CN207950692U - A kind of epoxychloropropane separator - Google Patents
A kind of epoxychloropropane separator Download PDFInfo
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- CN207950692U CN207950692U CN201820170363.3U CN201820170363U CN207950692U CN 207950692 U CN207950692 U CN 207950692U CN 201820170363 U CN201820170363 U CN 201820170363U CN 207950692 U CN207950692 U CN 207950692U
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- reaction kettle
- epoxychloropropane
- refrigerator
- blender
- evaporator
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Abstract
The utility model discloses a kind of epoxychloropropane separators, including reaction kettle, the bottom of the reaction kettle is equipped with discharge outlet, airscoop shroud is installed at the top of the inside of the reaction kettle, the oblique upper of the evaporator is equipped with mixed liquor and mouth is added, the refrigerator side is equipped with control panel, and refrigerator pipe is equipped on the refrigerator, and one end of the refrigerator pipe is equipped with connector.There are two evaporators for the side installation of the reaction kettle of the utility model, mixed liquor of epoxychloropropane water can be evaporated gasification by it, mixed gas enters in reaction kettle, cold air can be manufactured by refrigerator to be discharged into reaction kettle, the temperature in reaction kettle can be controlled by temperature sense bar, to which the different condensation temperatures of epoxychloropropane and water detach epoxychloropropane and water, separating effect can be improved with continual multi-cycle separation by such closed control.
Description
Technical field
The utility model is related to separator field, specifically a kind of epoxychloropropane separator.
Background technology
Currently, often making to carry out condensation reaction as raw material using epoxychloropropane during preparing glycolylurea, anti-
Due to will appear heating during answering, the vapor in epoxychloropropane can be caused to volatilize, however epoxychloropropane is molten
In water, so the loss of epoxychloropropane can be carried during miscellaneous vapor volatilizees, carried in the vapor evaporated
Epoxychloropropane can have following two points：First, the waste that can lead to raw material, improves production cost；Secondly, epoxy chlorine
Propane directly evaporate into air and pollutes the environment, and separator is that mixed substance is separated into two or more is different
The machine of substance, separator are wanted that good separating effect can be kept, need to be controlled its liquid level and pressure.Conventional separators liquid
The control of position and pressure uses constant DP control technology.In the pressure changeable level control of separator, float liquid level controller is utilized
The gentle regulating valve of oil is driven, its teamwork is made, the liquid measure of former oil and gas is controlled, completes the tune to liquid level in separator
Section, controls without the pressure to separator.
A kind of appearance of epoxychloropropane separator greatly facilitates the separation of epoxychloropropane water, but the current stage
A kind of epoxychloropropane separator there are many shortcomings, for example, inferior separating effect, can not circulation continuous separation,
Universal performance is poor.
Utility model content
The purpose of this utility model is to provide a kind of epoxychloropropane separators, to solve separation in the prior art
Effect is poor, can not circulation continuous separation, the problem of universal performance difference.
To achieve the above object, the utility model provides the following technical solutions：A kind of epoxychloropropane separator, including
The bottom of reaction kettle, the reaction kettle is equipped with discharge outlet, and airscoop shroud is equipped at the top of the inside of the reaction kettle, described anti-
Answer the top of kettle that connecting tube is installed, the connecting tube top is equipped with epoxychloropropane gas collection tank, the reaction kettle
Side is equipped with evaporator and mixed gas and is added mouth, and the inside of the evaporator is equipped with blender, the blender it is outer
Side is equipped with fixed frame, and heating tube is equipped on the fixed frame, and one end of the blender is equipped with motor, the evaporator
Oblique upper mixed liquor is installed mouth is added, the interior side of the reaction kettle is equipped with cold air outlet and temperature sense bar, institute
The other side for stating reaction kettle is equipped with refrigerator, and the refrigerator side is equipped with control panel, is equipped on the refrigerator
One end of refrigerator pipe, the refrigerator pipe is equipped with connector.
Preferably, the temperature sense bar output end is electrically connected with control panel input terminal.
Preferably, the connector is mounted on the top of cold air outlet.
