CN211752617U - Crystallization device for chemical reagent preparation - Google Patents
Crystallization device for chemical reagent preparation Download PDFInfo
- Publication number
- CN211752617U CN211752617U CN201922404779.4U CN201922404779U CN211752617U CN 211752617 U CN211752617 U CN 211752617U CN 201922404779 U CN201922404779 U CN 201922404779U CN 211752617 U CN211752617 U CN 211752617U
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- China
- Prior art keywords
- collection box
- evaporating pot
- fixed mounting
- cold water
- chemical reagent
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000002425 crystallisation Methods 0.000 title claims abstract description 23
- 230000008025 crystallization Effects 0.000 title claims abstract description 23
- 239000003153 chemical reaction reagent Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 45
- 238000001704 evaporation Methods 0.000 claims abstract description 38
- 238000001816 cooling Methods 0.000 claims abstract description 29
- 239000007788 liquid Substances 0.000 claims description 25
- 230000008020 evaporation Effects 0.000 claims description 16
- 238000005485 electric heating Methods 0.000 claims description 11
- 238000009833 condensation Methods 0.000 claims description 7
- 230000005494 condensation Effects 0.000 claims description 7
- 238000011049 filling Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 abstract description 4
- 206010028347 Muscle twitching Diseases 0.000 abstract 1
- 125000004122 cyclic group Chemical group 0.000 abstract 1
- 238000011084 recovery Methods 0.000 description 16
- 238000004064 recycling Methods 0.000 description 7
- 239000000945 filler Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 101100298222 Caenorhabditis elegans pot-1 gene Proteins 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004451 qualitative analysis Methods 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a device is appeared with crystallization in chemical reagent preparation, including evaporating pot, electric pole, electric cabinet, collection box and circulative cooling case, the bottom position department fixed mounting of evaporating pot one side has the collection box, the input at collection box top passes through the output fixed connection at pipe and evaporating pot one side top, the surface cover of pipe has the condenser pipe, the positive fixed mounting of collection box has circulative cooling case, the output fixed connection of hose and condenser pipe is passed through to the input of collection box. The utility model discloses set up the circulative cooling case, the miniature circulating water pump of inside newKP of circulative cooling case circulates the twitching to the inside cold water of condenser pipe, and cold water is through B3-014 miniature heat exchanger at the in-process that the circulation flows, and B3-014 miniature heat exchanger is to the cold water cooling operation once more of intensification, keeps the cold water of storage intracavity portion to keep at constant temperature, has realized carrying out cyclic utilization to these cold water simultaneously.
Description
Technical Field
The utility model relates to a chemical reagent preparation technical field specifically is a chemical reagent preparation is with crystallization device of appearing.
Background
Chemical reagents (chemical reagents) are relatively standard substances for chemical research and component analysis, are important conditions for technological progress, are widely used for synthesis, separation, qualitative and quantitative analysis of substances, can be said to be eyes of chemists, and cannot be separated from chemical reagents in daily work of factories, schools, hospitals and research institutes, and a crystallization device is required to be used for preparing the chemical reagents.
The existing crystallization device has the following defects:
1. the conventional crystallization apparatus generally performs crystallization by evaporation, but lacks a mechanism for recovering evaporated gas, and cannot recover and utilize the evaporated gas.
2. The gas generated by the existing crystallization device needs to be continuously introduced with cold water for condensation when being condensed, and the cold water cannot be recycled.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a chemical reagent preparation is with crystallization device of appearing to solve the problem that proposes in the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: a crystallization and precipitation device for preparing chemical reagents, which comprises an evaporation tank, an electric heating rod, an electric cabinet, a recovery box and a circulating cooling box, a recovery box is fixedly arranged at the bottom position of one side of the evaporation tank, the input end at the top of the recovery box is fixedly connected with the output end at the top of one side of the evaporation tank through a guide pipe, the surface of the conduit is sleeved with a condenser pipe, the front surface of the recovery box is fixedly provided with a circulating cooling box, the input end of the recovery box is fixedly connected with the output end of the condensing pipe through a hose, the output end of the recovery box is fixedly connected with the input end of the condensing pipe through a hose, the bottom of the evaporation tank is fixedly provided with a supporting leg, the bottom of the supporting leg is adhered with an anti-skid pad, one side of the evaporating pot far away from the recycling box is fixedly provided with an electric cabinet, the inside of the evaporating pot is fixedly provided with an electric heating rod, and the electric heating rod is electrically connected with the electric cabinet through a wire.
