxygen water |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020984420.9U CN212504151U (en) | 2020-06-02 | 2020-06-02 | Deuterium removing reaction device for heavy oxygen water |
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| CN212504151U true CN212504151U (en) | 2021-02-09 |
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| CN202020984420.9U Active CN212504151U (en) | 2020-06-02 | 2020-06-02 | Deuterium removing reaction device for heavy oxygen water |
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- 2020-06-02 CN CN202020984420.9U patent/CN212504151U/en active Active
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