Preferably, there are two the evaporator is arranged altogether, and two evaporators are installed in the side of reaction kettle.
Preferably, the blender is cylindrical structure, and there are six fixed frames for installation on blender.
Compared with prior art, the utility model has the beneficial effects that：The side of the reaction kettle of the utility model is equipped with
The mixed liquor of epoxychloropropane water can be evaporated gasification by two evaporators by it, and mixed gas enters in reaction kettle,
Cold air can be manufactured by refrigerator to be discharged into reaction kettle, and the temperature in reaction kettle can be controlled by temperature sense bar, to
The different condensation temperatures of epoxychloropropane and water detach epoxychloropropane and water, can be continued by such closed control
Continuous multi-cycle separation improves separating effect, and epoxychloropropane is collected by airscoop shroud to epoxychloropropane gas collection
In tank, mouth, which is added, in evaporator and mixed gas to detach the epoxychloropropane and water of gaseous state and liquid, increases
Versatility.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model.
Fig. 2 is the side view of the blender of the utility model.
In figure：1- epoxychloropropane gas collections tank, 2- connecting tubes, 3- airscoop shrouds, 4- mixed liquors be added mouth, 5- motors,
6- blenders, 7- fixed frames, 8- heating tubes, 9- evaporators, 10- mixed gas be added mouth, 11- reaction kettles, 12- cold air outlets,
13- connectors, 14- refrigerator pipes, 15- refrigerators, 16- control panels, 17- temperature senses bar, 18- discharge outlet.
Specific implementation mode
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
The every other embodiment obtained, shall fall within the protection scope of the present invention.
Please refer to Fig.1~2, in the utility model embodiment, a kind of epoxychloropropane separator, including reaction kettle 11,
The bottom of reaction kettle 11 is equipped with discharge outlet 18, and discharge outlet 18 is used for liquefied water being discharged reaction kettle 11, reaction kettle 11 it is interior
Airscoop shroud 3 is installed, airscoop shroud 3 is used for absorbing epoxychloropropane gas, and the top of reaction kettle 11 is equipped with connection at the top of portion
Pipe 2,2 top of connecting tube are equipped with epoxychloropropane gas collection tank 1, and epoxychloropropane gas collection tank 1 is used for epoxy chlorine
Propane gas is collected, and the side of reaction kettle 11 is equipped with evaporator 9 and mixed gas is added mouth 10, and evaporator 9 is used for pair
Epoxychloropropane water mixed liquid is evaporated gasification, and the inside of evaporator 9 is equipped with blender 6, and blender 6 can increase mixing
The evaporation efficiency of liquid increases the uniformity of heat distribution, and the outside of blender 6 is equipped with fixed frame 7, is installed on fixed frame 7
There are heating tube 8, heating tube 8 to be used for carrying out heating evaporation to mixing liquid, one end of blender 6 is equipped with motor 5, and motor 5 is used
Blender 6 is driven to be rotated, the oblique upper of evaporator 9 is equipped with mixed liquor and mouth 4, the interior side peace of reaction kettle 11 is added
Equipped with cold air outlet 12 and temperature sense bar 17, the other side of reaction kettle 11 is equipped with refrigerator 15, and refrigerator 15 is used for freezing,
And be delivered to cold air at cold air outlet 12 by refrigerator pipe 14, cold air is discharged into reaction kettle 11 by cold air outlet 12, is made
15 side of cooler is equipped with control panel 16, and refrigerator pipe 14 is equipped on refrigerator 15, and temperature sense bar 17 is used for reaction kettle
Temperature in 11 is measured in real time, and one end of refrigerator pipe 14 is equipped with connector 13,17 output end of temperature sense bar and control plane
16 input terminal of plate is electrically connected, and connector 13 is mounted on the top of cold air outlet 12, and there are two the total settings of evaporator 9, and two steamings
Hair tank 9 is installed in the side of reaction kettle 11, and blender 6 is cylindrical structure, and there are six fixed frames 7 for installation on blender 6.