Preferably, a liquid outlet is formed in the bottom of the recycling box, and a valve is fixedly mounted on the surface of the liquid outlet.
Preferably, a NewKP micro circulating water pump is fixedly mounted at the inner top of the circulating cooling tank, the NewKP micro circulating water pump is electrically connected with the electric cabinet through a lead, the input end of the NewKP micro circulating water pump is fixedly connected with the input end of the circulating cooling tank, a B3-014 micro heat exchanger is fixedly mounted at the inner bottom of the circulating cooling tank, a B3-014 micro heat exchanger is electrically connected with the electric cabinet through a lead, the input end of the B3-014 micro heat exchanger is fixedly connected with the output end of the NewKP micro circulating water pump through a hose, and the output end of the B3-014 micro heat exchanger is fixedly connected with the output end of the circulating cooling tank.
Preferably, the inner wall of the condensation pipe is provided with a storage cavity, and cold water is stored in the storage cavity.
Preferably, one side at the evaporating pot top is equipped with the filling opening, and the top fixed mounting of filling opening has the top cap, the bottom of evaporating pot is equipped with the bin outlet, and the bottom fixed mounting of bin outlet has the bottom, and a week of bottom is equipped with anti-skidding line.
Preferably, the front surface of the electric cabinet is provided with a first control switch, a second control switch and a third control switch, and the bottom of one side of the electric cabinet is fixedly provided with a plug through a wire.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the chemical reagent preparation crystallization device is provided with the recycling box, when solution is added into the evaporation tank to be evaporated and crystallized, evaporated gas passes through the guide pipe, the condensing pipe on the surface of the guide pipe cools the gas, and then the gas is condensed into liquid to flow into the recycling box, so that the evaporated gas can be condensed into liquid to be recycled.
2. The crystallization device for preparing the chemical reagent is provided with a circulating cooling box, a NewKP micro circulating water pump in the circulating cooling box circularly pumps cold water in a condensation pipe, the cold water passes through a B3-014 micro heat exchanger in the circulating flowing process, and the B3-014 micro heat exchanger cools the heated cold water again, so that the cold water in a storage cavity is kept at a constant temperature, and the cold water is recycled.
Drawings
Fig. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic structural view of the circulation cooling box of the present invention;
fig. 3 is a schematic view of the structure of the condensation tube of the present invention.
In the figure: 1. an evaporator tank; 101. a liquid filling port; 102. a top cover; 103. a discharge outlet; 104. a bottom cover; 105. anti-skid lines; 2. an electric heating rod; 3. an electric cabinet; 301. a first control switch; 302. a second control switch; 303. a third control switch; 304. a plug; 4. a recycling bin; 401. a liquid outlet; 402. a valve; 5. a circulating cooling tank; 501. a NewKP micro circulating water pump; 502. b3-014 micro heat exchanger; 6. a conduit; 7. a condenser tube; 701. a storage chamber; 702. cold water; 8. supporting legs; 9. a non-slip mat.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front end", "rear end", "both ends", "one end", "the other end" and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element to which the reference is made must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "connected," and the like are to be construed broadly, and for example, "connected" may be either fixedly connected or detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1-3, the present invention provides an embodiment: a crystallization precipitation device for chemical reagent preparation comprises an evaporation tank 1, an electric heating rod 2, an electric cabinet 3, a recovery tank 4 and a circulating cooling tank 5, wherein a supporting leg 8 is welded at the bottom of the evaporation tank 1, the evaporation tank 1 is fixedly supported by the supporting leg 8, a non-slip mat 9 is adhered to the bottom of the supporting leg 8, the supporting stability of the supporting leg 8 is ensured by the non-slip mat 9, the electric heating rod 2 is fixedly installed in the evaporation tank 1 through a bolt, the electric heating rod 2 is electrically connected with the electric cabinet 3 through a wire, the solution in the evaporation tank 1 is heated by electrifying the electric heating rod 2, the solution is evaporated for crystallization, the recovery tank 4 is fixedly installed at the bottom of one side of the evaporation tank 1 through a bolt, the input end at the top of the recovery tank 4 is fixedly connected with the output end at the top of one side of the evaporation tank 1 through a guide pipe 6, a condensing pipe 7 is sleeved, condenser pipe 7 on pipe 6 carries out the condensation to steam and becomes liquid, liquid flows into and collects the recycle inside recovery box 4, there is cooling circulation box 5 in recovery box 4's front through bolt fixed mounting, the output fixed connection of hose and condenser pipe 7 is passed through to recovery box 4's input, the input fixed connection of hose and condenser pipe 7 is passed through to recovery box 4's output, cooling circulation box 5 carries out the circulative cooling to the inside cold water 702 of condenser pipe 7, there is electric cabinet 3 in one side that recovery box 4 was kept away from to evaporating pot 1 through bolt fixed mounting, electric cabinet 3 carries out power supply control to the device.
Further, a liquid outlet 401 is arranged at the bottom of the recycling tank 4, a valve 402 is fixedly mounted on the surface of the liquid outlet 401 through a thread structure, and the valve 402 is screwed to discharge the liquid in the recycling tank 4 from the liquid outlet 401.
Further, a NewKP micro circulating water pump 501 is fixedly installed at the inner top of the circulating cooling tank 5 through bolts, the NewKP micro circulating water pump 501 is electrically connected with the electric cabinet 3 through a lead, the input end of the NewKP micro circulating water pump 501 is fixedly connected with the input end of the circulating cooling tank 5, a B3-014 micro heat exchanger 502 is fixedly installed at the inner bottom of the circulating cooling tank 5 through bolts, the B3-014 micro heat exchanger 502 is electrically connected with the electric cabinet 3 through a lead, the input end of the B3-014 micro heat exchanger 502 is fixedly connected with the output end of the NewKP micro circulating water pump 501 through a hose, the output end of the B3-014 micro heat exchanger 502 is fixedly connected with the output end of the circulating cooling tank 5, the NewKP micro circulating water pump 501 circulates cold water 702, the warmed cold water 702 is cooled again through the B3-014 micro heat exchanger 502 and the B3-014 micro heat exchanger 502 during the circulation of the cold water 702 and then is discharged into the storage cavity 701 again, keeping the cold water 702 inside the storage chamber 701 at a constant temperature continues to condense the gas.
Further, a storage chamber 701 is provided on an inner wall of the condensation duct 7, cold water 702 is stored in the storage chamber 701, and the cold water 702 condenses the gas entering the inside of the duct 6 into liquid.
Further, one side at 1 top of evaporating pot is equipped with filler 101, there is top cap 102 at the top of filler 101 through helicitic texture fixed mounting, add chemical reagent through filler 101 to 1 inside of evaporating pot, then cover top cap 102 and seal, the bottom of evaporating pot 1 is equipped with bin outlet 103, there is bottom 104 bottom the bottom of bin outlet 103 through helicitic texture fixed mounting, a week of bottom 104 is equipped with anti-skidding line 105, 1 inside liquid evaporation crystallization of evaporating pot is accomplished the back, back 104 is unscrewed, 1 inside crystallization of evaporating pot is discharged from bin outlet 103, anti-skidding line 105 prevents that people from appearing sliding when twisting bottom 104.
Further, the front of the electric cabinet 3 is provided with a first control switch 301, a second control switch 302 and a third control switch 303, the first control switch 301, the second control switch 302 and the third control switch 303 control the working states of the electric heating rod 2, the NewKP micro circulating water pump 501 and the B3-014 micro heat exchanger 502, the bottom of one side of the electric cabinet 3 is fixedly provided with a plug 304 through a wire, and the electric cabinet 3 is connected with a power supply through the plug 304.
The working principle is as follows: firstly, liquid is added into an evaporation tank 1 through a liquid filling port 101, then a top cover 102 is covered for sealing, then the liquid is connected with a power supply of an electric cabinet 3 through a plug 304, then an electric heating rod 2 is controlled through a first control switch 301 to heat the liquid, the liquid is evaporated and crystallized under the action of high temperature, then evaporated gas enters a conduit 6 through the conduit, a condensing tube 7 on the conduit 6 condenses steam into liquid, the liquid flows into a recovery tank 4 for collection and reuse, in the process, a NewKP micro circulating water pump 501 and a B3-014 micro heat exchanger 502 are controlled through a second control switch 302 and a third control switch 303 to work, the NewKP micro circulating water pump 501 circulates cold water 702 in a storage cavity 701, the heated cold water 702 is cooled again through the B3-014 micro heat exchanger 502 and the B3-014 micro heat exchanger 502 in the circulation process of the cold water 702 and then is discharged into the storage cavity 701 again, the cold water 702 inside the storage chamber 701 is kept at a constant temperature, the gas is continuously condensed, and then the valve 402 is turned to discharge the liquid inside the recovery tank 4 from the liquid outlet 401.