The operation principle of the utility model is：The equipment is added by mixed liquor when in use, by epoxychloropropane water mixed liquid
Entrance 4 is added in evaporator 9, and controlling blender 6 by motor 5 rotates, by blender 6 to the mixing liquid in evaporator 9
It is mixed, while the mixing liquid in evaporator 9 is evaporated by the heating tube in the outside of blender 68, mixed vapour
It is discharged into reaction kettle 11, while the temperature in reaction kettle 11 is detected by temperature sense bar 17, be then transmitted to detection information
On control panel 16, refrigerator 15 is controlled by control panel 16 and manufactures cold air, and cold air outlet is delivered to by refrigerator pipe 14
At 12, it is delivered in reaction kettle 11 by cold air outlet 12, until the temperature in reaction kettle 11 keeps water vapour condensable, and epoxy
Chloropropane does not condense, and water is discharged by discharge outlet 18 after liquefaction, and gaseous epoxychloropropane is collected by airscoop shroud 3 to epoxychloropropane
Caching in gas collection tank 1.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and
And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this practicality is new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this practicality is new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing in the equivalent requirements of the claims will be fallen
All changes in justice and range are embraced therein.Any reference numeral in claim should not be considered as limitation
Involved claim.
Claims (5)
1. a kind of epoxychloropropane separator, including reaction kettle (11), it is characterised in that：Pacify the bottom of the reaction kettle (11)
Equipped with discharge outlet (18), airscoop shroud (3), the top of the reaction kettle (11) are installed at the top of the inside of the reaction kettle (11)
Connecting tube (2) is installed, connecting tube (2) top is equipped with epoxychloropropane gas collection tank (1), the reaction kettle (11)
Side evaporator (9) and mixed gas are installed mouth (10) are added, the inside of the evaporator (9) is equipped with blender (6),
Fixed frame (7) is installed on the outside of the blender (6), heating tube (8), the blender are installed on the fixed frame (7)
(6) one end is equipped with motor (5), and the oblique upper of the evaporator (9) is equipped with mixed liquor and mouth (4), the reaction kettle is added
(11) interior side is equipped with cold air outlet (12) and temperature sense bar (17), and the other side of the reaction kettle (11) is equipped with
Refrigerator (15), refrigerator (15) side are equipped with control panel (16), refrigerator pipe are equipped on the refrigerator (15)
(14), one end of the refrigerator pipe (14) is equipped with connector (13).
2. a kind of epoxychloropropane separator according to claim 1, it is characterised in that：The temperature sense bar (17)
Output end is electrically connected with control panel (16) input terminal.
3. a kind of epoxychloropropane separator according to claim 1, it is characterised in that：The connector (13) is mounted on
The top of cold air outlet (12).
4. a kind of epoxychloropropane separator according to claim 1, it is characterised in that：The evaporator (9) sets altogether
There are two setting, and two evaporators (9) are installed in the side of reaction kettle (11).
5. a kind of epoxychloropropane separator according to claim 1, it is characterised in that：The blender (6) is circle
Column construction, and there are six fixed frames (7) for installation on blender (6).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820170363.3U CN207950692U (en) | 2018-01-31 | 2018-01-31 | A kind of epoxychloropropane separator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820170363.3U CN207950692U (en) | 2018-01-31 | 2018-01-31 | A kind of epoxychloropropane separator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207950692U true CN207950692U (en) | 2018-10-12 |
Family
ID=63736319
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820170363.3U Active CN207950692U (en) | 2018-01-31 | 2018-01-31 | A kind of epoxychloropropane separator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207950692U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115400546A (en) * | 2022-09-01 | 2022-11-29 | 山东神驰石化有限公司 | Persistent separating tower for normal butane and isobutane in normal butane isomerization |
-
2018
- 2018-01-31 CN CN201820170363.3U patent/CN207950692U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115400546A (en) * | 2022-09-01 | 2022-11-29 | 山东神驰石化有限公司 | Persistent separating tower for normal butane and isobutane in normal butane isomerization |
| CN115400546B (en) * | 2022-09-01 | 2023-08-25 | 山东神驰石化有限公司 | Persistent separation tower for n-butane and isobutane in n-butane isomerism |
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