It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (6)
1. The utility model provides a chemical reagent preparation is with crystallization device, includes evaporating pot (1), electric hot rod (2), electric cabinet (3), collection box (4) and circulative cooling case (5), its characterized in that: the utility model discloses an evaporation tank, including evaporating pot (1), condenser, supporting leg (8), non-slip mat (9) are pasted to the bottom of supporting leg (8), one side fixed mounting that evaporating pot (1) kept away from one side of evaporating pot (1) has collection box (4) fixed mounting, the input at collection box (4) top passes through pipe (6) and the output fixed connection at evaporating pot (1) one side top, the surface cover of pipe (6) has condenser pipe (7), the positive fixed mounting of collection box (4) has circulative cooling case (5), the input of collection box (4) passes through the output fixed connection of hose and condenser pipe (7), the output of collection box (4) passes through the input fixed connection of hose and condenser pipe (7), the bottom fixed mounting of evaporating pot (1) has supporting leg (8), non-slip mat (9) is pasted to the bottom of supporting leg (8), one side fixed mounting that evaporating pot (1) kept away from collection box (4) has electric cabinet, the electric heating rod (2) is electrically connected with the electric cabinet (3) through a wire.
2. The crystallization apparatus for chemical reagent preparation according to claim 1, wherein: the bottom of collection box (4) is equipped with liquid outlet (401), and the fixed surface of liquid outlet (401) installs valve (402).
3. The crystallization apparatus for chemical reagent preparation according to claim 1, wherein: the novel KP micro circulating water pump (501) is fixedly installed at the inner top of the circulating cooling box (5), the novel KP micro circulating water pump (501) is electrically connected with the electric control box (3) through a lead, the input end of the novel KP micro circulating water pump (501) is fixedly connected with the input end of the circulating cooling box (5), the B3-014 micro heat exchanger (502) is fixedly installed at the inner bottom of the circulating cooling box (5), the B3-014 micro heat exchanger (502) is electrically connected with the electric control box (3) through a lead, the input end of the B3-014 micro heat exchanger (502) is fixedly connected with the output end of the novel KP micro circulating water pump (501) through a hose, and the output end of the B3-014 micro heat exchanger (502) is fixedly connected with the output end of the circulating cooling box (5).
4. The crystallization apparatus for chemical reagent preparation according to claim 1, wherein: the inner wall of the condensation pipe (7) is provided with a storage cavity (701), and cold water (702) is stored in the storage cavity (701).
5. The crystallization apparatus for chemical reagent preparation according to claim 1, wherein: one side at evaporating pot (1) top is equipped with filling opening (101), and the top fixed mounting of filling opening (101) has top cap (102), the bottom of evaporating pot (1) is equipped with bin outlet (103), and the bottom fixed mounting of bin outlet (103) has bottom (104), and a week of bottom (104) is equipped with anti-skidding line (105).
6. The crystallization apparatus for chemical reagent preparation according to claim 1, wherein: the front of electric cabinet (3) is equipped with first control switch (301), second control switch (302) and third control switch (303), there is plug (304) bottom of electric cabinet (3) one side through wire fixed mounting.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922404779.4U CN211752617U (en) | 2019-12-27 | 2019-12-27 | Crystallization device for chemical reagent preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922404779.4U CN211752617U (en) | 2019-12-27 | 2019-12-27 | Crystallization device for chemical reagent preparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN211752617U true CN211752617U (en) | 2020-10-27 |
Family
ID=72980703
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201922404779.4U Expired - Fee Related CN211752617U (en) | 2019-12-27 | 2019-12-27 | Crystallization device for chemical reagent preparation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN211752617U (en) |
-
2019
- 2019-12-27 CN CN201922404779.4U patent/CN211752617U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20201027 |
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| CF01 | Termination of patent right due to non-payment of annual fee |